The hardening on surface of complex profles such as thread and spline manufactured by cold rolling can efectively improve the mechanical properties and surface quality of rolled parts. The distribution of hardness in ...The hardening on surface of complex profles such as thread and spline manufactured by cold rolling can efectively improve the mechanical properties and surface quality of rolled parts. The distribution of hardness in superfcial layer is closely related to the deformation by rolling. To establish the suitable correlation model for describing the relationship between strain and hardness during cold rolling forming process of complex profles is helpful to the optimization of rolling parameters and improvement of rolling process. In this study, a physical analog experiment refecting the uneven deformation during complex-profle rolling process has been extracted and designed, and then the large date set (more than 400 data points) of training samples refecting the local deformation characteristics of complexprofle rolling have been obtained. Several types of polynomials and power functions were adopted in regression analysis, and the regression correlation models of 45# steel were evaluated by the single-pass and multi-pass physical analog experiments and the complex-profle rolling experiment. The results indicated that the predicting accuracy of polynomial regression model is better in the strain range (i.e., ε < 1.2) of training samples, and the correlation relationship between strain and hardness out strain range (i.e., ε > 1.2) of training samples can be well described by power regression model;so the correlation relationship between strain and hardness during complex-profle rolling process of 45# steel can be characterized by a segmented function such as third-order polynomial in the range ε < 1.2 and power function with a ftting constant in the range ε > 1.2;and the predicting error of the regression model by segmented function is less than 10%.展开更多
The coarsening behaviors of γ″-phase particles in Inconel 718 alloy aged at 750, 800, and 850℃ were investigated by scanning electron microscopy(SEM). Detailed observations and quantitative measurements were conduc...The coarsening behaviors of γ″-phase particles in Inconel 718 alloy aged at 750, 800, and 850℃ were investigated by scanning electron microscopy(SEM). Detailed observations and quantitative measurements were conducted to characterize the coarsening behavior of the γ″-phase under various aging conditions. The experimental results indicate that the existence of the δ-phase retards the formation and coarsening of the γ″-phase, without influencing its final particle size or amount. Moreover, when cold rolled with a reduction of 50%, the dimensions of the γ″ particles in Inconel 718 alloy decrease with increasing aging time. Furthermore, the coarsening behavior of the γ″-phase in the Inconel 718 alloy after a normal aging treatment(sample A) and that of the primary δ-phase(sample B) follow the Lifshitz–Slyozov–Wagner(LSW) diffusion-controlled growth theory; the thus-obtained activation energies for the γ″-phase are 292 k J·mol^(-1)and 302 k J·mol^(-1), respectively.展开更多
A new processing method,equal channel angular pressing(ECAP)plus cold rolling(CR),was applied to producing ultra-fine grained FeCoV alloy.The microstructures of ultra-fine grained FeCoV alloy after ECAP,ECAP plus CR,a...A new processing method,equal channel angular pressing(ECAP)plus cold rolling(CR),was applied to producing ultra-fine grained FeCoV alloy.The microstructures of ultra-fine grained FeCoV alloy after ECAP,ECAP plus CR,and the effect of tempering treatment on the microstructure of FeCoV alloy produced by ECAP plus CR were investigated.The results show that an elongated substructure with a width of about 0.3μm is obtained after four-pass ECAP using Route A.Cold rolling after ECAP cannot change the morphologies of elongated substructure,and it results in higher fraction of high-angle boundaries and higher dislocation density compared with the identical ECAP without rolling.Subsequent tempering for 30 min at 853 K brings about many nano-phases precipitating at subgrain boundaries and insides the grains,and the size of precipitated phase is measured to be about 10 nm.Nano-phases grow up with increasing tempering temperature and equiaxed structure forms at 883 K.展开更多
In order to know the cause of cracks in cold rolling of QSn6.5 0.1 copper alloy strip, a lot of experiments and analysis were done. The microstructure changes of QSn6.5 0.1 were investigated by means of metallurgical ...In order to know the cause of cracks in cold rolling of QSn6.5 0.1 copper alloy strip, a lot of experiments and analysis were done. The microstructure changes of QSn6.5 0.1 were investigated by means of metallurgical microscope. The morphology of cracks and surface defects were examined using scanning electron microscope. Macroscopic residual stresses produced in every process during manufacturing in the QSn6.5 0.1 strip were measured by X ray diffraction method and hole drilling method. The results show that the cracks in the QSn6.5 0.1 cold rolling strip were caused due to the derivation of metallurgical defects, such as SnO 2, S, fine looses,the inverse segregation unable to clear up when milling, and the accumulation of all kinds of resi dual stresses. When the accumulation of the residual stress reaches the material′s breaking strength, the cracks will be generated. Several measures to avoid the development of these kinds of cracks were put forward, such as: controlling the casting technology, improving homogenization annealing procedure (680 ℃/7 h) and milling quality(using the second milling when necessary), working out a more reasonable rolling technology to ensure intermediate annealing in time.展开更多
On the condition of the width to thickness ratio 625 of rolled strip, the asymmetrical cold strip rolling process about the width center is studied by using computer numerical simulation method and experimental method...On the condition of the width to thickness ratio 625 of rolled strip, the asymmetrical cold strip rolling process about the width center is studied by using computer numerical simulation method and experimental method. The simulated results of the transverse distributions of the rolling pressure. the 2-directional frictions and the front and back.tensions agree with the experimental reuslts well. It is an important discovery that the rolling pressure has three peak values across the strip width on the condition of large width to thickness ratio.展开更多
Lubrication in cold rolling process is used not only to control friction,but also to control surface quality and thermal chamber.Successful cold rolling of strip at high speeds requires an optimum presence of lubrican...Lubrication in cold rolling process is used not only to control friction,but also to control surface quality and thermal chamber.Successful cold rolling of strip at high speeds requires an optimum presence of lubricant film thickness at the contact.In order to have a better control on rolling process the awareness for the prediction and maintenance of desired minimum film thickness.On the basis of learning and summarizing the theories early founded by experts around the world,this paper constructed the mixed lubrication model. This paper investigated the lubrication state variation caused by oil and rolling condition differences by cold rolling experiments.The experiments indicated that oil has a big influence to rolling process,and rolling speed directly influence the lubrication state.展开更多
This paper describes the formation mechanism and mode of the emulsion odor of the cold rolling process,and introduces the relevant environmental regulations and methods used to measure the emulsion odor.Studies were c...This paper describes the formation mechanism and mode of the emulsion odor of the cold rolling process,and introduces the relevant environmental regulations and methods used to measure the emulsion odor.Studies were conducted with respect to these issues.The technical measures used to minimize the emulsion odor,particularly the adjustment of the chemical formula of the cold rolling emulsion,are illustrated in detail.The study results have been successfully applied in cold rolling production,and a significant reduction in the emulsion odor is achieved.展开更多
Accurate calculation results of roll temperature are the key factors in rolling cooling and lubricating technology during the single-stand reversing cold rolling process. By combining the high-strength steel rolling e...Accurate calculation results of roll temperature are the key factors in rolling cooling and lubricating technology during the single-stand reversing cold rolling process. By combining the high-strength steel rolling experiments,the numerical simulation of roll temperature,and the influence factors in reversing cold rolling were studied. The research results correspond with those of rolling experiments and show that the research method could provide effective instruction for roll cooling and emulsion flow rate control during the on-site rolling process.展开更多
Aiming at the problem of insufficient prediction accuracy of strip flatness at the outlet of cold tandem rolling,the prediction performance of strip flatness based on different ensemble methods was studied and a high-...Aiming at the problem of insufficient prediction accuracy of strip flatness at the outlet of cold tandem rolling,the prediction performance of strip flatness based on different ensemble methods was studied and a high-precision prediction ensemble model of strip flatness at the outlet was established.Firstly,based on linear regression(LR),K nearest neighbors(KNN),support vector regression,regression trees(RT),and backpropagation neural network(BPN),bagging,boosting,and stacking ensemble methods were used for ensemble experiments.Secondly,three existing ensemble models,i.e.,random forest,extreme random tree(ET)and extreme gradient boosting,were used to conduct experiments and compare the results.The research shows that bagging,boosting,and stacking three ensemble methods have the most significant improvement in the prediction accuracy of the regression trees model,which is increased by 5.28%,6.51%,and 5.32%,respectively.At the same time,the stacking ensemble method improves both the simple model and the complex model,and the improvement effect on the simple base model is the greatest,which is 4.69%higher than that of the base model KNN.Comparing all of the ensemble models,the stacking ensemble model of level-1(ET,AdaBoost-RT,LR,BPN)paired with level-2(LR)was discovered to be the best model(EALB-LR)and can be further studied for industrial applications.展开更多
Severe fluctuation of the effective roll gap in the acceleration and deceleration section of the cold rolling process is a significant factor causing thickness deviation.However,the conventional roll gap compensation ...Severe fluctuation of the effective roll gap in the acceleration and deceleration section of the cold rolling process is a significant factor causing thickness deviation.However,the conventional roll gap compensation method and control strategy do not meet the stringent strip quality requirements.The roll gap model in the acceleration and deceleration process is studied to increase the thickness control precision.In order to improve model accuracy,a roll gap prediction method based on data-driven is proposed.Given the complexities of the cold rolling process,the extreme gradient boosting(XGBoost)method is used to predict the roll gap model as the rolling speed changes.Meanwhile,support vector regression and neural network-based methods are taken to evaluate and compare the prediction performances.Based on the field data,the simulation experiments are carried out.It demonstrated that the prediction performance of the proposed method outperformed the other two methods.The values of root mean square error,determination coefficient value,mean absolute percentage error and mean absolute error obtained from the XGBoost model were equal to 0.000346,0.952,7.02,and 0.00028,respectively.In addition,the proposed method analyzed the contribution rates of the rolling affecting parameters on the roll gap.The data showed that in the controllable rolling parameters,the rolling speed is the most impacting factor that disturbs the roll gap model in the acceleration and deceleration process,which can provide a useful direction for actual roll gap adjustment.展开更多
In the traditional rolling force model of tandem cold rolling mills,the calculation of the deformation resistance of the strip head does not consider the actual size and mechanical properties of the incoming material,...In the traditional rolling force model of tandem cold rolling mills,the calculation of the deformation resistance of the strip head does not consider the actual size and mechanical properties of the incoming material,which results in a mismatch between the deformation resistance setting and the actual state of the incoming material and thus affects the accuracy of the rolling force during the low-speed rolling process of the strip head.The inverse calculation of deformation resistance was derived to obtain the actual deformation resistance of the strip head in the tandem cold rolling process,and the actual process parameters of the strip in the hot and cold rolling processes were integrated to create the cross-process dataset as the basis to establish the support vector regression(SVR)model.The grey wolf optimization(GWO)algorithm was used to optimize the hyperparameters in the SVR model,and a deformation resistance prediction model based on GWO–SVR was established.Compared with the traditional model,the GWO–SVR model shows different degrees of improvement in each stand,with significant improvement in stands S3–S5.The prediction results of the GWO–SVR model were applied to calculate the head rolling setting of a 1420 mm tandem rolling mill.The head rolling force had a similar degree of improvement in accuracy to the deformation resistance,and the phenomenon of low head rolling force setting from stands S3 to S5 was obviously improved.Meanwhile,the thickness quality and shape quality of the strip head were improved accordingly,and the application results were consistent with expectations.展开更多
The feasibility of improving the overall performance of medium Mn steels was demonstrated via tailoring the initial microstructure and cold rolling reduction.The combined effects of cooling patterns after hot rolling(...The feasibility of improving the overall performance of medium Mn steels was demonstrated via tailoring the initial microstructure and cold rolling reduction.The combined effects of cooling patterns after hot rolling(HR) and cold rolling(CR) reductions show:(1) as the cooling pattern varied from furnace cooling(FC) to oil quenching(OQ),the intercritically annealed microstructure was dramatically refined and the fraction of recrystallized ferrite dropped,regardless of CR reductions.This resulted in both high yield/ultimate tensile strengths(YS/UTS) but low total elongation to fracture(El);(2) as the CR reduction increased from 50% to 75%,the OQ-samples after annealing exhibited a more refined microstructure with relatively higher fractions of retained austenite and sub-structure,leading to higher YS and UTS but lower El; whereas the FC samples appeared to exhibit little difference in overall tensile properties in both cases.The differences in microstructural evolution with cooling patterns and CR reductions were explained by the calculated accumulated effective strain(εAES),which was considered to be related to degrees of recovery and recrystallization of the deformed martensite(α').The optimal tensile properties of ~1 GPa YS and ~40 GPa·% UTS×El were achieved in the OQ-50%CR annealed samples at 650?C for 1 h.This was quite beneficial to large-scale production of ultra-high strength steels,owing to its serious springback during heavy cold working.展开更多
The oxidation behavior and mechanism of as-received and 30 % cold-rolled alumina-forming austenitic(AFA) steel were investigated in dry air at 700℃.The results show that the mass gain per unit area curves of as-recei...The oxidation behavior and mechanism of as-received and 30 % cold-rolled alumina-forming austenitic(AFA) steel were investigated in dry air at 700℃.The results show that the mass gain per unit area curves of as-received and 30 % cold-rolled steels subject to near-parabolic law before 100 h oxidation time.Two samples both show higher high-temperature oxidation resistance due to the formation of dense Al_(2)O_(3) oxide scale.Gradual spallation of outer scale results in the formation of continuous and dense alumina scale.Dislocations can act as short-circuit diffusion channel for the diffusion of Al from alloy matrix to surface,and also provide nucleation sites for B2-NiAl phase,which ensure the continuous formation of Al_(2)O_(3) scale.展开更多
This study demonstrates that the initial texture of Mg alloy significantly affects the microstructure developed during cold rolling and the recrystallization behavior during subsequent annealing. In a sample with a te...This study demonstrates that the initial texture of Mg alloy significantly affects the microstructure developed during cold rolling and the recrystallization behavior during subsequent annealing. In a sample with a texture oriented toward the normal direction(ND sample), thick and large-sized shear bands are intensively formed during cold rolling and the deformation is strongly localized along these bands. In contrast,in a sample with a texture oriented toward the transverse direction(TD sample), many {10-12} twins are formed at the early stage of cold rolling, and then, numerous small-sized shear bands are formed in these twins. Results of nanoindentation tests reveal that the cold-rolled ND sample has internal strain energy that is substantially concentrated along the shear bands, whereas the cold-rolled TD sample has a large amount of internal strain energy that is homogeneously distributed throughout the material;this latter behavior is strongly related to the extensive {10-12} twinning and the resultant microstructural variations in the TD sample. During subsequent annealing, recrystallization occurs locally along the shear bands in the ND sample, which leads to the formation of a bimodal grain structure comprising fine recrystallized grains and coarse unrecrystallized grains. In contrast, during subsequent annealing of the TD sample, static recrystallization occurs homogeneously throughout the material, which results in the formation of a uniform grain structure that mostly comprises equiaxed recrystallized grains.展开更多
In cold rolling process,the flatness actuator efficiency is the basis of the flatness control system.The precision of flatness is determined by the setpoints of flatness actuators.In the presence of modeling uncertain...In cold rolling process,the flatness actuator efficiency is the basis of the flatness control system.The precision of flatness is determined by the setpoints of flatness actuators.In the presence of modeling uncertainties and unmodeled nonlinearities in rolling process,it is difficult to obtain efficiency factors and setpoints of flatness actuators accurately.Based on the production data,a method to obtain the flatness actuator efficiency by using partial least square(PLS)combined with orthogonal signal correction(OSC)was adopted.Compared with the experiential method and principal component analysis method,the OSC-PLS method shows superior performance in obtaining the flatness actuator efficiency factors at the last stand.Furthermore,kernel partial least square combined with artificial neural network(KPLS-ANN)was proposed to predict the flatness values and optimize the setpoints of flatness actuators.Compared with KPLS or ANN,KPLS-ANN shows the best predictive ability.The root mean square error,mean absolute error and mean absolute percentage error are 0.51 IU,0.34 IU and 0.09,respectively.After the setpoints of flatness actuators are optimized,KPLS-ANN shows better optimization ability.The result in an average flatness standard deviation is 2.22 IU,while the unoptimized value is 4.10 IU.展开更多
The influence of cold rolling reduction on microstructure and mechanical properties of the twinning induced plasticity(TWIP) steel with a chemical composition of Fe-20Mn-3Si-3Al-0.045 C has been investigated.Tensile t...The influence of cold rolling reduction on microstructure and mechanical properties of the twinning induced plasticity(TWIP) steel with a chemical composition of Fe-20Mn-3Si-3Al-0.045 C has been investigated.Tensile tests were carried out to explore the mechanical properties of TWIP steel with different cold rolling reductions.The microstructures were observed by optical microscopy and transmission electron microscopy(TEM).The misorientation and the development of recrystallization texture in TWIP steel sheets were investigated by Electron Back Scatter Diffraction(EBSD) technique.The results indicated that the steel exhibited attractively mechanical properties when cold rolling reduction was about 10%.The tensile strength of the steel with a rolling reduction of 10%is higher than 900 MPa and the yield strength is about 800 MPa,while the elongation is above 35%.The microstructure is composed of austenitic matrix and deformation twins at room temperature,at the same time,a significant amount of deformation twins,stacking faults and dislocations are observed by TEM.TEM observations showed the presence of deformation twinning in the sample at low rolling reduction.As the strain increases the volume fraction of twins increases.Mechanical twins play a dominant role during deformation and result in excellent mechanical properties for the investigated steel.By TEM observation,the possible deformation mechanisms can be suggested as:with the increasing strain,formation of the twin will gradually play a more important role during deformation.The interaction between twins and dislocations enhances the strain hardening rate in the sample.Consequently,the necking is delayed and a good ductility is obtained.Twins were always observed in the region with high density of dislocation and faults,suggesting that the interaction among blocked dislocations and faults as well as deformation twins promote the increase in material strength.EBSD observation showed that the textures has evolved according to the following trend:the brass orientation {110}〈112〉and Goss orientation {110}〈001〉are dominant at every strain level,those intensities increase with increasing strain,while with the increase of the strain level,the change of S orientation {123}〈634〉was not obviously.展开更多
The texture evolution behavior and its triggered mechanical anisotropy of commercially pure titanium(CP Ti) during severe cold rolling and subsequent annealing are discussed based on the optical microscopy and the ele...The texture evolution behavior and its triggered mechanical anisotropy of commercially pure titanium(CP Ti) during severe cold rolling and subsequent annealing are discussed based on the optical microscopy and the electron backscattered diffraction analyses. Some enlightening results are found. It is shown that planar textures exist under all treatments, namely the {11–29}<10–10> under rolling state, the {11–27}<10–10> under 300 °C annealing state and the {11–24}<10–10> under 500 °C annealing state. This indicates that the crystal plane indices of planar texture change toward {-12–10} with increasing annealing temperature, which is a result of crystal lattice rotation. Planar texture triggers anisotropy of the mechanical properties for CP Ti sheets under all treatments. In particular, CP Ti sheets exhibit severe and similar anisotropy behavior under rolling and 300 °C annealing states. Generally speaking, the rolling direction(RD) specimens get relatively low yield strength, high ultimate tensile strength and good plasticity, and RD + 45° specimens show relatively high yield strength, low ultimate tensile strength and good plasticity. The transverse direction specimens, however, usually exhibit high yield strength and low plasticity. It is proved that the above anisotropy behavior is mainly determined by the Schmid factor distribution of the(10–10)[11–20] prismatic slip system in different directions. Due to the non-negligible influence exerted by the(0001)[11–20] basal slip system after 500 °C annealing, the anisotropy behavior under this state is obviously different.展开更多
Deformation behaviors during cold rolling and static recrystallization behaviors upon subsequent annealing of an extruded WE43 alloys with different initial textures were investigated in this study.Three types of diff...Deformation behaviors during cold rolling and static recrystallization behaviors upon subsequent annealing of an extruded WE43 alloys with different initial textures were investigated in this study.Three types of differently textured WE43 initial alloys were labeled as samplesⅠ,ⅡandⅢ.The results showed that multiple twinning modes and basal slip dominated the deformation of samples during cold rolling.Cold-rolled sampleⅠactivated the larger number of double twins with high strain energy,accompanied by the more uniform strain distribution,than cold-rolled samplesⅡandⅢ.During subsequent annealing,recrystallized grains preferentially occurred in double twins,twin-twin intersections and grain boundaries,thereby making cold-rolled sampleⅠhave the more rapid recrystallization rate.Similar recrystallization textures formed in three types of cold-rolled samples at the recrystallization nucleation stage,and they never largely changed with the annealing time due to the uniform grain growth induced by the solute drag and the precipitation pinning at grain boundaries.After full recrystallization,the grain growth was controlled by the solute drag,instead of precipitates which were re-dissolved into the matrix.Finally,the nucleation and growth kinetics of static recrystallization were calculated,and the effects of initial texture on activation energies of recrystallization nucleation and growth were discussed.展开更多
The evolution of microstructure and texture at four strain levels was investigated in Ni-5 at%W alloy by means of electron backscatter diffraction(EBSD)technique.The deformation microstructure evolves gradually from m...The evolution of microstructure and texture at four strain levels was investigated in Ni-5 at%W alloy by means of electron backscatter diffraction(EBSD)technique.The deformation microstructure evolves gradually from microbands(MBs)to typical lamellar structures with strain increasing in cold-rolled materials,while only lamellar structures in heavily cold-rolled materials.Subsequently,quantitative analysis of microstructure and texture was performed.It indicates that the texture is a typical pure metal deformation texture,but a few cube and rolling direction(RD)-rotated cube orientations also can be observed in the deformed samples.The use of high-temperature annealing enables an area fraction of cube orientation>95%to be obtained for high strained substrate.In addition,it is worth noting that the point-to-point misorientation inside the band with various orientations is found to keep quite low.But the point-to-origin misorientation over the same distance is dependent on strain and orientation type in the band.The cube-oriented regions were characterized by a high accumulated orientation gradient,close to 28°,compared to the non-cube-oriented regions.This means that the accumulated orientation gradient only occurs in the cube band with the reduction of 98%,which partly explains the formation of strong cube texture after high-temperature annealing.展开更多
Low - carbon becomes a high - frequency and fashionable word which gets the greatest concern in the world.Low - carbon refers to a minimal output of greenhouse gas emissions into the biosphere, specifically refers to ...Low - carbon becomes a high - frequency and fashionable word which gets the greatest concern in the world.Low - carbon refers to a minimal output of greenhouse gas emissions into the biosphere, specifically refers to the greenhouse gas carbon dioxide.To reduce energy consumption of automobile,more and more high strength steels are used by vehicle companies.To meet the request of vehicle companies, various high strength steels are developed in steel companies all over the world.Ansteel can provide,ultra-low carbon bake hardening(BH) steels,dual phase(DP) steels and transformation - induced plasticity (TRIP) steels with the grades of under 780 MPa,up to now.AHSS steels have much different composition, microstructure and strenght than conventional vehicle steels,so there are some trouble in producing in cold rolling mills,for example,difficult to join,poor thickness and flatness,accurate temperature and velocity control and so on.To reduce the opportunity of strip breakage,we have done many welding experiments and special research.Now,DP and TRIP steels can be continuously produced in Ansteel.To assure thickness and flatness of strips,we optimized the hot rolling parameter to get low deformation resistance,optimized rolling oil to get fit frictional coefficient and fix on the targat rolling curve.To get more accurate and repetitive results over the production shifts,the Mathematical Model(MM) is used in Ansteel.The MM analyses information transmitted by various sensors and transmitters,compares the collected data with the chosen parameters and adjusts the settings of the various pieces of equipment to hone on the parameter setpoints.At present,the key production technologies of AHSS were grasped by cold rolling mill Ansteel,and Ansteel is the first company to apply the TRIP with the grade of 780 MPa.展开更多
基金Supported by National Natural Science Foundation of China(Grant No.51675415)Key Research and Development Program of Shaanxi,China(Grant No.2021GXLH-Z-049).
文摘The hardening on surface of complex profles such as thread and spline manufactured by cold rolling can efectively improve the mechanical properties and surface quality of rolled parts. The distribution of hardness in superfcial layer is closely related to the deformation by rolling. To establish the suitable correlation model for describing the relationship between strain and hardness during cold rolling forming process of complex profles is helpful to the optimization of rolling parameters and improvement of rolling process. In this study, a physical analog experiment refecting the uneven deformation during complex-profle rolling process has been extracted and designed, and then the large date set (more than 400 data points) of training samples refecting the local deformation characteristics of complexprofle rolling have been obtained. Several types of polynomials and power functions were adopted in regression analysis, and the regression correlation models of 45# steel were evaluated by the single-pass and multi-pass physical analog experiments and the complex-profle rolling experiment. The results indicated that the predicting accuracy of polynomial regression model is better in the strain range (i.e., ε < 1.2) of training samples, and the correlation relationship between strain and hardness out strain range (i.e., ε > 1.2) of training samples can be well described by power regression model;so the correlation relationship between strain and hardness during complex-profle rolling process of 45# steel can be characterized by a segmented function such as third-order polynomial in the range ε < 1.2 and power function with a ftting constant in the range ε > 1.2;and the predicting error of the regression model by segmented function is less than 10%.
基金the China National Funds for Distinguished Young Scientists (No.51325401)the National High Technology Research and Development Program of China (No.2015AA042504)the National Natural Science Foundation of China (No.51474156) for grant and financial support
文摘The coarsening behaviors of γ″-phase particles in Inconel 718 alloy aged at 750, 800, and 850℃ were investigated by scanning electron microscopy(SEM). Detailed observations and quantitative measurements were conducted to characterize the coarsening behavior of the γ″-phase under various aging conditions. The experimental results indicate that the existence of the δ-phase retards the formation and coarsening of the γ″-phase, without influencing its final particle size or amount. Moreover, when cold rolled with a reduction of 50%, the dimensions of the γ″ particles in Inconel 718 alloy decrease with increasing aging time. Furthermore, the coarsening behavior of the γ″-phase in the Inconel 718 alloy after a normal aging treatment(sample A) and that of the primary δ-phase(sample B) follow the Lifshitz–Slyozov–Wagner(LSW) diffusion-controlled growth theory; the thus-obtained activation energies for the γ″-phase are 292 k J·mol^(-1)and 302 k J·mol^(-1), respectively.
基金Project(50675133)supported by the National Natural Science Foundation of ChinaProject(2006CB705401)supported by the National Basic Research Program of China
文摘A new processing method,equal channel angular pressing(ECAP)plus cold rolling(CR),was applied to producing ultra-fine grained FeCoV alloy.The microstructures of ultra-fine grained FeCoV alloy after ECAP,ECAP plus CR,and the effect of tempering treatment on the microstructure of FeCoV alloy produced by ECAP plus CR were investigated.The results show that an elongated substructure with a width of about 0.3μm is obtained after four-pass ECAP using Route A.Cold rolling after ECAP cannot change the morphologies of elongated substructure,and it results in higher fraction of high-angle boundaries and higher dislocation density compared with the identical ECAP without rolling.Subsequent tempering for 30 min at 853 K brings about many nano-phases precipitating at subgrain boundaries and insides the grains,and the size of precipitated phase is measured to be about 10 nm.Nano-phases grow up with increasing tempering temperature and equiaxed structure forms at 883 K.
文摘In order to know the cause of cracks in cold rolling of QSn6.5 0.1 copper alloy strip, a lot of experiments and analysis were done. The microstructure changes of QSn6.5 0.1 were investigated by means of metallurgical microscope. The morphology of cracks and surface defects were examined using scanning electron microscope. Macroscopic residual stresses produced in every process during manufacturing in the QSn6.5 0.1 strip were measured by X ray diffraction method and hole drilling method. The results show that the cracks in the QSn6.5 0.1 cold rolling strip were caused due to the derivation of metallurgical defects, such as SnO 2, S, fine looses,the inverse segregation unable to clear up when milling, and the accumulation of all kinds of resi dual stresses. When the accumulation of the residual stress reaches the material′s breaking strength, the cracks will be generated. Several measures to avoid the development of these kinds of cracks were put forward, such as: controlling the casting technology, improving homogenization annealing procedure (680 ℃/7 h) and milling quality(using the second milling when necessary), working out a more reasonable rolling technology to ensure intermediate annealing in time.
文摘On the condition of the width to thickness ratio 625 of rolled strip, the asymmetrical cold strip rolling process about the width center is studied by using computer numerical simulation method and experimental method. The simulated results of the transverse distributions of the rolling pressure. the 2-directional frictions and the front and back.tensions agree with the experimental reuslts well. It is an important discovery that the rolling pressure has three peak values across the strip width on the condition of large width to thickness ratio.
文摘Lubrication in cold rolling process is used not only to control friction,but also to control surface quality and thermal chamber.Successful cold rolling of strip at high speeds requires an optimum presence of lubricant film thickness at the contact.In order to have a better control on rolling process the awareness for the prediction and maintenance of desired minimum film thickness.On the basis of learning and summarizing the theories early founded by experts around the world,this paper constructed the mixed lubrication model. This paper investigated the lubrication state variation caused by oil and rolling condition differences by cold rolling experiments.The experiments indicated that oil has a big influence to rolling process,and rolling speed directly influence the lubrication state.
文摘This paper describes the formation mechanism and mode of the emulsion odor of the cold rolling process,and introduces the relevant environmental regulations and methods used to measure the emulsion odor.Studies were conducted with respect to these issues.The technical measures used to minimize the emulsion odor,particularly the adjustment of the chemical formula of the cold rolling emulsion,are illustrated in detail.The study results have been successfully applied in cold rolling production,and a significant reduction in the emulsion odor is achieved.
文摘Accurate calculation results of roll temperature are the key factors in rolling cooling and lubricating technology during the single-stand reversing cold rolling process. By combining the high-strength steel rolling experiments,the numerical simulation of roll temperature,and the influence factors in reversing cold rolling were studied. The research results correspond with those of rolling experiments and show that the research method could provide effective instruction for roll cooling and emulsion flow rate control during the on-site rolling process.
基金This study was supported by the National Key Research and Development Program of China(No.2017YFB0304100)Key Projects of the National Natural Science Foundation of China(No.51634002).
文摘Aiming at the problem of insufficient prediction accuracy of strip flatness at the outlet of cold tandem rolling,the prediction performance of strip flatness based on different ensemble methods was studied and a high-precision prediction ensemble model of strip flatness at the outlet was established.Firstly,based on linear regression(LR),K nearest neighbors(KNN),support vector regression,regression trees(RT),and backpropagation neural network(BPN),bagging,boosting,and stacking ensemble methods were used for ensemble experiments.Secondly,three existing ensemble models,i.e.,random forest,extreme random tree(ET)and extreme gradient boosting,were used to conduct experiments and compare the results.The research shows that bagging,boosting,and stacking three ensemble methods have the most significant improvement in the prediction accuracy of the regression trees model,which is increased by 5.28%,6.51%,and 5.32%,respectively.At the same time,the stacking ensemble method improves both the simple model and the complex model,and the improvement effect on the simple base model is the greatest,which is 4.69%higher than that of the base model KNN.Comparing all of the ensemble models,the stacking ensemble model of level-1(ET,AdaBoost-RT,LR,BPN)paired with level-2(LR)was discovered to be the best model(EALB-LR)and can be further studied for industrial applications.
基金supported by the National Natural Science Foundation of China(Grant Nos.U21A20117 and 52074085)the Liao Ning Revitalization Talents Program(XLYC1907065)+1 种基金Liao Ning Province Doctoral Initiation Fund(2022-BS-188)Open Research Fund from State Key Laboratory of Rolling and Automation(No.2021RALKFKT006).
文摘Severe fluctuation of the effective roll gap in the acceleration and deceleration section of the cold rolling process is a significant factor causing thickness deviation.However,the conventional roll gap compensation method and control strategy do not meet the stringent strip quality requirements.The roll gap model in the acceleration and deceleration process is studied to increase the thickness control precision.In order to improve model accuracy,a roll gap prediction method based on data-driven is proposed.Given the complexities of the cold rolling process,the extreme gradient boosting(XGBoost)method is used to predict the roll gap model as the rolling speed changes.Meanwhile,support vector regression and neural network-based methods are taken to evaluate and compare the prediction performances.Based on the field data,the simulation experiments are carried out.It demonstrated that the prediction performance of the proposed method outperformed the other two methods.The values of root mean square error,determination coefficient value,mean absolute percentage error and mean absolute error obtained from the XGBoost model were equal to 0.000346,0.952,7.02,and 0.00028,respectively.In addition,the proposed method analyzed the contribution rates of the rolling affecting parameters on the roll gap.The data showed that in the controllable rolling parameters,the rolling speed is the most impacting factor that disturbs the roll gap model in the acceleration and deceleration process,which can provide a useful direction for actual roll gap adjustment.
基金This work was supported by the National Key Research and Development Plan of China(Grant No.2020YFB1713600)the National Natural Science Foundation of China(Grant No.51975043)+1 种基金China Postdoctoral Science Foundation(Grant No.2021M69035)Fundamental Research Funds for the Central Universities(Grant Nos.FRF-TP-19-002A3 and FRF-TP-20-105A1).
文摘In the traditional rolling force model of tandem cold rolling mills,the calculation of the deformation resistance of the strip head does not consider the actual size and mechanical properties of the incoming material,which results in a mismatch between the deformation resistance setting and the actual state of the incoming material and thus affects the accuracy of the rolling force during the low-speed rolling process of the strip head.The inverse calculation of deformation resistance was derived to obtain the actual deformation resistance of the strip head in the tandem cold rolling process,and the actual process parameters of the strip in the hot and cold rolling processes were integrated to create the cross-process dataset as the basis to establish the support vector regression(SVR)model.The grey wolf optimization(GWO)algorithm was used to optimize the hyperparameters in the SVR model,and a deformation resistance prediction model based on GWO–SVR was established.Compared with the traditional model,the GWO–SVR model shows different degrees of improvement in each stand,with significant improvement in stands S3–S5.The prediction results of the GWO–SVR model were applied to calculate the head rolling setting of a 1420 mm tandem rolling mill.The head rolling force had a similar degree of improvement in accuracy to the deformation resistance,and the phenomenon of low head rolling force setting from stands S3 to S5 was obviously improved.Meanwhile,the thickness quality and shape quality of the strip head were improved accordingly,and the application results were consistent with expectations.
基金financially supported by the National Natural Science Foundation of China (Grant.No.51401050)the Fundamental Research Funding for the Central Universities (Grant.No.N160204001),China (A/Prof.Cai)supported by grants through the Australian Research Council (ARC) Laureate Fellowship (Prof.Hodgson)
文摘The feasibility of improving the overall performance of medium Mn steels was demonstrated via tailoring the initial microstructure and cold rolling reduction.The combined effects of cooling patterns after hot rolling(HR) and cold rolling(CR) reductions show:(1) as the cooling pattern varied from furnace cooling(FC) to oil quenching(OQ),the intercritically annealed microstructure was dramatically refined and the fraction of recrystallized ferrite dropped,regardless of CR reductions.This resulted in both high yield/ultimate tensile strengths(YS/UTS) but low total elongation to fracture(El);(2) as the CR reduction increased from 50% to 75%,the OQ-samples after annealing exhibited a more refined microstructure with relatively higher fractions of retained austenite and sub-structure,leading to higher YS and UTS but lower El; whereas the FC samples appeared to exhibit little difference in overall tensile properties in both cases.The differences in microstructural evolution with cooling patterns and CR reductions were explained by the calculated accumulated effective strain(εAES),which was considered to be related to degrees of recovery and recrystallization of the deformed martensite(α').The optimal tensile properties of ~1 GPa YS and ~40 GPa·% UTS×El were achieved in the OQ-50%CR annealed samples at 650?C for 1 h.This was quite beneficial to large-scale production of ultra-high strength steels,owing to its serious springback during heavy cold working.
基金financially supported by the National Natural Science Foundation of China and Shanghai Baosteel Group Company(No. U1960204)the National Natural Science Foundation of China(Nos. 51871042 and 51501034)the Fundamental Research Funds for the Central Universities (No. N2023026)。
文摘The oxidation behavior and mechanism of as-received and 30 % cold-rolled alumina-forming austenitic(AFA) steel were investigated in dry air at 700℃.The results show that the mass gain per unit area curves of as-received and 30 % cold-rolled steels subject to near-parabolic law before 100 h oxidation time.Two samples both show higher high-temperature oxidation resistance due to the formation of dense Al_(2)O_(3) oxide scale.Gradual spallation of outer scale results in the formation of continuous and dense alumina scale.Dislocations can act as short-circuit diffusion channel for the diffusion of Al from alloy matrix to surface,and also provide nucleation sites for B2-NiAl phase,which ensure the continuous formation of Al_(2)O_(3) scale.
基金supported by the National Research Foundation of Korea (NRF) grant funded by the Korean government(MSIP,South Korea,No.2019R1A2C1085272)。
文摘This study demonstrates that the initial texture of Mg alloy significantly affects the microstructure developed during cold rolling and the recrystallization behavior during subsequent annealing. In a sample with a texture oriented toward the normal direction(ND sample), thick and large-sized shear bands are intensively formed during cold rolling and the deformation is strongly localized along these bands. In contrast,in a sample with a texture oriented toward the transverse direction(TD sample), many {10-12} twins are formed at the early stage of cold rolling, and then, numerous small-sized shear bands are formed in these twins. Results of nanoindentation tests reveal that the cold-rolled ND sample has internal strain energy that is substantially concentrated along the shear bands, whereas the cold-rolled TD sample has a large amount of internal strain energy that is homogeneously distributed throughout the material;this latter behavior is strongly related to the extensive {10-12} twinning and the resultant microstructural variations in the TD sample. During subsequent annealing, recrystallization occurs locally along the shear bands in the ND sample, which leads to the formation of a bimodal grain structure comprising fine recrystallized grains and coarse unrecrystallized grains. In contrast, during subsequent annealing of the TD sample, static recrystallization occurs homogeneously throughout the material, which results in the formation of a uniform grain structure that mostly comprises equiaxed recrystallized grains.
基金This study is financially supported by the National Key Research and Development Program of China(No.2017YFB0304100)the National Natural Science Foundation of China(Nos.51774084,51704067,and 51634002)+1 种基金the Fundamental Research Funds for the Central Universities(Nos.N160704004,N170708020,and N2004010)Liaoning Revitalization Talents Program(XLYC1907065).
文摘In cold rolling process,the flatness actuator efficiency is the basis of the flatness control system.The precision of flatness is determined by the setpoints of flatness actuators.In the presence of modeling uncertainties and unmodeled nonlinearities in rolling process,it is difficult to obtain efficiency factors and setpoints of flatness actuators accurately.Based on the production data,a method to obtain the flatness actuator efficiency by using partial least square(PLS)combined with orthogonal signal correction(OSC)was adopted.Compared with the experiential method and principal component analysis method,the OSC-PLS method shows superior performance in obtaining the flatness actuator efficiency factors at the last stand.Furthermore,kernel partial least square combined with artificial neural network(KPLS-ANN)was proposed to predict the flatness values and optimize the setpoints of flatness actuators.Compared with KPLS or ANN,KPLS-ANN shows the best predictive ability.The root mean square error,mean absolute error and mean absolute percentage error are 0.51 IU,0.34 IU and 0.09,respectively.After the setpoints of flatness actuators are optimized,KPLS-ANN shows better optimization ability.The result in an average flatness standard deviation is 2.22 IU,while the unoptimized value is 4.10 IU.
文摘The influence of cold rolling reduction on microstructure and mechanical properties of the twinning induced plasticity(TWIP) steel with a chemical composition of Fe-20Mn-3Si-3Al-0.045 C has been investigated.Tensile tests were carried out to explore the mechanical properties of TWIP steel with different cold rolling reductions.The microstructures were observed by optical microscopy and transmission electron microscopy(TEM).The misorientation and the development of recrystallization texture in TWIP steel sheets were investigated by Electron Back Scatter Diffraction(EBSD) technique.The results indicated that the steel exhibited attractively mechanical properties when cold rolling reduction was about 10%.The tensile strength of the steel with a rolling reduction of 10%is higher than 900 MPa and the yield strength is about 800 MPa,while the elongation is above 35%.The microstructure is composed of austenitic matrix and deformation twins at room temperature,at the same time,a significant amount of deformation twins,stacking faults and dislocations are observed by TEM.TEM observations showed the presence of deformation twinning in the sample at low rolling reduction.As the strain increases the volume fraction of twins increases.Mechanical twins play a dominant role during deformation and result in excellent mechanical properties for the investigated steel.By TEM observation,the possible deformation mechanisms can be suggested as:with the increasing strain,formation of the twin will gradually play a more important role during deformation.The interaction between twins and dislocations enhances the strain hardening rate in the sample.Consequently,the necking is delayed and a good ductility is obtained.Twins were always observed in the region with high density of dislocation and faults,suggesting that the interaction among blocked dislocations and faults as well as deformation twins promote the increase in material strength.EBSD observation showed that the textures has evolved according to the following trend:the brass orientation {110}〈112〉and Goss orientation {110}〈001〉are dominant at every strain level,those intensities increase with increasing strain,while with the increase of the strain level,the change of S orientation {123}〈634〉was not obviously.
基金the National Natural Science Foundation of China(Grant No.51801132)the China Scholarship Council(CSC NO.201906935013)for X.H.Shi+1 种基金the School Foundation of Taiyuan University of Technology(Grant No.2017QN02)the National Key Laboratory for Remanufacturing,Academy of Armored Forces Engineering(No.61420050204)。
文摘The texture evolution behavior and its triggered mechanical anisotropy of commercially pure titanium(CP Ti) during severe cold rolling and subsequent annealing are discussed based on the optical microscopy and the electron backscattered diffraction analyses. Some enlightening results are found. It is shown that planar textures exist under all treatments, namely the {11–29}<10–10> under rolling state, the {11–27}<10–10> under 300 °C annealing state and the {11–24}<10–10> under 500 °C annealing state. This indicates that the crystal plane indices of planar texture change toward {-12–10} with increasing annealing temperature, which is a result of crystal lattice rotation. Planar texture triggers anisotropy of the mechanical properties for CP Ti sheets under all treatments. In particular, CP Ti sheets exhibit severe and similar anisotropy behavior under rolling and 300 °C annealing states. Generally speaking, the rolling direction(RD) specimens get relatively low yield strength, high ultimate tensile strength and good plasticity, and RD + 45° specimens show relatively high yield strength, low ultimate tensile strength and good plasticity. The transverse direction specimens, however, usually exhibit high yield strength and low plasticity. It is proved that the above anisotropy behavior is mainly determined by the Schmid factor distribution of the(10–10)[11–20] prismatic slip system in different directions. Due to the non-negligible influence exerted by the(0001)[11–20] basal slip system after 500 °C annealing, the anisotropy behavior under this state is obviously different.
基金financially supported by the National Key Research and Development Program of China(No.U1764253)the National Natural Science Foundation of China(No.52105405)the Opening Project of State Key Laboratory of Advanced Welding and Joining in Harbin Institute of Technology(No.AWJ-22M04)。
文摘Deformation behaviors during cold rolling and static recrystallization behaviors upon subsequent annealing of an extruded WE43 alloys with different initial textures were investigated in this study.Three types of differently textured WE43 initial alloys were labeled as samplesⅠ,ⅡandⅢ.The results showed that multiple twinning modes and basal slip dominated the deformation of samples during cold rolling.Cold-rolled sampleⅠactivated the larger number of double twins with high strain energy,accompanied by the more uniform strain distribution,than cold-rolled samplesⅡandⅢ.During subsequent annealing,recrystallized grains preferentially occurred in double twins,twin-twin intersections and grain boundaries,thereby making cold-rolled sampleⅠhave the more rapid recrystallization rate.Similar recrystallization textures formed in three types of cold-rolled samples at the recrystallization nucleation stage,and they never largely changed with the annealing time due to the uniform grain growth induced by the solute drag and the precipitation pinning at grain boundaries.After full recrystallization,the grain growth was controlled by the solute drag,instead of precipitates which were re-dissolved into the matrix.Finally,the nucleation and growth kinetics of static recrystallization were calculated,and the effects of initial texture on activation energies of recrystallization nucleation and growth were discussed.
基金financially supported by the National Natural Science Foundation of China(No.51171215)。
文摘The evolution of microstructure and texture at four strain levels was investigated in Ni-5 at%W alloy by means of electron backscatter diffraction(EBSD)technique.The deformation microstructure evolves gradually from microbands(MBs)to typical lamellar structures with strain increasing in cold-rolled materials,while only lamellar structures in heavily cold-rolled materials.Subsequently,quantitative analysis of microstructure and texture was performed.It indicates that the texture is a typical pure metal deformation texture,but a few cube and rolling direction(RD)-rotated cube orientations also can be observed in the deformed samples.The use of high-temperature annealing enables an area fraction of cube orientation>95%to be obtained for high strained substrate.In addition,it is worth noting that the point-to-point misorientation inside the band with various orientations is found to keep quite low.But the point-to-origin misorientation over the same distance is dependent on strain and orientation type in the band.The cube-oriented regions were characterized by a high accumulated orientation gradient,close to 28°,compared to the non-cube-oriented regions.This means that the accumulated orientation gradient only occurs in the cube band with the reduction of 98%,which partly explains the formation of strong cube texture after high-temperature annealing.
文摘Low - carbon becomes a high - frequency and fashionable word which gets the greatest concern in the world.Low - carbon refers to a minimal output of greenhouse gas emissions into the biosphere, specifically refers to the greenhouse gas carbon dioxide.To reduce energy consumption of automobile,more and more high strength steels are used by vehicle companies.To meet the request of vehicle companies, various high strength steels are developed in steel companies all over the world.Ansteel can provide,ultra-low carbon bake hardening(BH) steels,dual phase(DP) steels and transformation - induced plasticity (TRIP) steels with the grades of under 780 MPa,up to now.AHSS steels have much different composition, microstructure and strenght than conventional vehicle steels,so there are some trouble in producing in cold rolling mills,for example,difficult to join,poor thickness and flatness,accurate temperature and velocity control and so on.To reduce the opportunity of strip breakage,we have done many welding experiments and special research.Now,DP and TRIP steels can be continuously produced in Ansteel.To assure thickness and flatness of strips,we optimized the hot rolling parameter to get low deformation resistance,optimized rolling oil to get fit frictional coefficient and fix on the targat rolling curve.To get more accurate and repetitive results over the production shifts,the Mathematical Model(MM) is used in Ansteel.The MM analyses information transmitted by various sensors and transmitters,compares the collected data with the chosen parameters and adjusts the settings of the various pieces of equipment to hone on the parameter setpoints.At present,the key production technologies of AHSS were grasped by cold rolling mill Ansteel,and Ansteel is the first company to apply the TRIP with the grade of 780 MPa.
