The steady state creep rate equdtion of a nickel base superalloy Inconel 718, strengthened by coherent ordered disc-shaped bct γ^(11) phase and coherent spherical fcc γ~1 phase precipitates, has been established in ...The steady state creep rate equdtion of a nickel base superalloy Inconel 718, strengthened by coherent ordered disc-shaped bct γ^(11) phase and coherent spherical fcc γ~1 phase precipitates, has been established in the stress and temperature ranges of 620-840 MN m^(-2) and 853-943K, respecti- vely. Constant stress tensile creep tests were used to medsure the values of steady state creep rate, ε_s, and the consecutive stress reduction method was used to measure the back stress during creep deformation. The values of effective stress exponent, n_e, were detemined from the slopes of the lgε_s vs. lg(σ_a-σ_0)/G plots. The effect of grain size, d, on steady state creep rdte has been also studied in this investigation, and the grain size sensitive exponents m were detemined from the slopes of lgε_s vs. lg(b/d) plots. The creep rate equations of Inconel 718, in the above stress and temperature ranges, have been proposed to be ε_s=1.6×10^(-5)(D_1Gb/KT) (b/d )^(0.19)[(σ_a-σ_0)/G]^(1.35) in diffusional creep region, and ε_s =75(D_1Gb/KT) (b/d)^(-0.42)[(σ_a-σ_0)/G]^(5.5) in dislocation power law creep region.展开更多
The strain rate sensitivity to creep of single crystal Cu（110）, metal tantalum, and 128°Y-X LiNbO3 piezoelectric single crystal were measured at room temperature by MTS Nanoindenter XP. Among the three kinds of...The strain rate sensitivity to creep of single crystal Cu（110）, metal tantalum, and 128°Y-X LiNbO3 piezoelectric single crystal were measured at room temperature by MTS Nanoindenter XP. Among the three kinds of materials studied, Cu showed the highest degree of resistance to creep-induced deformation, which is followed by Ta, while the LiNbO3 single crystal deformed more readily than the others. The values of the steady-state strain rate sensitivities determined by the indentation methods are in the range of 0.002-0.006, 0.02-0.06 and 0.02-0.03 for Cu, Ta, and LiNbO3, respectively. The mechanisms for the indentation-induced creeping behavior and the factors that influenced the creeping are discussed.展开更多
Mg-Gd-Zn based alloys have better creep resistance than other Mg alloys and attract more attention at elevated temperatures.However,the multiple alloying elements and various heat treatment conditions,combined with co...Mg-Gd-Zn based alloys have better creep resistance than other Mg alloys and attract more attention at elevated temperatures.However,the multiple alloying elements and various heat treatment conditions,combined with complex microstructural evolution during creep tests,bring great challenges in understanding and predicting creep behaviors.In this study,we proposed to predict the creep properties and reveal the creep mechanisms of Mg-Gd-Zn based alloys by machine learning.On the one hand,the minimum creep rates were effectively predicted by using a support vector regression model.The complex and nonmonotonic effects of test temperature,test stress,alloying elements,and heat treatment conditions on the creep properties were revealed.On the other hand,the creep stress exponents and creep activation energies were calculated by machine learning to analyze the variation of creep mechanisms,based on which the constitutive equations of Mg-Gd-Zn based alloys were obtained.This study introduces an efficient method to comprehend creep behaviors through machine learning,offering valuable insights for the future design and selection of Mg alloys.展开更多
G115 steel was jointly developed by China Iron & Steel Research Institute Group Co.,Ltd.and Baosteel for usage in 600-650 ℃ ultrasupercritical boiler tubes.Using a hot extruded G115 tube,creep tests were conducte...G115 steel was jointly developed by China Iron & Steel Research Institute Group Co.,Ltd.and Baosteel for usage in 600-650 ℃ ultrasupercritical boiler tubes.Using a hot extruded G115 tube,creep tests were conducted under a constant stress of 130 MPa and temperatures of 625,650 and 675 ℃.Comparing creep curves under different temperatures,it is observed that the creep performance of a G115 tube is more sensitive to temperature than stress.Steady-state creep rates of creep specimens are significantly increased by enhancing the temperature.A micro-structural analysis of ruptured creep specimens under a stress of 130 MPa and temperatures of 650 ℃ and 675 ℃ was performed;the fracture mechanism of creep specimens under these two temperatures mainly included the appearance of creep holes on the grain boundary and a decrease in the martensite lath density.展开更多
Traditionally the deformation resistance in creep is characterized by the minimum creep rate εmin and its sensitivity to stress （stress exponent n） and temperature （activation energy Q）. Various values of constan...Traditionally the deformation resistance in creep is characterized by the minimum creep rate εmin and its sensitivity to stress （stress exponent n） and temperature （activation energy Q）. Various values of constant n have been reported in the literature and interpreted in terms of specific mechanisms. The present case study of coarse-grained Cu at 573 K yields a stress exponent n = 9 for εmin. in tension and a relatively low activation energy. The evolution of the deformation resistance with strain at constant tensile creep load and comparison with creep in compression without fracture indicates that the tensile εmin. result from transition from uniform deformation to strain localization during fracture. This is confirmed by the results of creep in compression where fracture is suppressed. Both the tensile εmin, and the compressive creep rate at strains around 0.3 can be described using existing equations for quasi-stationary deformation containing the subgrain boundary misorientation θ as structure parameter. While in the latter case constant θ leads to monotonic increase of n with stress, the tensile nine-power-law results from variable θ, and has no simple meaning. The result of this case study means that uncritical interpretation of minimum tensile creep rates as stationary ones bears a high risk of systematic errors in the determination of creep parameters and identification of creep mechanisms.展开更多
The effect of cooling rate during quenching on the microstructure and creep property of nickel-based superalloy FGH96 was investigated. Three groups of samples were quenched continuously with three fixed cooling rates...The effect of cooling rate during quenching on the microstructure and creep property of nickel-based superalloy FGH96 was investigated. Three groups of samples were quenched continuously with three fixed cooling rates, respectively, then subjected to a creep test under a constant load of 690 MPa at 700℃. Clear differences in size of secondary γ′ precipitates, creep properties and substructure of creep-tested samples were observed. The quantitative relationship among cooling rate, the size of secondary γ′ precipitates, and steady creep rate was constructed. It was found that with increasing cooling rate, the size of secondary γ′ precipitates decreases gradually, showing that the relationship between the size of secondary γ′ precipitates and the cooling rate obeys a power law, with an exponent of about –0.6, and the creep rate of steady state follows a good parabola relationship with cooling γ′ precipitate size. For 235℃/min, FGH96 alloy exhibited very small steady creep rate. The density of dislocation was low, and the isolated stacking fault was the dominant deformation mechanism. With decreasing cooling rates, the density of dislocation increased remarkably, and deformation microtwinning was the dominant deformation process. Detailed mechanisms for different cooling rate were discussed.展开更多
Instantaneous creep in face-centered cubic metals, 5N Al（99.999%）, 2N Al （99%） and 4N Cu （99.99%） with different grain sizes, was firstly investigated by sudden stress-change experiments at ultra- low strain rat...Instantaneous creep in face-centered cubic metals, 5N Al（99.999%）, 2N Al （99%） and 4N Cu （99.99%） with different grain sizes, was firstly investigated by sudden stress-change experiments at ultra- low strain rates ε ≤10-10 s-1 and temperature T 〈 0.32 Tn. The experimental results indicate that the observed instantaneous creep is strongly dependent on grain size, the concentration of impurity, and stacking fault energy. Creep in high-purity aluminum, 5N Al, with a very large grain size, d 〉 1600μm, shows non-viscous behavior, and is controlled by the recovery of dislocations in the boundary of dislocation cells. On the other hand, for 5N A1 with a small grain size, d=30μm, and low-purity aluminum, 2N A1, with d8= 25μm, creep shows viscous behavior and may be related to ＇low temperature grain boundary sliding＇. For high-purity copper, 4N Cu, with d= 40 grn and lower stacking fault energy, creep shows a non-viscous behavior, and is controlled by the recovery process of dislocations. For all of the samples, creep shows anelastic behavior.展开更多
The influence of two different grain shapes and carbides in the HK40 alloy,the material for use of furnace tube,on the rate of creep crack growth has been investigated.The resistance to creep crack growth of the mater...The influence of two different grain shapes and carbides in the HK40 alloy,the material for use of furnace tube,on the rate of creep crack growth has been investigated.The resistance to creep crack growth of the material with columnar grains is inferior than that with equiaxial grains when the load line is perpendicular to the columnar grain axis.The influence of secon- dary carbide on the rate of creep crack propagation depends upon the Brain shape.展开更多
The creep and fracture behavior of the cast K417 and forged GH4049 nickel-based superalloys were investigated in the temperature range of 700-900℃ C. Within the ranges of stress and temperature studied, the steady st...The creep and fracture behavior of the cast K417 and forged GH4049 nickel-based superalloys were investigated in the temperature range of 700-900℃ C. Within the ranges of stress and temperature studied, the steady state creep rates exhibited a power law relationship with the applied stress and temperature. The time to rupture is inversely proportional to the steady state creep rate. Under all testing conditions, the creep fracture process was mainly controled by crack initiation and growth of the intergranular oxidation. Casting porosities, pores and carbides were also prefecentral locations of creep crack initiation in the cast K417 alloy. In addition, the intergranular fracture feature in the forged GH4049 alloy was apparently associated with the formation and coalescence of the cavitations on the grain boundaries.展开更多
文摘The steady state creep rate equdtion of a nickel base superalloy Inconel 718, strengthened by coherent ordered disc-shaped bct γ^(11) phase and coherent spherical fcc γ~1 phase precipitates, has been established in the stress and temperature ranges of 620-840 MN m^(-2) and 853-943K, respecti- vely. Constant stress tensile creep tests were used to medsure the values of steady state creep rate, ε_s, and the consecutive stress reduction method was used to measure the back stress during creep deformation. The values of effective stress exponent, n_e, were detemined from the slopes of the lgε_s vs. lg(σ_a-σ_0)/G plots. The effect of grain size, d, on steady state creep rdte has been also studied in this investigation, and the grain size sensitive exponents m were detemined from the slopes of lgε_s vs. lg(b/d) plots. The creep rate equations of Inconel 718, in the above stress and temperature ranges, have been proposed to be ε_s=1.6×10^(-5)(D_1Gb/KT) (b/d )^(0.19)[(σ_a-σ_0)/G]^(1.35) in diffusional creep region, and ε_s =75(D_1Gb/KT) (b/d)^(-0.42)[(σ_a-σ_0)/G]^(5.5) in dislocation power law creep region.
基金This work was financially supported by the National Natural Science Foundation of China (No.90406024).
文摘The strain rate sensitivity to creep of single crystal Cu（110）, metal tantalum, and 128°Y-X LiNbO3 piezoelectric single crystal were measured at room temperature by MTS Nanoindenter XP. Among the three kinds of materials studied, Cu showed the highest degree of resistance to creep-induced deformation, which is followed by Ta, while the LiNbO3 single crystal deformed more readily than the others. The values of the steady-state strain rate sensitivities determined by the indentation methods are in the range of 0.002-0.006, 0.02-0.06 and 0.02-0.03 for Cu, Ta, and LiNbO3, respectively. The mechanisms for the indentation-induced creeping behavior and the factors that influenced the creeping are discussed.
基金supported by the National Science and Technology Major Project(Grant number J2019-VI-0004-0118)the National Natural Science Foundation of China(Grant number 51771152)+2 种基金the National Key R&D Program of China(Grant number 2018YFB1106800)supported by the Brain Pool Program through the National Research Foundation of Korea(NRF)(Grant No.RS-2023-00304296)supported by the Brain Pool Program through National Research Foundation of Korea(NRF)(Grant No.RS-2023-00222130).
文摘Mg-Gd-Zn based alloys have better creep resistance than other Mg alloys and attract more attention at elevated temperatures.However,the multiple alloying elements and various heat treatment conditions,combined with complex microstructural evolution during creep tests,bring great challenges in understanding and predicting creep behaviors.In this study,we proposed to predict the creep properties and reveal the creep mechanisms of Mg-Gd-Zn based alloys by machine learning.On the one hand,the minimum creep rates were effectively predicted by using a support vector regression model.The complex and nonmonotonic effects of test temperature,test stress,alloying elements,and heat treatment conditions on the creep properties were revealed.On the other hand,the creep stress exponents and creep activation energies were calculated by machine learning to analyze the variation of creep mechanisms,based on which the constitutive equations of Mg-Gd-Zn based alloys were obtained.This study introduces an efficient method to comprehend creep behaviors through machine learning,offering valuable insights for the future design and selection of Mg alloys.
文摘G115 steel was jointly developed by China Iron & Steel Research Institute Group Co.,Ltd.and Baosteel for usage in 600-650 ℃ ultrasupercritical boiler tubes.Using a hot extruded G115 tube,creep tests were conducted under a constant stress of 130 MPa and temperatures of 625,650 and 675 ℃.Comparing creep curves under different temperatures,it is observed that the creep performance of a G115 tube is more sensitive to temperature than stress.Steady-state creep rates of creep specimens are significantly increased by enhancing the temperature.A micro-structural analysis of ruptured creep specimens under a stress of 130 MPa and temperatures of 650 ℃ and 675 ℃ was performed;the fracture mechanism of creep specimens under these two temperatures mainly included the appearance of creep holes on the grain boundary and a decrease in the martensite lath density.
基金supported by the project CZ.1.05/1.1.00/02.0068 granted by the European Regional Development Fund
文摘Traditionally the deformation resistance in creep is characterized by the minimum creep rate εmin and its sensitivity to stress （stress exponent n） and temperature （activation energy Q）. Various values of constant n have been reported in the literature and interpreted in terms of specific mechanisms. The present case study of coarse-grained Cu at 573 K yields a stress exponent n = 9 for εmin. in tension and a relatively low activation energy. The evolution of the deformation resistance with strain at constant tensile creep load and comparison with creep in compression without fracture indicates that the tensile εmin. result from transition from uniform deformation to strain localization during fracture. This is confirmed by the results of creep in compression where fracture is suppressed. Both the tensile εmin, and the compressive creep rate at strains around 0.3 can be described using existing equations for quasi-stationary deformation containing the subgrain boundary misorientation θ as structure parameter. While in the latter case constant θ leads to monotonic increase of n with stress, the tensile nine-power-law results from variable θ, and has no simple meaning. The result of this case study means that uncritical interpretation of minimum tensile creep rates as stationary ones bears a high risk of systematic errors in the determination of creep parameters and identification of creep mechanisms.
基金financially supported by the National Material Special Program of China (No. JPPT-F2008-5-1)
文摘The effect of cooling rate during quenching on the microstructure and creep property of nickel-based superalloy FGH96 was investigated. Three groups of samples were quenched continuously with three fixed cooling rates, respectively, then subjected to a creep test under a constant load of 690 MPa at 700℃. Clear differences in size of secondary γ′ precipitates, creep properties and substructure of creep-tested samples were observed. The quantitative relationship among cooling rate, the size of secondary γ′ precipitates, and steady creep rate was constructed. It was found that with increasing cooling rate, the size of secondary γ′ precipitates decreases gradually, showing that the relationship between the size of secondary γ′ precipitates and the cooling rate obeys a power law, with an exponent of about –0.6, and the creep rate of steady state follows a good parabola relationship with cooling γ′ precipitate size. For 235℃/min, FGH96 alloy exhibited very small steady creep rate. The density of dislocation was low, and the isolated stacking fault was the dominant deformation mechanism. With decreasing cooling rates, the density of dislocation increased remarkably, and deformation microtwinning was the dominant deformation process. Detailed mechanisms for different cooling rate were discussed.
基金Funded by the Tianjin Research Program of Application Foundation and Advanced Technology(12JCYBJC32100)the Scientific Research Foundation for the Returned Overseas Chinese Scholars,State Education Ministryin part by Grants-in-Aid from the Japan Society for the Promotion of Science(JSPS)
文摘Instantaneous creep in face-centered cubic metals, 5N Al（99.999%）, 2N Al （99%） and 4N Cu （99.99%） with different grain sizes, was firstly investigated by sudden stress-change experiments at ultra- low strain rates ε ≤10-10 s-1 and temperature T 〈 0.32 Tn. The experimental results indicate that the observed instantaneous creep is strongly dependent on grain size, the concentration of impurity, and stacking fault energy. Creep in high-purity aluminum, 5N Al, with a very large grain size, d 〉 1600μm, shows non-viscous behavior, and is controlled by the recovery of dislocations in the boundary of dislocation cells. On the other hand, for 5N A1 with a small grain size, d=30μm, and low-purity aluminum, 2N A1, with d8= 25μm, creep shows viscous behavior and may be related to ＇low temperature grain boundary sliding＇. For high-purity copper, 4N Cu, with d= 40 grn and lower stacking fault energy, creep shows a non-viscous behavior, and is controlled by the recovery process of dislocations. For all of the samples, creep shows anelastic behavior.
基金the financial supports from the National Key Laboratory of Science and Technology for National Defence on High-Strength Lightweight Structural Materials of China(No.20190104)State Key Laboratory of High-Performance Complex Manufacturing of Central South University,China(No.ZZYJKT2020-03)the National Key Research and Development Program of China(No.2016YFB0300801)。
文摘The influence of two different grain shapes and carbides in the HK40 alloy,the material for use of furnace tube,on the rate of creep crack growth has been investigated.The resistance to creep crack growth of the material with columnar grains is inferior than that with equiaxial grains when the load line is perpendicular to the columnar grain axis.The influence of secon- dary carbide on the rate of creep crack propagation depends upon the Brain shape.
文摘The creep and fracture behavior of the cast K417 and forged GH4049 nickel-based superalloys were investigated in the temperature range of 700-900℃ C. Within the ranges of stress and temperature studied, the steady state creep rates exhibited a power law relationship with the applied stress and temperature. The time to rupture is inversely proportional to the steady state creep rate. Under all testing conditions, the creep fracture process was mainly controled by crack initiation and growth of the intergranular oxidation. Casting porosities, pores and carbides were also prefecentral locations of creep crack initiation in the cast K417 alloy. In addition, the intergranular fracture feature in the forged GH4049 alloy was apparently associated with the formation and coalescence of the cavitations on the grain boundaries.
