The effects of different hot deformation amounts on the evolution of inclusion and microstructure in Ti-Zr deoxidized steel were studied by utilizing the Thermecmaster-Z hot simulation test machine,automatic scanning ...The effects of different hot deformation amounts on the evolution of inclusion and microstructure in Ti-Zr deoxidized steel were studied by utilizing the Thermecmaster-Z hot simulation test machine,automatic scanning electron microscope equipped with energy-dispersive spectrometer,and electron backscattered diffraction.The results indicated that hot deformation amount has no significant effect on the number density of oxide,but the MnS that precipitated on the Ti-Zr oxide surface undergoes extension and breakage,resulting in the changes in oxide aspect ratio.Moreover,the fracture of nitride mainly occurs in the sample with the second pass deformation amount of 42.9%and 71.4%,and the degree of fragmentation of nitride is more serious with the deformation amount increasing.During the hot compression,sulfide undergoes breakage and extension,and with the second pass deformation amount increasing,the breakage and extension of sulfide present a periodic change.Finally,with the increase in hot compression amount,the ferrite types in microstructure change from acicular ferrite and bainitic ferrite to polygonal ferrite,and the ferrite grain size is refined.When the total deformation amount increases from 30%to 80%,the ferrite grain sizes of grain boundary with the misorientation of 4°and 15°decrease from 4.14 and 5.67μm to 3.47 and 4.40μm,respectively.However,when the total deformation amount increases to 80%,the harmful ferrite/pearlite banded structure appears in the micro structure.Refining ferrite grain size and avoiding harmful microstructure are the key for the optimization of hot compression process.展开更多
The optimization of hot compression technique of as-cast 0Cr23Ni13 stainless steel at high strain rate was discussed,and its corrosion resistance was evaluated after hot compression treatment experimentally.By adjusti...The optimization of hot compression technique of as-cast 0Cr23Ni13 stainless steel at high strain rate was discussed,and its corrosion resistance was evaluated after hot compression treatment experimentally.By adjusting the dynamic recrys-tallization(DRX)ratio of 0Cr23Nil3 stainless steel during hot pressing,the content of low Σ coincident site lattice(ΣCSL)grain boundaries is increased,and the grain orientation is optimized.The results show that ferrite and austenite are completely recrystallized at 1050 and 1150℃,respectively.The number of grains in the<111>and<101>directions increases significantly,the corrosion potential increases,and the corrosion current density decreases,which will signifi-cantly improve the corrosion resistance of 0Cr23Nil3 stainless steel.After the optimization of grain boundary distribution,corrosion resistance is noticeably improved due to the existence of lowΣCSL boundaries.The interference effect of lowΣCSL grain boundary on random grain boundary network becomes intense with the increase in DRX ratio,which is the fundamental measure to improve the corrosion resistance.展开更多
In this study, microstructure and texture evolution of TB8 titanium alloys during hot deformation were investigated by using electron back-scattered diffraction(EBSD) analysis. The results showed that dynamic recrysta...In this study, microstructure and texture evolution of TB8 titanium alloys during hot deformation were investigated by using electron back-scattered diffraction(EBSD) analysis. The results showed that dynamic recrystallization(DRX) behavior of TB8 titanium alloys was drastically sensitive to the strain. As the true strain raised from 0.2 to 0.8, the degree of DRX gradually increased. The nucleation mechanism of recrystallization was observed, including discontinuous dynamic recrystallization(DDRX) resulting from the bulging of original boundaries. Furthermore, continuous dynamic recrystallization(CDRX) occurred because of the transformation of low-angle grain boundaries(LAGBs) to high-angle grain boundaries(HAGBs) in the interior of the original deformed grains. The texture evolution of TB8 titanium alloy during hot deformation process was analyzed in detail, and five texture components were observed,including{001}h100 i,{011}h100 i,{112}h110 i,{111}h110 i, and {111}h112 i. As the true strain increased,deformation textures were gradually weakened due to an increase in the volume fraction of DRX grains. When the true strain was 0.8, the main texture components consisted of the recrystallization texture components of the{001}h100 i and {011}h100 i textures.展开更多
By means of isothermal compression at temperatures in the range of 650-900℃and strain rates in the range of 0.001-1 s^(-1),the dynamic recrystallization behavior and microstructural evolution of a Cu-3.28 Ni-0.6 Si-0...By means of isothermal compression at temperatures in the range of 650-900℃and strain rates in the range of 0.001-1 s^(-1),the dynamic recrystallization behavior and microstructural evolution of a Cu-3.28 Ni-0.6 Si-0.22 Zn-0.11 Cr-0.04 P(wt%)alloy designed by a machine learning method were investigated.A semiempirical constitutive equation,processing maps and an average activation energy were generated.The microstructure under different conditions and the effect of strain rate on the texture of the alloy at 800-900℃were observed.The results show that the suitable temperature is800-900℃;when the strain is less than 0.4,the appropriate strain rate is 0.01-0.5 s^(-1);and when the strain is greater than 0.4,the appropriate strain rate is below0.05 s^(-1).After deformation at 800℃,the main texture changed from{112}<111>of copper to a uniform distribution with the increase in strain rate,but the sample did not have obvious texture after deformation at 850 and900℃.The above results can provide a reference for the selection of process parameters.展开更多
This paper models hot compression testing using a dilatometer in loading mode.These small-scale tests provide a high throughput at low cost,but are susceptible to inhomogeneity due to friction and temperature gradient...This paper models hot compression testing using a dilatometer in loading mode.These small-scale tests provide a high throughput at low cost,but are susceptible to inhomogeneity due to friction and temperature gradients.A novel method is presented for correcting the true stress-strain constitutive response over the full range of temperatures,strain-rates and strain.The nominal response from the tests is used to predict the offset in the stress-strain curves due to inhomogeneity,and this stress offsetΔσis applied piecewise to the data,correcting the constitutive response in one iteration.A key new feature is the smoothing and fitting of the flow stress data as a function of temperature and strain-rate,at multiple discrete strains.The corrected model then provides quantitative prediction of the spatial and temporal variation in strain-rate and strain throughout the sample,needed to correlate the local deformation conditions with the microstructure and texture evolution.The study uses a detailed series of 144 hot compression tests of a Zr-Nb alloy.While this is an important wrought nuclear alloy in its own right,it also serves here as a test case for modelling the dilatometer for hot testing of high temperature alloys,particularly those with dualα-βphase microstructures(such as titanium alloys).展开更多
The evolution of microstructure during hot deformation is key to achieving good mechanical properties in aluminum alloys.We have developed a cellular automaton(CA) based model to simulate the microstructural evolution...The evolution of microstructure during hot deformation is key to achieving good mechanical properties in aluminum alloys.We have developed a cellular automaton(CA) based model to simulate the microstructural evolution in 7075 aluminum alloy during hot deformation.Isothermal compression tests were conducted to obtain material parameters for 7075 aluminum alloy,leading to the establishment of models for dislocation density,nucleation of recrystallized grains,and grain growth.Integrating these aspects with grain topological deformation,our CA model effectively predicts flow stress,dynamic recrystallization(DRX) volume fraction,and average grain size under diverse deformation conditions.A systematic comparison was made between electron back scattered diffraction(EBSD) maps and CA model simulated under different deformation temperatures(573 to 723 K),strain rates(0.001 to 1 s^(-1)),and strain amounts(30% to 70%).These analyses indicate that large strain,high temperature,and low strain rate facilitate dynamic recrystallization and grain refinement.The results from the CA model show good accuracy and predictive capability,with experimental error within 10%.展开更多
The microstructure evolution of Mg-5.65 Zn-0.66 Zr(wt.%)alloy was studied based on the hot compression tests.The results indicated that the flow stress increased rapidly to a peak point at the initial stage,and then i...The microstructure evolution of Mg-5.65 Zn-0.66 Zr(wt.%)alloy was studied based on the hot compression tests.The results indicated that the flow stress increased rapidly to a peak point at the initial stage,and then it gradually decreased.Moreover,high temperature and low strain rate resulted in the decreasing of flow stress.All samples exhibited a necklace grain structure because of the occurrence of partial dynamic recrystallization(DRX).High temperature increased both the size and fraction of DRXed grains,while high strain rate showed an opposite tendency.At the conditions of 350°C/0.001 s^(-1)and 350°C/0.1 s^(-1),the twins were not exhibited and DRX played a dominant role.Importantly,the obvious split of basal texture was observed.The pyramidal<c+a>slip with high value of Schmid factor was active in large deformed grains,which corresponded to the peak split point in(0001)pole figure.A mechanism about the grain rotation was proposed to explain the relationship between the pyramidal slip and the split of basal texture.Finally,it was found that large number of{10–12}extension twins were formed during the initial stage at condition of 300°C/1 s^(-1),and the number of twins decreased with the increase of strain.The twins greatly contributed to the fast formation of basal texture and grain rotation.Moreover,the non-basal slips were active in twining region,which could facilitate the nucleation of DRX.展开更多
Hot compression tests were performed on AISI 321 austenitic stainless steel in the deformation temperature range of 800–1200℃ and constant strain rates of 0.001,0.01,0.1,and 1 s^(−1).Hot flow curves were used to det...Hot compression tests were performed on AISI 321 austenitic stainless steel in the deformation temperature range of 800–1200℃ and constant strain rates of 0.001,0.01,0.1,and 1 s^(−1).Hot flow curves were used to determine the strain hardening exponent and the strain rate sensitivity exponent,and to construct the processing maps.Variations of the strain hardening exponent with strain were used to predict the microstructural evolutions during the hot deformation.Four variations were distinguished reflecting the different microstructural changes.Based on the analysis of the strain hardening exponent versus strain curves,the microstructural evolutions were dynamic recovery,single and multiple peak dynamic recrystallization,and interactions between dynamic recrystallization and precipitation.The strain rate sensitivity variations at an applied strain of 0.8 and strain rate of 0.1 s^(−1) were compared with the microstructural evolutions.The results demonstrate the existence of a reliable correlation between the strain rate sensitivity values and evolved microstructures.Additionally,the power dissipation map at the applied strain of 0.8 was compared with the resultant microstructures at predetermined deformation conditions.The microstructural evolutions strongly correlated to the power dissipation ratio,and dynamic recrystallization occurred completely at lower power dissipation ratios.展开更多
Hot compression tests on AZ40 magnesium alloy were conducted on a Gleeble 1500 d hot simulation testing machine in a deformation temperature range of 330 ℃-420 ℃ and a strain rate range of 0.002-2 s^(-1). Hot deform...Hot compression tests on AZ40 magnesium alloy were conducted on a Gleeble 1500 d hot simulation testing machine in a deformation temperature range of 330 ℃-420 ℃ and a strain rate range of 0.002-2 s^(-1). Hot deformation behaviors were investigated on the basis of the analysis of the flow stressstrain curves, constitutive equation, and processing map. The stress exponent and apparent activation energy were calculated to be 5.821 and 173.96 k J/mol, respectively. Deformation twins and cracks located in grain boundaries were generated at 330 ℃ and 0.02 s^(-1), which are associated with a high strain rate and a limited number of available slip systems. With increasing temperature and decreasing strain rate, the twins disappeared and the degree of dynamic recrystallization increased. The alloy was completely dynamically recrystallized at 420 ℃ and 0.002 s^(-1), with a homogenous grain size of approximately 13.7 μm. The instability domains of the deformation behavior can be recognized by processing maps. By considering the processing maps and characterizing the microstructure, the optimum hot deformation parameters in this experiment were determined to be 420 ℃ and 0.002 s^(-1).展开更多
The hot deformation behaviors of FGH98 nickel-based powder superalloy were experimentally investigated and theoretically analyzed by Arrhenius models and machine learning(ML).Hot compression tests were conducted with ...The hot deformation behaviors of FGH98 nickel-based powder superalloy were experimentally investigated and theoretically analyzed by Arrhenius models and machine learning(ML).Hot compression tests were conducted with a Gleeble-3800 thermo-mechanical simulation machine on the FGH98 superalloy at strain rates of 0.001–1 s–1 and temperatures of 1025–1175℃.The peak stresses under different deformation conditions were analyzed via the Sellars model and an ML-inspired Gaussian process regression(GPR)model.The prediction of the GPR model outperformed that from the Sellars model.In addition,the stress-strain responses were predicted by the GPR model and tested by experimentally measured stress-strain curves.The results indicate that the developed GPR model has great power with wide generalization capability in the prediction of hot deformation behaviors of FGH98 superalloy,as evidenced by the R2 value higher than 0.99 on the test dataset.展开更多
The Cu-10 %Fe-1.5 %Ag in situ composite with high strength, high conductivity and low cost was prepared, and its hot deformation behavior was investigated by isothermal compression test with true strain of 0.69, tempe...The Cu-10 %Fe-1.5 %Ag in situ composite with high strength, high conductivity and low cost was prepared, and its hot deformation behavior was investigated by isothermal compression test with true strain of 0.69, temperature range of 750-950 ℃ and strain rate of 0.002-1.000 s^(-1). The flow stress-strain response shows the characterization of dynamic recrystallization(DRX), and the peak stress increases gradually with deformation temperature decreasing and strain rate increasing. The deformation activation energy of the composite for DRX is calculated as 241.864 kJ·mol^(-1). The constitutive relation of the composite was got by Arrhenius equation. Furthermore, according to the dynamic material modeling and Kumar-Prasad's instability criteria, the processing map was constructed and the unsafe regions for hot deformation were analyzed. Based on the processing map and microstructural evolution, the optimal parameter range for hot deformation processing is 750-863 ℃ at the strain rate of 0.002-0.013 s^(-1).展开更多
An Al-Cu-Mg-Zr alloy,which obtained different homogenization cooling rates by changing the heattreated sample size,was compressed to various strains at the deformation temperature of 300℃ and strain rate of 0.01 s^(-...An Al-Cu-Mg-Zr alloy,which obtained different homogenization cooling rates by changing the heattreated sample size,was compressed to various strains at the deformation temperature of 300℃ and strain rate of 0.01 s^(-1).The results showed that the homogenization cooling rate had strong effects on the hot deformation behavior of the alloy.The flow stress and relative dynamic softening rate of the alloy were significantly higher under a high cooling rate(HCR) than those under a low cooling rate(LCR).Furthermore,based on X-ray diffraction,scanning electron microscopy,transmission electron microscopy,and thermodynamic equilibrium phase calculation,the substructure evolution in the grain interior,morphology,and spatial distribution of the precipitates were studied to determine the differences in the flow softening mechanism.The main softening mechanism could be summarized as dynamic recovery and precipitation coarsening for the LCR alloy and dynamic precipitation for the HCR alloy.展开更多
In this study, hot compression bonding was first applied to join 14Cr ferrite steel at temperatures of 950–1200°C and strains of 0.11–0.51 under strain rates of 0.01–30 s^(-1).Subsequently, tensile tests were ...In this study, hot compression bonding was first applied to join 14Cr ferrite steel at temperatures of 950–1200°C and strains of 0.11–0.51 under strain rates of 0.01–30 s^(-1).Subsequently, tensile tests were performed on the joints to evaluate the reliability of the joints formed.Detailed microstructural analyses suggest that two different competing dynamic recrystallization(DRX) mechanisms occur during the bonding process depending on the strain rate, and the joints obtained at different strain rate exhibits distinct healing effect.At a low strain rate(0.01 s^(-1)), continuous DRX occurs, as expected in high-stackingfault-energy materials, and is characterized by the progressive conversion of the sub-boundaries into larger-angle boundaries, which involves very limited grain boundaries migration.In addition, straininduced precipitation(SIP) is sufficient under this condition, further impeding the healing of bonding interface.Hence, the joints obtained at low strain rate fractured at the bonding interface easily.Whereas discontinuous DRX is activated at high strain rates(10 and 30 s^(-1)).Under this condition, the formation of sub-boundaries is severely suppressed, resulting in the piling-up of dislocations and hence the storage of a greater amount of stored energy for nucleation and subsequent nuclei growth via the long-distance grain boundaries migration.Meanwhile, the SIP process is sluggish, making the conditions much more favorable for grain boundaries migration which plays a key role in the healing of the original bonding interface.Thus, the joints can be successfully bonded when a high strain rate is applied, with the joints exhibiting tensile properties similar to that of the base material.展开更多
The hot deformation behavior and microstructure evolution of an Fe–30Cr–2Mo ultra-pure super ferritic stainless steel were investigated at the temperature range of 950–1150℃ and strain rate varying from 0.01 to 10...The hot deformation behavior and microstructure evolution of an Fe–30Cr–2Mo ultra-pure super ferritic stainless steel were investigated at the temperature range of 950–1150℃ and strain rate varying from 0.01 to 10 s^(−1).A strain compensated constitutive equation based on the Arrhenius-type model was established to predict the flow stress.The hot processing map based on the dynamic materials model was achieved to identify the optimum processing parameters.In addition,the features of microstructure evolution combined with the processing map were systematically investigated.The experimental results revealed that the flow stress increased with decreasing deformation temperature or increasing strain rate.Dynamic recovery was confirmed to be the predominant softening mechanism.The values of flow stress predicted by the strain compensated constitutive equation agreed well with the experimental values.The extent of dynamic recrystallization and recrystallized grain size increased with increasing deformation temperature or decreasing strain rate,and the continuous dynamic recrystallization was attributed to be the predominant mechanism of recrystallization during hot deformation.The optimum hot working parameters were determined to be the deformation temperature of 1070–1150℃ and strain rate of 0.1–1 s^(−1) with a peak power dissipation efficiency of 42%.展开更多
In this work,the flow behaviors and microstructure evolution of a powder metallurgy nickel-based superalloy during superplastic compression is investigated.Based on the strain rate sensitivity m determined by flow dat...In this work,the flow behaviors and microstructure evolution of a powder metallurgy nickel-based superalloy during superplastic compression is investigated.Based on the strain rate sensitivity m determined by flow data,superplastic region is estimated at relatively low temperature and strain rate domains,specifically around 1000℃/10^-3s^-1.Thereafter,the cylinder specimens are isothermally compressed at 1000℃/10^-3s^-1 and 1025℃/10^-3s^-1 with different strains,to exam the superplasticity and related mechanisms.The experimental results indicate that the accumulated dislocations are mainly annihilated by dynamic recovery and dynamic recrystallization(DRX),and the grain boundary sliding(GBS)contributes to the total strain during superplastic compression as well.In addition,the cavities and cracks at triple junctions or interfaces between matrix and second phase particle have not been detected,which is different from superplastic tensile deformation.展开更多
The hot compression behavior of the nickel-based heat-resistant alloy C-HRA-2®was investigated by a Gleeble-1500 thermo-mechanical simulator with the deformation temperature range of 950-1150℃and the strain rate...The hot compression behavior of the nickel-based heat-resistant alloy C-HRA-2®was investigated by a Gleeble-1500 thermo-mechanical simulator with the deformation temperature range of 950-1150℃and the strain rate of 0.001-10 s^−1.The constitutive equation of the alloy was established by using a hyperbolic sine function,and the peak stress followed a power law relationship with the Zener-Hollomon parameter(Z).The activation energy was about 446 kJ mol^−1 for the whole hot deformation domain in this alloy.The optimum hot deformation condition was obtained in the temperature range of 1050-1150℃and the strain rate range of 0.005-0.1 s^−1.Unsafe domains during the hot deformation would occur in the strain rate range of 0.1-10 s^−1 with inhomogeneous microstructure and high-density twins in the alloy.The dominant nucleation mechanism of dynamic recrystallization(DRX)was continuous dynamic recrystallization with sub-grain rotation at high strain rate,while DRX at low strain rate was discontinuous dynamic recrystallization with original grain boundaries bulging.展开更多
The hot compressive deformation behavior of hot isostatically pressed Ti-47.5Al-2Cr-2Nb-0.2W-0.2B alloy using gas atomization powders was systematically investigated and the processing map was obtained in the temperat...The hot compressive deformation behavior of hot isostatically pressed Ti-47.5Al-2Cr-2Nb-0.2W-0.2B alloy using gas atomization powders was systematically investigated and the processing map was obtained in the temperature range of 1323-1473 Kand strain rate range of 0.001-0.5s^(-1).The calculated activation energy in the above variational ranges of temperature and strain rate possesses a low activation energy value of approximately 365.6kJ/mol based on the constitutive relationship models developed with the Arrhenius-type constitutive model respectively considering the strain rate and deformation temperature.The hot working flow behavior during the deformation process was analyzed combined with the microstructural evolution.Meanwhile,the processing maps during the deformation process were established based on the dynamic material model and Prasad instability criterion under different deformation conditions.Finally,the optimal hot processing window of this alloy corresponding to the wide temperature range of 1353-1453 Kand the low strain rate of 0.001-0.1s^(-1) was obtained.展开更多
Objective:To compare the clinical effect differences of biān(砭)stone hot compress combined with acupuncture at cervical Jiājǐ(夹脊EX-B2)acupoint and simple acupuncture at cervical EX-B2 for axial pain after cervic...Objective:To compare the clinical effect differences of biān(砭)stone hot compress combined with acupuncture at cervical Jiājǐ(夹脊EX-B2)acupoint and simple acupuncture at cervical EX-B2 for axial pain after cervical laminectomy with implant fixation(LIF)operation.Methods:A total of 80 patients with axial pain after cervical LIF operation were randomly assigned into the biān(砭)stone hot compress combined with acupuncture at cervical EX-B2 group(Group A)and the acupuncture at cervical EX-B2 group(Group B),and 40 patients in each group.The group A was treated by biān(砭)stone hot compress and acupuncture at cervical EX-B2,while the group B was treated by acupuncture at cervical EX-B2.Both of groups were treated once a day,one course of treatment consisted of 7 days,6-day treatment plus 1-day rest,and there were 3 courses of treatment in total.The pain score(Visual analogue scale,VAS),neck dysfunction indices(NDI),and serum creatine phosphokinase(CPK)levels of patients were compared before and after the treatment,and their clinical effects were evaluated.Results:The VAS score,NDI,and CPK in patients of the two groups after treatment were all lower than those before treatment(all P<0.05),and the indicators in the group A after treatment were all lower than those in the group B after treatment(all P<0.05).The effective rate in the group A was 92.5%,higher than that(77.5%)in the group B,and there was statistically significant difference(P<0.05).Conclusions:The biān(砭)stone hot compress combined with acupuncture at cervical EX-B2 acupoint was better than acupuncture at cervical EX-B2 alone in treatment of axial pain after cervical LIF operation.In the group A,therapeutic effects were improved by relieving pain,improving neck function,and repairing muscle injury.展开更多
基金The present work was financially supported by the National Natural Science Foundation of China(Nos.52074207 and 51874081)Key Laboratory of Ecological Metallurgy of Multimetallic Mineral(Northeastern University)of Ministry of Education.
文摘The effects of different hot deformation amounts on the evolution of inclusion and microstructure in Ti-Zr deoxidized steel were studied by utilizing the Thermecmaster-Z hot simulation test machine,automatic scanning electron microscope equipped with energy-dispersive spectrometer,and electron backscattered diffraction.The results indicated that hot deformation amount has no significant effect on the number density of oxide,but the MnS that precipitated on the Ti-Zr oxide surface undergoes extension and breakage,resulting in the changes in oxide aspect ratio.Moreover,the fracture of nitride mainly occurs in the sample with the second pass deformation amount of 42.9%and 71.4%,and the degree of fragmentation of nitride is more serious with the deformation amount increasing.During the hot compression,sulfide undergoes breakage and extension,and with the second pass deformation amount increasing,the breakage and extension of sulfide present a periodic change.Finally,with the increase in hot compression amount,the ferrite types in microstructure change from acicular ferrite and bainitic ferrite to polygonal ferrite,and the ferrite grain size is refined.When the total deformation amount increases from 30%to 80%,the ferrite grain sizes of grain boundary with the misorientation of 4°and 15°decrease from 4.14 and 5.67μm to 3.47 and 4.40μm,respectively.However,when the total deformation amount increases to 80%,the harmful ferrite/pearlite banded structure appears in the micro structure.Refining ferrite grain size and avoiding harmful microstructure are the key for the optimization of hot compression process.
基金This research was financially supported by the Science and Technology Major Project of Gansu Province(Grant No.17ZD2GB012)the City Key Research and Development Plan of Jiayuguan(Grant Nos.20-16).
文摘The optimization of hot compression technique of as-cast 0Cr23Ni13 stainless steel at high strain rate was discussed,and its corrosion resistance was evaluated after hot compression treatment experimentally.By adjusting the dynamic recrys-tallization(DRX)ratio of 0Cr23Nil3 stainless steel during hot pressing,the content of low Σ coincident site lattice(ΣCSL)grain boundaries is increased,and the grain orientation is optimized.The results show that ferrite and austenite are completely recrystallized at 1050 and 1150℃,respectively.The number of grains in the<111>and<101>directions increases significantly,the corrosion potential increases,and the corrosion current density decreases,which will signifi-cantly improve the corrosion resistance of 0Cr23Nil3 stainless steel.After the optimization of grain boundary distribution,corrosion resistance is noticeably improved due to the existence of lowΣCSL boundaries.The interference effect of lowΣCSL grain boundary on random grain boundary network becomes intense with the increase in DRX ratio,which is the fundamental measure to improve the corrosion resistance.
基金This study was financially supported by the National Natural Science Foundation of China(No.51804087)the Science and Technology Cooperative Foundation of Guizhou province(Nos.[2017]7240 and[2017]5788)+1 种基金the Basic Research Program of Guizhou Province(No.[2019]1091)the Youth Science and Technology Talent Growth Project of Guizhou Education Bureau(No.[2018]107)。
文摘In this study, microstructure and texture evolution of TB8 titanium alloys during hot deformation were investigated by using electron back-scattered diffraction(EBSD) analysis. The results showed that dynamic recrystallization(DRX) behavior of TB8 titanium alloys was drastically sensitive to the strain. As the true strain raised from 0.2 to 0.8, the degree of DRX gradually increased. The nucleation mechanism of recrystallization was observed, including discontinuous dynamic recrystallization(DDRX) resulting from the bulging of original boundaries. Furthermore, continuous dynamic recrystallization(CDRX) occurred because of the transformation of low-angle grain boundaries(LAGBs) to high-angle grain boundaries(HAGBs) in the interior of the original deformed grains. The texture evolution of TB8 titanium alloy during hot deformation process was analyzed in detail, and five texture components were observed,including{001}h100 i,{011}h100 i,{112}h110 i,{111}h110 i, and {111}h112 i. As the true strain increased,deformation textures were gradually weakened due to an increase in the volume fraction of DRX grains. When the true strain was 0.8, the main texture components consisted of the recrystallization texture components of the{001}h100 i and {011}h100 i textures.
基金financially supported by the National Key Research and Development Program of China(No.2016YFB0301300)the National Natural Science Foundation of China(Nos.51974028 and U1602271)。
文摘By means of isothermal compression at temperatures in the range of 650-900℃and strain rates in the range of 0.001-1 s^(-1),the dynamic recrystallization behavior and microstructural evolution of a Cu-3.28 Ni-0.6 Si-0.22 Zn-0.11 Cr-0.04 P(wt%)alloy designed by a machine learning method were investigated.A semiempirical constitutive equation,processing maps and an average activation energy were generated.The microstructure under different conditions and the effect of strain rate on the texture of the alloy at 800-900℃were observed.The results show that the suitable temperature is800-900℃;when the strain is less than 0.4,the appropriate strain rate is 0.01-0.5 s^(-1);and when the strain is greater than 0.4,the appropriate strain rate is below0.05 s^(-1).After deformation at 800℃,the main texture changed from{112}<111>of copper to a uniform distribution with the increase in strain rate,but the sample did not have obvious texture after deformation at 850 and900℃.The above results can provide a reference for the selection of process parameters.
基金Light Form,a UK Engineering and Physical Sciences Research Council(EPSRC)programme grant(EP/R001715/1)。
文摘This paper models hot compression testing using a dilatometer in loading mode.These small-scale tests provide a high throughput at low cost,but are susceptible to inhomogeneity due to friction and temperature gradients.A novel method is presented for correcting the true stress-strain constitutive response over the full range of temperatures,strain-rates and strain.The nominal response from the tests is used to predict the offset in the stress-strain curves due to inhomogeneity,and this stress offsetΔσis applied piecewise to the data,correcting the constitutive response in one iteration.A key new feature is the smoothing and fitting of the flow stress data as a function of temperature and strain-rate,at multiple discrete strains.The corrected model then provides quantitative prediction of the spatial and temporal variation in strain-rate and strain throughout the sample,needed to correlate the local deformation conditions with the microstructure and texture evolution.The study uses a detailed series of 144 hot compression tests of a Zr-Nb alloy.While this is an important wrought nuclear alloy in its own right,it also serves here as a test case for modelling the dilatometer for hot testing of high temperature alloys,particularly those with dualα-βphase microstructures(such as titanium alloys).
基金Funded by the Central Government Guides Local Funds for Science and Technology Development(No.YDZJSX20231A045)the Fundamental Research Program of Shanxi Province(Nos.202103021223288 and 202103021224282)。
文摘The evolution of microstructure during hot deformation is key to achieving good mechanical properties in aluminum alloys.We have developed a cellular automaton(CA) based model to simulate the microstructural evolution in 7075 aluminum alloy during hot deformation.Isothermal compression tests were conducted to obtain material parameters for 7075 aluminum alloy,leading to the establishment of models for dislocation density,nucleation of recrystallized grains,and grain growth.Integrating these aspects with grain topological deformation,our CA model effectively predicts flow stress,dynamic recrystallization(DRX) volume fraction,and average grain size under diverse deformation conditions.A systematic comparison was made between electron back scattered diffraction(EBSD) maps and CA model simulated under different deformation temperatures(573 to 723 K),strain rates(0.001 to 1 s^(-1)),and strain amounts(30% to 70%).These analyses indicate that large strain,high temperature,and low strain rate facilitate dynamic recrystallization and grain refinement.The results from the CA model show good accuracy and predictive capability,with experimental error within 10%.
基金financial support from National Natural Science Foundation of China(51875317)Key Research and Development Program of Shandong Province(2019GGX104087)National Natural Science Foundation of Shandong Province(ZR2019QEE030)
文摘The microstructure evolution of Mg-5.65 Zn-0.66 Zr(wt.%)alloy was studied based on the hot compression tests.The results indicated that the flow stress increased rapidly to a peak point at the initial stage,and then it gradually decreased.Moreover,high temperature and low strain rate resulted in the decreasing of flow stress.All samples exhibited a necklace grain structure because of the occurrence of partial dynamic recrystallization(DRX).High temperature increased both the size and fraction of DRXed grains,while high strain rate showed an opposite tendency.At the conditions of 350°C/0.001 s^(-1)and 350°C/0.1 s^(-1),the twins were not exhibited and DRX played a dominant role.Importantly,the obvious split of basal texture was observed.The pyramidal<c+a>slip with high value of Schmid factor was active in large deformed grains,which corresponded to the peak split point in(0001)pole figure.A mechanism about the grain rotation was proposed to explain the relationship between the pyramidal slip and the split of basal texture.Finally,it was found that large number of{10–12}extension twins were formed during the initial stage at condition of 300°C/1 s^(-1),and the number of twins decreased with the increase of strain.The twins greatly contributed to the fast formation of basal texture and grain rotation.Moreover,the non-basal slips were active in twining region,which could facilitate the nucleation of DRX.
文摘Hot compression tests were performed on AISI 321 austenitic stainless steel in the deformation temperature range of 800–1200℃ and constant strain rates of 0.001,0.01,0.1,and 1 s^(−1).Hot flow curves were used to determine the strain hardening exponent and the strain rate sensitivity exponent,and to construct the processing maps.Variations of the strain hardening exponent with strain were used to predict the microstructural evolutions during the hot deformation.Four variations were distinguished reflecting the different microstructural changes.Based on the analysis of the strain hardening exponent versus strain curves,the microstructural evolutions were dynamic recovery,single and multiple peak dynamic recrystallization,and interactions between dynamic recrystallization and precipitation.The strain rate sensitivity variations at an applied strain of 0.8 and strain rate of 0.1 s^(−1) were compared with the microstructural evolutions.The results demonstrate the existence of a reliable correlation between the strain rate sensitivity values and evolved microstructures.Additionally,the power dissipation map at the applied strain of 0.8 was compared with the resultant microstructures at predetermined deformation conditions.The microstructural evolutions strongly correlated to the power dissipation ratio,and dynamic recrystallization occurred completely at lower power dissipation ratios.
基金Funded by the National Natural Science Foundation of China(No.51204020)the National Program on Key Basic Research Project(No 2013CB632202)the Qinghai Provincial Science and Technology Support Project(2014-GX-106A)
文摘Hot compression tests on AZ40 magnesium alloy were conducted on a Gleeble 1500 d hot simulation testing machine in a deformation temperature range of 330 ℃-420 ℃ and a strain rate range of 0.002-2 s^(-1). Hot deformation behaviors were investigated on the basis of the analysis of the flow stressstrain curves, constitutive equation, and processing map. The stress exponent and apparent activation energy were calculated to be 5.821 and 173.96 k J/mol, respectively. Deformation twins and cracks located in grain boundaries were generated at 330 ℃ and 0.02 s^(-1), which are associated with a high strain rate and a limited number of available slip systems. With increasing temperature and decreasing strain rate, the twins disappeared and the degree of dynamic recrystallization increased. The alloy was completely dynamically recrystallized at 420 ℃ and 0.002 s^(-1), with a homogenous grain size of approximately 13.7 μm. The instability domains of the deformation behavior can be recognized by processing maps. By considering the processing maps and characterizing the microstructure, the optimum hot deformation parameters in this experiment were determined to be 420 ℃ and 0.002 s^(-1).
基金supported by the National Natural Science Foundation of China(No.91860115)the Science,Technology,and Innovation Commission of Shenzhen Municipality(No.JSGG20210802093205015).
文摘The hot deformation behaviors of FGH98 nickel-based powder superalloy were experimentally investigated and theoretically analyzed by Arrhenius models and machine learning(ML).Hot compression tests were conducted with a Gleeble-3800 thermo-mechanical simulation machine on the FGH98 superalloy at strain rates of 0.001–1 s–1 and temperatures of 1025–1175℃.The peak stresses under different deformation conditions were analyzed via the Sellars model and an ML-inspired Gaussian process regression(GPR)model.The prediction of the GPR model outperformed that from the Sellars model.In addition,the stress-strain responses were predicted by the GPR model and tested by experimentally measured stress-strain curves.The results indicate that the developed GPR model has great power with wide generalization capability in the prediction of hot deformation behaviors of FGH98 superalloy,as evidenced by the R2 value higher than 0.99 on the test dataset.
基金financially supported by the National Natural Science Foundation of China(No.50571035)the National High-Tech Research and Development Project (No.2006AA03Z528)
文摘The Cu-10 %Fe-1.5 %Ag in situ composite with high strength, high conductivity and low cost was prepared, and its hot deformation behavior was investigated by isothermal compression test with true strain of 0.69, temperature range of 750-950 ℃ and strain rate of 0.002-1.000 s^(-1). The flow stress-strain response shows the characterization of dynamic recrystallization(DRX), and the peak stress increases gradually with deformation temperature decreasing and strain rate increasing. The deformation activation energy of the composite for DRX is calculated as 241.864 kJ·mol^(-1). The constitutive relation of the composite was got by Arrhenius equation. Furthermore, according to the dynamic material modeling and Kumar-Prasad's instability criteria, the processing map was constructed and the unsafe regions for hot deformation were analyzed. Based on the processing map and microstructural evolution, the optimal parameter range for hot deformation processing is 750-863 ℃ at the strain rate of 0.002-0.013 s^(-1).
基金financially supported by the National Natural Science Foundation of China(Nos.51674111 and51605234)the Research Fund for the Doctoral Program of Higher Education of China(No.20130161110007)。
文摘An Al-Cu-Mg-Zr alloy,which obtained different homogenization cooling rates by changing the heattreated sample size,was compressed to various strains at the deformation temperature of 300℃ and strain rate of 0.01 s^(-1).The results showed that the homogenization cooling rate had strong effects on the hot deformation behavior of the alloy.The flow stress and relative dynamic softening rate of the alloy were significantly higher under a high cooling rate(HCR) than those under a low cooling rate(LCR).Furthermore,based on X-ray diffraction,scanning electron microscopy,transmission electron microscopy,and thermodynamic equilibrium phase calculation,the substructure evolution in the grain interior,morphology,and spatial distribution of the precipitates were studied to determine the differences in the flow softening mechanism.The main softening mechanism could be summarized as dynamic recovery and precipitation coarsening for the LCR alloy and dynamic precipitation for the HCR alloy.
基金financial support from the National Key Research and Development Program of China(Grant No.2018YFA0702900)the National Natural Science Foundation of China(Grant Nos.U1508215,51774265)+2 种基金the Key Program of the Chinese Academy of Sciences(Grant No.ZDRW-CN-2017-1)the National Science and Technology Major Project of China(Grant No.2019ZX06004010)the CAS Interdisciplinary Innovation Team。
文摘In this study, hot compression bonding was first applied to join 14Cr ferrite steel at temperatures of 950–1200°C and strains of 0.11–0.51 under strain rates of 0.01–30 s^(-1).Subsequently, tensile tests were performed on the joints to evaluate the reliability of the joints formed.Detailed microstructural analyses suggest that two different competing dynamic recrystallization(DRX) mechanisms occur during the bonding process depending on the strain rate, and the joints obtained at different strain rate exhibits distinct healing effect.At a low strain rate(0.01 s^(-1)), continuous DRX occurs, as expected in high-stackingfault-energy materials, and is characterized by the progressive conversion of the sub-boundaries into larger-angle boundaries, which involves very limited grain boundaries migration.In addition, straininduced precipitation(SIP) is sufficient under this condition, further impeding the healing of bonding interface.Hence, the joints obtained at low strain rate fractured at the bonding interface easily.Whereas discontinuous DRX is activated at high strain rates(10 and 30 s^(-1)).Under this condition, the formation of sub-boundaries is severely suppressed, resulting in the piling-up of dislocations and hence the storage of a greater amount of stored energy for nucleation and subsequent nuclei growth via the long-distance grain boundaries migration.Meanwhile, the SIP process is sluggish, making the conditions much more favorable for grain boundaries migration which plays a key role in the healing of the original bonding interface.Thus, the joints can be successfully bonded when a high strain rate is applied, with the joints exhibiting tensile properties similar to that of the base material.
基金This work is supported by the Liaoning Province Programs of Science and Technology Development(No.2019JH2/10100009).
文摘The hot deformation behavior and microstructure evolution of an Fe–30Cr–2Mo ultra-pure super ferritic stainless steel were investigated at the temperature range of 950–1150℃ and strain rate varying from 0.01 to 10 s^(−1).A strain compensated constitutive equation based on the Arrhenius-type model was established to predict the flow stress.The hot processing map based on the dynamic materials model was achieved to identify the optimum processing parameters.In addition,the features of microstructure evolution combined with the processing map were systematically investigated.The experimental results revealed that the flow stress increased with decreasing deformation temperature or increasing strain rate.Dynamic recovery was confirmed to be the predominant softening mechanism.The values of flow stress predicted by the strain compensated constitutive equation agreed well with the experimental values.The extent of dynamic recrystallization and recrystallized grain size increased with increasing deformation temperature or decreasing strain rate,and the continuous dynamic recrystallization was attributed to be the predominant mechanism of recrystallization during hot deformation.The optimum hot working parameters were determined to be the deformation temperature of 1070–1150℃ and strain rate of 0.1–1 s^(−1) with a peak power dissipation efficiency of 42%.
基金supported financially by the National Key Research and Development Program of China (No.2016YFB0701404)the National Natural Science Foundation of China (No.91860105)the Fund from Innovation and Entrepreneur Team Introduced by Guangdong Province (No. 201301G0105337290)
文摘In this work,the flow behaviors and microstructure evolution of a powder metallurgy nickel-based superalloy during superplastic compression is investigated.Based on the strain rate sensitivity m determined by flow data,superplastic region is estimated at relatively low temperature and strain rate domains,specifically around 1000℃/10^-3s^-1.Thereafter,the cylinder specimens are isothermally compressed at 1000℃/10^-3s^-1 and 1025℃/10^-3s^-1 with different strains,to exam the superplasticity and related mechanisms.The experimental results indicate that the accumulated dislocations are mainly annihilated by dynamic recovery and dynamic recrystallization(DRX),and the grain boundary sliding(GBS)contributes to the total strain during superplastic compression as well.In addition,the cavities and cracks at triple junctions or interfaces between matrix and second phase particle have not been detected,which is different from superplastic tensile deformation.
基金the financial support from the National Key Research and Development Plan(Grant No.2017YFB0305201).
文摘The hot compression behavior of the nickel-based heat-resistant alloy C-HRA-2®was investigated by a Gleeble-1500 thermo-mechanical simulator with the deformation temperature range of 950-1150℃and the strain rate of 0.001-10 s^−1.The constitutive equation of the alloy was established by using a hyperbolic sine function,and the peak stress followed a power law relationship with the Zener-Hollomon parameter(Z).The activation energy was about 446 kJ mol^−1 for the whole hot deformation domain in this alloy.The optimum hot deformation condition was obtained in the temperature range of 1050-1150℃and the strain rate range of 0.005-0.1 s^−1.Unsafe domains during the hot deformation would occur in the strain rate range of 0.1-10 s^−1 with inhomogeneous microstructure and high-density twins in the alloy.The dominant nucleation mechanism of dynamic recrystallization(DRX)was continuous dynamic recrystallization with sub-grain rotation at high strain rate,while DRX at low strain rate was discontinuous dynamic recrystallization with original grain boundaries bulging.
基金the financial supports from the National Natural Science Foundation of China(Grant Nos.51301157 and 51434007)the National High Technology Research and Development Program of China 863 Program(Grant No.2013AA031103)
文摘The hot compressive deformation behavior of hot isostatically pressed Ti-47.5Al-2Cr-2Nb-0.2W-0.2B alloy using gas atomization powders was systematically investigated and the processing map was obtained in the temperature range of 1323-1473 Kand strain rate range of 0.001-0.5s^(-1).The calculated activation energy in the above variational ranges of temperature and strain rate possesses a low activation energy value of approximately 365.6kJ/mol based on the constitutive relationship models developed with the Arrhenius-type constitutive model respectively considering the strain rate and deformation temperature.The hot working flow behavior during the deformation process was analyzed combined with the microstructural evolution.Meanwhile,the processing maps during the deformation process were established based on the dynamic material model and Prasad instability criterion under different deformation conditions.Finally,the optimal hot processing window of this alloy corresponding to the wide temperature range of 1353-1453 Kand the low strain rate of 0.001-0.1s^(-1) was obtained.
文摘Objective:To compare the clinical effect differences of biān(砭)stone hot compress combined with acupuncture at cervical Jiājǐ(夹脊EX-B2)acupoint and simple acupuncture at cervical EX-B2 for axial pain after cervical laminectomy with implant fixation(LIF)operation.Methods:A total of 80 patients with axial pain after cervical LIF operation were randomly assigned into the biān(砭)stone hot compress combined with acupuncture at cervical EX-B2 group(Group A)and the acupuncture at cervical EX-B2 group(Group B),and 40 patients in each group.The group A was treated by biān(砭)stone hot compress and acupuncture at cervical EX-B2,while the group B was treated by acupuncture at cervical EX-B2.Both of groups were treated once a day,one course of treatment consisted of 7 days,6-day treatment plus 1-day rest,and there were 3 courses of treatment in total.The pain score(Visual analogue scale,VAS),neck dysfunction indices(NDI),and serum creatine phosphokinase(CPK)levels of patients were compared before and after the treatment,and their clinical effects were evaluated.Results:The VAS score,NDI,and CPK in patients of the two groups after treatment were all lower than those before treatment(all P<0.05),and the indicators in the group A after treatment were all lower than those in the group B after treatment(all P<0.05).The effective rate in the group A was 92.5%,higher than that(77.5%)in the group B,and there was statistically significant difference(P<0.05).Conclusions:The biān(砭)stone hot compress combined with acupuncture at cervical EX-B2 acupoint was better than acupuncture at cervical EX-B2 alone in treatment of axial pain after cervical LIF operation.In the group A,therapeutic effects were improved by relieving pain,improving neck function,and repairing muscle injury.
