Two kinds of nanopowders were studied.One is NiFe 2O 4 spherical nanopowders which have different particle sizes.Another is ZnO nanopowders including two series of spherical particles and tetrapod nanowhiskers.Through...Two kinds of nanopowders were studied.One is NiFe 2O 4 spherical nanopowders which have different particle sizes.Another is ZnO nanopowders including two series of spherical particles and tetrapod nanowhiskers.Through measuring the infrared diffuse reflection spectra of nanopowders,it can be found that the particle size and morphology affect the infrared diffuse reflection spectra.For the NiFe 2O 4 nanopowders the smaller the particle size,the larger the K-M value.And when the particle size is large enough,the effect of the particle size on infrared diffuse reflection spectra would disappear.For the ZnO nanopowders the effects of the particle size and morphology are more special.The effect of the particle sizes of tetrapod whisker nanopowders on infrared diffuse reflection spectra is more than that of spherical nanopowders.展开更多
Barium (Bag) ferrite ultra fine powders were synthesized by using sol-gel in which polyethylene glycol 200(PEG200) was used as gelling agent. The transition of Ba ferrite was studied by thermal gravimetric and differe...Barium (Bag) ferrite ultra fine powders were synthesized by using sol-gel in which polyethylene glycol 200(PEG200) was used as gelling agent. The transition of Ba ferrite was studied by thermal gravimetric and differential thermal analysis (TG-DTA) technology. The micro structural changes were analyzed using X-ray diffraction (XRD) and atomic force microscopy (AFM) for the specimens annealed at different temperatures. The transition temperatures were 414.55°C and separately corresponding to BaFe2O4 and BaFe,2O19. There were three types of microstructures for Ba ferrite ultrafine powder specimen annealed at 800°C. For the specimens annealed at different temperatures, there were different kinds of Ba ferrites. The ferrite powder consists of BaFet2O19 and BaFe2O4 for the specimen annealed at 800°C, and only BaFe^O^ can be found in the specimen annealed at 1000°C. The magnetic properties, a , and H c of BaFC|2O19 ultrafine powders are different from that of BaFe12O19 bulk material.展开更多
文摘Two kinds of nanopowders were studied.One is NiFe 2O 4 spherical nanopowders which have different particle sizes.Another is ZnO nanopowders including two series of spherical particles and tetrapod nanowhiskers.Through measuring the infrared diffuse reflection spectra of nanopowders,it can be found that the particle size and morphology affect the infrared diffuse reflection spectra.For the NiFe 2O 4 nanopowders the smaller the particle size,the larger the K-M value.And when the particle size is large enough,the effect of the particle size on infrared diffuse reflection spectra would disappear.For the ZnO nanopowders the effects of the particle size and morphology are more special.The effect of the particle sizes of tetrapod whisker nanopowders on infrared diffuse reflection spectra is more than that of spherical nanopowders.
文摘Barium (Bag) ferrite ultra fine powders were synthesized by using sol-gel in which polyethylene glycol 200(PEG200) was used as gelling agent. The transition of Ba ferrite was studied by thermal gravimetric and differential thermal analysis (TG-DTA) technology. The micro structural changes were analyzed using X-ray diffraction (XRD) and atomic force microscopy (AFM) for the specimens annealed at different temperatures. The transition temperatures were 414.55°C and separately corresponding to BaFe2O4 and BaFe,2O19. There were three types of microstructures for Ba ferrite ultrafine powder specimen annealed at 800°C. For the specimens annealed at different temperatures, there were different kinds of Ba ferrites. The ferrite powder consists of BaFet2O19 and BaFe2O4 for the specimen annealed at 800°C, and only BaFe^O^ can be found in the specimen annealed at 1000°C. The magnetic properties, a , and H c of BaFC|2O19 ultrafine powders are different from that of BaFe12O19 bulk material.
