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Pollen viability of Polygala paniculata L.(Polygalaceae)using different staining methods 被引量:1
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作者 VIVIANE DAL-SOUTO FRESCURA HAYWOOD DAIL LAUGHINGHOUSE IV +1 位作者 THAIS SCOTTI DO CANTO-DOROW SOLANGE BOSIO TEDESCO 《BIOCELL》 SCIE 2012年第3期143-145,共3页
Polygala paniculata L.is a medicinal plant that grows in the Brazilian Atlantic coast,known as‘barba-de-São-João’,‘barba-de-bode’,‘vassourinha branca’,and‘mimosa’.In this study,pollen viability was e... Polygala paniculata L.is a medicinal plant that grows in the Brazilian Atlantic coast,known as‘barba-de-São-João’,‘barba-de-bode’,‘vassourinha branca’,and‘mimosa’.In this study,pollen viability was estimated by three different staining methods:2%acetic orcein,2%acetic carmine,and Alexander’s stain.The young inflorescences of twenty accessions were collected and fixed in a solution of ethanol:acetic acid(3:1)for 24 hours,then stored in ethanol 70%under refrigeration.Six slides per plant,two for each stain,were prepared by squashing,and 300 pollen grains per slide were analyzed.Pollen viability was high(>70%)for most accessions of P.paniculata using the Alexander’s stain,which proved the most adequate method to estimate pollen viability. 展开更多
关键词 pollen grains barba-de-bode acetic orcein acetic carmine Alexander’s stain
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COMPARISON OF DIFFERENT STAINING METHODS FOR ANALYSING ESTERASE (EST) ISOZYME OF FUNGI AND PLANTS
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作者 池玉杰 张明 +1 位作者 程东升 许翠青 《Journal of Northeast Forestry University》 SCIE CAS CSCD 1996年第4期24-27,共4页
EST isozymes are one of the frequently used biochemical markers in genetic analysis of fungi. and the staining is an important process in electrophoresis analysis of studying Est.The effects were compared ainong diffe... EST isozymes are one of the frequently used biochemical markers in genetic analysis of fungi. and the staining is an important process in electrophoresis analysis of studying Est.The effects were compared ainong different stain recipes for Est of 3 kinds of fungi-Lentinus edodes. Pleurotus sapidus. Phellinus igriarius and 2 kinds of plants-Populus sp and Brassica chinensis. Of the four kinds of Est staining recipes tested.the recipe α-acetic acid-naphther showed the best effect.and followed by β-aceticacid-naphther, semicontent α-aceticacid-naphther and α+β-aceticacidnathpher. 展开更多
关键词 FUNGI ESTERASE ISOZYME staining methods
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A RAPID STAINING METHOD SHOWING AgNOR AND DNA IN PATHOLOGICAL DIAGNOSIS
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作者 龚志锦 郑唯强 +1 位作者 詹镕洲 陶文照 《Chinese Journal of Cancer Research》 SCIE CAS CSCD 1994年第2期139-143,共5页
ARAPIDSTAININGMETHODSHOWINGAgNORANDDNAINPATHOLOGICALDIAGNOSISGongZhijin;龚志锦;ZhengWeiqiang;郑唯强;ZhanRongzhou;詹... ARAPIDSTAININGMETHODSHOWINGAgNORANDDNAINPATHOLOGICALDIAGNOSISGongZhijin;龚志锦;ZhengWeiqiang;郑唯强;ZhanRongzhou;詹镕洲;TaoWenzhao;陶文照... 展开更多
关键词 AGNOR staining method DNA stainingmethod.
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Fluorescence of Tb-Ibuprofenum-Phen Complex and New Tissue Staining Method
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作者 李桂芝 刘永明 《Journal of Rare Earths》 SCIE EI CAS CSCD 2005年第S1期33-35,共3页
A new complex Tb(IB)3(phen)·2H2O that gives off green fluorescence was synthesized. The results show that the strong fluorescence emitting of 490 and 545 nm for Tb 3+ in the Tb(IB)3(phen)·2H2O comple... A new complex Tb(IB)3(phen)·2H2O that gives off green fluorescence was synthesized. The results show that the strong fluorescence emitting of 490 and 545 nm for Tb 3+ in the Tb(IB)3(phen)·2H2O complex is related to the transitions 5D4-7F6 and 5D4-7F5, respectively. The results indicate that the complex is concentrated on the nuclei regions in the section of onion toot tip tissues and the nuclei are high lighted under fluorescent microscope. It is possible that the Tb(IB)3(phen)·2H2O complex can be developed as a fluorescent dye in biological and pathological studies. 展开更多
关键词 TB 3+-complex ibuprofenum PHEN FLUORESCENCE TISSUE staining rare earths
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Application of an indirect immunofluorescent staining method for detection of Salmonella enteritidis in paraffin slices and antigen location in infected duck tissues 被引量:7
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作者 Bin Yan An-Chun Cheng +5 位作者 Ming-Shu Wang Shu-Xuan Deng Zhen-Hua Zhang Nian-Chun Yin Ping Cao Sheng-Yan Cao 《World Journal of Gastroenterology》 SCIE CAS CSCD 2008年第5期776-781,共6页
AIM:To detect Salmonella enteritidis (S. enteritidis) in paraffin slices and antigen location in infected duck tissues. METHODS:Rabbits were immunized with purified bacillus to obtain S. enteritidis-specific antibody,... AIM:To detect Salmonella enteritidis (S. enteritidis) in paraffin slices and antigen location in infected duck tissues. METHODS:Rabbits were immunized with purified bacillus to obtain S. enteritidis-specific antibody, which were then extracted by the caprylic-ammonium sulphate method, purified through High-Q columns. An indirect immuno-fluorescent staining method (IFA) was established to detect the S. enteritidis antigen in paraffin slices. S. enteritidis was detected in each organ tissue of ducklings experimentally infected with S. enteritidis. RESULTS:The gland of Garder, heart, kidney, spleen, liver, brain, ileum, jejunum, bursa of Fabricius from S. enteritidis experimentally infected ducklings were positive or strongly positive, and the S. enteritidis antigen was mainly distributed in the infected cell cytoplasm.CONCLUSION:IFA is an intuitionist, sensitive and specific method in detecting S. enteritidis antigen in paraffin wax slices, and it is a good method in diagnosis and antigen location of S. enteritidis. We also conclude that the gland of Garder, heart, kidney, spleen, liver, ileum, jejunum are target organs in S. enteritidis infections of duck, and S. enteritidis is an intracellular parasitic bacterium. 展开更多
关键词 沙门氏菌肠炎 检测方法 疾病 症状
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A NEW STAINING METHOD FOR THE MEASUREMENT OF PROTEIN USING TETRAPHENYLPORPHYRIN TETRASULFONATE(TPPS_4)
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作者 Shen Yang TONG Na LI Chemistry Department,Peking University,Beijing,100871 《Chinese Chemical Letters》 SCIE CAS CSCD 1993年第12期1079-1080,共2页
A new dye-staining method for protein assay is described.The reactionbetween TPPS<sub>4</sub> and protein molecule causes a shift in the absorption of TPPS<sub>4</sub>from 435 nm to 488nm.The a... A new dye-staining method for protein assay is described.The reactionbetween TPPS<sub>4</sub> and protein molecule causes a shift in the absorption of TPPS<sub>4</sub>from 435 nm to 488nm.The absorbance at 488 nm is proportional to theconcentration of protein.The range of Beer’s law was 1-5 ug/ml and the Sandell’ssensitivity was 0.0087 ug/cm<sup>2</sup>. 展开更多
关键词 ABSORBANCE staining proportional blank DILUTED herein BRADFORD bovine deter IgG
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A Comparative Study on Four Staining Methods for Antitumor Active Fraction of Periplaneta americana
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作者 Shaohui WU Chenggui ZHANG +1 位作者 Xiumei WU Guangming LIU 《Agricultural Biotechnology》 CAS 2012年第1期61-63,共3页
[Objective] This study aimed to compare four staining methods for proteins of SDS-polyacrylamide gel electrophoresis(SDS-PAGE) and explore a suitable staining method for the antitumor active fraction of P.americana af... [Objective] This study aimed to compare four staining methods for proteins of SDS-polyacrylamide gel electrophoresis(SDS-PAGE) and explore a suitable staining method for the antitumor active fraction of P.americana after polyacrylamide gel electrophoresis.[Method] BSA was used as the standard for the comparison of Coomassie brilliant blue staining method,potassium staining method,calcium staining method and silver staining method,on the basis,antitumor active fraction samples of P.americana were used for SDS-PAGE electrophoresis and staining.[Result] The results showed that silver staining method could be accurately,quickly and easily used for SDS-PAGE staining of the antitumor active fraction of P.americana.[Conclusion] This study laid the foundation for exploring the medicinal value of P.americana. 展开更多
关键词 染色方法 美洲大蠊 抗肿瘤 SDS-PAGE电泳 活性组分 聚丙烯酰胺凝胶电泳 银染色法 活性部位
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A Review on Sources,Extractions and Analysis Methods of a Sustainable Biomaterial:Tannins
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作者 Antonio Pizzi Marie-Pierre Laborie Zeki Candan 《Journal of Renewable Materials》 EI CAS 2024年第3期397-425,共29页
Condensed and hydrolysable tannins are non-toxic natural polyphenols that are a commercial commodity industrialized for tanning hides to obtain leather and for a growing number of other industrial applications mainly ... Condensed and hydrolysable tannins are non-toxic natural polyphenols that are a commercial commodity industrialized for tanning hides to obtain leather and for a growing number of other industrial applications mainly to substitute petroleum-based products.They are a definite class of sustainable materials of the forestry industry.They have been in operation for hundreds of years to manufacture leather and now for a growing number of applications in a variety of other industries,such as wood adhesives,metal coating,pharmaceutical/medical applications and several others.This review presents the main sources,either already or potentially commercial of this forestry by-materials,their industrial and laboratory extraction systems,their systems of analysis with their advantages and drawbacks,be these methods so simple to even appear primitive but nonetheless of proven effectiveness,or very modern and instrumental.It constitutes a basic but essential summary of what is necessary to know of these sustainable materials.In doing so,the review highlights some of the main challenges that remain to be addressed to deliver the quality and economics of tannin supply necessary to fulfill the industrial production requirements for some materials-based uses. 展开更多
关键词 TANNINS FLAVONOIDS SOURCES extraction methods analysis methods
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Review of Collocation Methods and Applications in Solving Science and Engineering Problems
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作者 Weiwu Jiang Xiaowei Gao 《Computer Modeling in Engineering & Sciences》 SCIE EI 2024年第7期41-76,共36页
The collocation method is a widely used numerical method for science and engineering problems governed by partial differential equations.This paper provides a comprehensive review of collocation methods and their appl... The collocation method is a widely used numerical method for science and engineering problems governed by partial differential equations.This paper provides a comprehensive review of collocation methods and their applications,focused on elasticity,heat conduction,electromagnetic field analysis,and fluid dynamics.The merits of the collocation method can be attributed to the need for element mesh,simple implementation,high computational efficiency,and ease in handling irregular domain problems since the collocation method is a type of node-based numerical method.Beginning with the fundamental principles of the collocation method,the discretization process in the continuous domain is elucidated,and how the collocation method approximation solutions for solving differential equations are explained.Delving into the historical development of the collocation methods,their earliest applications and key milestones are traced,thereby demonstrating their evolution within the realm of numerical computation.The mathematical foundations of collocation methods,encompassing the selection of interpolation functions,definition of weighting functions,and derivation of integration rules,are examined in detail,emphasizing their significance in comprehending the method’s effectiveness and stability.At last,the practical application of the collocation methods in engineering contexts is emphasized,including heat conduction simulations,electromagnetic coupled field analysis,and fluid dynamics simulations.These specific case studies can underscore collocation method’s broad applicability and effectiveness in addressing complex engineering challenges.In conclusion,this paper puts forward the future development trend of the collocation method through rigorous analysis and discussion,thereby facilitating further advancements in research and practical applications within these fields. 展开更多
关键词 Collocation method meshless method discrete schemes for functions numerical calculation
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Stabilization With Prescribed Instant via Lyapunov Method
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作者 Jiyuan Kuang Yabin Gao +2 位作者 Yizhuo Sun Aohua Liu Jianxing Liu 《IEEE/CAA Journal of Automatica Sinica》 SCIE EI CSCD 2024年第2期557-559,共3页
Dear Editor,This letter presents a prescribed-instant stabilization approach to high-order integrator systems by the Lyapunov method. Under the presented controller, the settling time of controlled systems is independ... Dear Editor,This letter presents a prescribed-instant stabilization approach to high-order integrator systems by the Lyapunov method. Under the presented controller, the settling time of controlled systems is independent of the initial conditions and equals the prescribed time instant. 展开更多
关键词 method. PRESCRIBED INSTANT
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An Evidence-Based CoCoSo Framework with Double Hierarchy Linguistic Data for Viable Selection of Hydrogen Storage Methods
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作者 Raghunathan Krishankumar Dhruva Sundararajan +1 位作者 K.S.Ravichandran Edmundas Kazimieras Zavadskas 《Computer Modeling in Engineering & Sciences》 SCIE EI 2024年第3期2845-2872,共28页
Hydrogen is the new age alternative energy source to combat energy demand and climate change.Storage of hydrogen is vital for a nation’s growth.Works of literature provide different methods for storing the produced h... Hydrogen is the new age alternative energy source to combat energy demand and climate change.Storage of hydrogen is vital for a nation’s growth.Works of literature provide different methods for storing the produced hydrogen,and the rational selection of a viable method is crucial for promoting sustainability and green practices.Typically,hydrogen storage is associated with diverse sustainable and circular economy(SCE)criteria.As a result,the authors consider the situation a multi-criteria decision-making(MCDM)problem.Studies infer that previous models for hydrogen storage method(HSM)selection(i)do not consider preferences in the natural language form;(ii)weights of experts are not methodically determined;(iii)hesitation of experts during criteria weight assessment is not effectively explored;and(iv)three-stage solution of a suitable selection of HSM is unexplored.Driven by these gaps,in this paper,authors put forward a new integrated framework,which considers double hierarchy linguistic information for rating,criteria importance through inter-criteria correlation(CRITIC)for expert weight calculation,evidence-based Bayesian method for criteria weight estimation,and combined compromise solution(CoCoSo)for ranking HSMs.The applicability of the developed framework is testified by using a case example of HSM selection in India.Sensitivity and comparative analysis reveal the merits and limitations of the developed framework. 展开更多
关键词 Hydrogen storage methods double hierarchy hesitant fuzzy linguistic term set evidence theory CoCoSo method sustainability circular economy
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A Hierarchical Method for Locating the Interferometric Fringes of Celestial Sources in the Visibility Data
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作者 Rong Ma Ruiqing Yan +7 位作者 Hanshuai Cui Xiaochun Cheng Jixia Li Fengquan Wu Zongyao Yin Hao Wang Wenyi Zeng Xianchuan Yu 《Research in Astronomy and Astrophysics》 SCIE CAS CSCD 2024年第3期110-128,共19页
In source detection in the Tianlai project,locating the interferometric fringe in visibility data accurately will influence downstream tasks drastically,such as physical parameter estimation and weak source exploratio... In source detection in the Tianlai project,locating the interferometric fringe in visibility data accurately will influence downstream tasks drastically,such as physical parameter estimation and weak source exploration.Considering that traditional locating methods are time-consuming and supervised methods require a great quantity of expensive labeled data,in this paper,we first investigate characteristics of interferometric fringes in the simulation and real scenario separately,and integrate an almost parameter-free unsupervised clustering method and seeding filling or eraser algorithm to propose a hierarchical plug and play method to improve location accuracy.Then,we apply our method to locate single and multiple sources’interferometric fringes in simulation data.Next,we apply our method to real data taken from the Tianlai radio telescope array.Finally,we compare with unsupervised methods that are state of the art.These results show that our method has robustness in different scenarios and can improve location measurement accuracy effectively. 展开更多
关键词 methods data analysis-techniques image processing-techniques INTERFEROMETRIC
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Nonlinear Flap-Wise Vibration Characteristics ofWind Turbine Blades Based onMulti-Scale AnalysisMethod
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作者 Qifa Lang Yuqiao Zheng +2 位作者 Tiancai Cui Chenglong Shi Heyu Zhang 《Energy Engineering》 EI 2024年第2期483-498,共16页
This work presents a novel approach to achieve nonlinear vibration response based on the Hamilton principle.We chose the 5-MW reference wind turbine which was established by the National Renewable Energy Laboratory(NR... This work presents a novel approach to achieve nonlinear vibration response based on the Hamilton principle.We chose the 5-MW reference wind turbine which was established by the National Renewable Energy Laboratory(NREL),to research the effects of the nonlinear flap-wise vibration characteristics.The turbine wheel is simplified by treating the blade of a wind turbine as an Euler-Bernoulli beam,and the nonlinear flap-wise vibration characteristics of the wind turbine blades are discussed based on the simplification first.Then,the blade’s large-deflection flap-wise vibration governing equation is established by considering the nonlinear term involving the centrifugal force.Lastly,it is truncated by the Galerkin method and analyzed semi-analytically using the multi-scale analysis method,and numerical simulations are carried out to compare the simulation results of finite elements with the numerical simulation results using Campbell diagram analysis of blade vibration.The results indicated that the rotational speed of the impeller has a significant impact on blade vibration.When the wheel speed of 12.1 rpm and excitation amplitude of 1.23 the maximum displacement amplitude of the blade has increased from 0.72 to 3.16.From the amplitude-frequency curve,it can be seen that the multi-peak characteristic of blade amplitude frequency is under centrifugal nonlinearity.Closed phase trajectories in blade nonlinear vibration,exhibiting periodic motion characteristics,are found through phase diagrams and Poincare section diagrams. 展开更多
关键词 Wind turbine blades nonlinear vibration Galerkin method multi-scales method
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Efficient method to calculate the eigenvalues of the Zakharov–Shabat system
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作者 崔世坤 王振 《Chinese Physics B》 SCIE EI CAS CSCD 2024年第1期243-249,共7页
A numerical method is proposed to calculate the eigenvalues of the Zakharov–Shabat system based on Chebyshev polynomials. A mapping in the form of tanh(ax) is constructed according to the asymptotic of the potential ... A numerical method is proposed to calculate the eigenvalues of the Zakharov–Shabat system based on Chebyshev polynomials. A mapping in the form of tanh(ax) is constructed according to the asymptotic of the potential function for the Zakharov–Shabat eigenvalue problem. The mapping can distribute Chebyshev nodes very well considering the gradient for the potential function. Using Chebyshev polynomials, tanh(ax) mapping, and Chebyshev nodes, the Zakharov–Shabat eigenvalue problem is transformed into a matrix eigenvalue problem. This method has good convergence for the Satsuma–Yajima potential and the convergence rate is faster than the Fourier collocation method. This method is not only suitable for simple potential functions but also converges quickly for a complex Y-shape potential. It can also be further extended to other linear eigenvalue problems. 展开更多
关键词 Zakharov–Shabat system EIGENVALUE numerical method Chebyshev polynomials
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Research into Applicability of Wöhler Curve Method for Low-Cycle Fatigue of Metallic Materials
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作者 Xiangqiao Yan 《Journal of Harbin Institute of Technology(New Series)》 CAS 2024年第2期22-37,共16页
Recently,a description on a practicability of the Wöhler Curve Method for low-cycle fatigue of metals was given by the author.By the description and the low cycle fatigue test data of 16 MnR steel,it is important... Recently,a description on a practicability of the Wöhler Curve Method for low-cycle fatigue of metals was given by the author.By the description and the low cycle fatigue test data of 16 MnR steel,it is important to show that,for low cycle fatigue of metals,such a way that a stress-based intensity parameter calculated by the linear-elastic analysis is taken to be a stress intensity parameter,S,to establish a relationship between the stress intensity parameter,S,and the fatigue life,N,is practicable.In this paper,many metallic materials from the literature are given to show that the Wöhler Curve Method is well suitable for low-cycle fatigue analysis of metals. 展开更多
关键词 low cycle fatigue Wöhler curve method coffin-manson curve method METALS
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Recommendation Method for Contrastive Enhancement of Neighborhood Information
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作者 Hairong Wang Beijing Zhou +1 位作者 Lisi Zhang He Ma 《Computers, Materials & Continua》 SCIE EI 2024年第1期453-472,共20页
Knowledge graph can assist in improving recommendation performance and is widely applied in various person-alized recommendation domains.However,existing knowledge-aware recommendation methods face challenges such as ... Knowledge graph can assist in improving recommendation performance and is widely applied in various person-alized recommendation domains.However,existing knowledge-aware recommendation methods face challenges such as weak user-item interaction supervisory signals and noise in the knowledge graph.To tackle these issues,this paper proposes a neighbor information contrast-enhanced recommendation method by adding subtle noise to construct contrast views and employing contrastive learning to strengthen supervisory signals and reduce knowledge noise.Specifically,first,this paper adopts heterogeneous propagation and knowledge-aware attention networks to obtain multi-order neighbor embedding of users and items,mining the high-order neighbor informa-tion of users and items.Next,in the neighbor information,this paper introduces weak noise following a uniform distribution to construct neighbor contrast views,effectively reducing the time overhead of view construction.This paper then performs contrastive learning between neighbor views to promote the uniformity of view information,adjusting the neighbor structure,and achieving the goal of reducing the knowledge noise in the knowledge graph.Finally,this paper introduces multi-task learning to mitigate the problem of weak supervisory signals.To validate the effectiveness of our method,experiments are conducted on theMovieLens-1M,MovieLens-20M,Book-Crossing,and Last-FM datasets.The results showthat compared to the best baselines,our method shows significant improvements in AUC and F1. 展开更多
关键词 Contrastive learning knowledge graph recommendation method
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Dynamic Coupling Analysis of Semisubmersible Platform Float-over Method for Docking Case
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作者 DING Hongyan QIN Licheng +2 位作者 ZHANG Puyang SONG Zhengrong XIE Weiwei 《Journal of Ocean University of China》 CAS CSCD 2024年第2期345-357,共13页
In this paper,the multi-body coupled dynamic characteristics of a semisubmersible platform and an HYSY 229 barge were investigated.First,coupled hydrodynamic analysis of the HYSY 229 barge and the semisubmersible plat... In this paper,the multi-body coupled dynamic characteristics of a semisubmersible platform and an HYSY 229 barge were investigated.First,coupled hydrodynamic analysis of the HYSY 229 barge and the semisubmersible platform was performed.Relevant hydrodynamic parameters were obtained using the retardation function method of three-dimensional frequency-domain potential flow theory.The results of the hydrodynamic analysis were highly consistent with the test findings,verifying the accuracy of the multifloating hydrodynamic coupling analysis,and key hydrodynamic parameters were solved for different water depths and the coupling effect.According to the obtained results,the hydrodynamic influence was the largest in shallow waters when the coupling effect was considered.Furthermore,the coupled motion equation combined with viscous damping,fender system,and mooring system was established,and the hydrodynamics,floating body motion,and dynamic response of the fender system were analyzed.Motion analysis revealed good agreement among the surge,sway,and yaw motions of the two floating bodies.However,when the wave period reached 10 s,the motion of the two floating bodies showed severe shock,and a relative motion was also observed.Therefore,excessive constraints should be added between the two floating bodies during construction to ensure construction safety.The numerical analysis and model test results of the semisubmersible platform and HYSY 229 barge at a water depth of 42 m and sea conditions of 0°,45°,and 90° were in good agreement,and the error was less than 5%.The maximum movement of the HYSY 229 barge reached 2.61 m in the sway direction,whereas that of the semisubmersible platform was 2.11 m.During construction,excessive constraints should be added between the two floating bodies to limit their relative movement and ensure construction safety. 展开更多
关键词 float-over method semisubmersible platform coupling hydrodynamic fender system time-domain analysis
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Comparison study on measurement of rail weld joint between inertial reference method and multi-point chord reference method
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作者 Yifan Shi Yuan Wang +1 位作者 Xiaozhou Liu Ping Wang 《Railway Sciences》 2024年第1期69-83,共15页
Purpose – Straightness measurement of rail weld joint is of essential importance to railway maintenance. Dueto the lack of efficient measurement equipment, there has been limited in-depth research on rail weld joint ... Purpose – Straightness measurement of rail weld joint is of essential importance to railway maintenance. Dueto the lack of efficient measurement equipment, there has been limited in-depth research on rail weld joint with a5-m wavelength range, leaving a significant knowledge gap in this field.Design/methodology/approach – In this study, the authors used the well-established inertial referencemethod (IR-method), and the state-of-the-art multi-point chord reference method (MCR-method). Two methodshave been applied in different types of rail straightness measurement trollies, respectively. These instrumentswere tested in a high-speed rail section within a certain region of China. The test results were ultimatelyvalidated through using traditional straightedge and feeler gauge methods as reference data to evaluate the railweld joint straightness within the 5-m wavelength range.Findings – The research reveals that IR-method and MCR-method produce reasonably similar measurementresults for wavelengths below 1 m. However, MCR-method outperforms IR-method in terms of accuracy forwavelengths exceeding 3 m. Furthermore, it was observed that IR-method, while operating at a slower speed,carries the risk of derailing and is incapable of detecting rail weld joints and low joints within the track.Originality/value – The research compare two methods’ measurement effects in a longer wavelength rangeand demonstrate the superiority of MCR-method. 展开更多
关键词 Rail weld joint Inertial reference method Short-wavelength irregularities Multi-point chord reference method 5-m wavelength range
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Simplified quantitative analysis method and its application in the insitu synthesized copper-based azide chips
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作者 Jie Ren Yunfeng Li +3 位作者 Mingyu Li Xingyu Wu Jiabao Wang Qingxuan Zeng 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2024年第2期309-316,共8页
Copper-based azide(Cu(N_(3))2 or CuN_(3),CA)chips synthesized by in-situ azide reaction and utilized in miniaturized explosive systems has become a hot research topic in recent years.However,the advantages of in-situ ... Copper-based azide(Cu(N_(3))2 or CuN_(3),CA)chips synthesized by in-situ azide reaction and utilized in miniaturized explosive systems has become a hot research topic in recent years.However,the advantages of in-situ synthesis method,including small size and low dosage,bring about difficulties in quantitative analysis and differences in ignition capabilities of CA chips.The aim of present work is to develop a simplified quantitative analysis method for accurate and safe analysis of components in CA chips to evaluate and investigate the corresponding ignition ability.In this work,Cu(N_(3))2 and CuN_(3)components in CA chips were separated through dissolution and distillation by utilizing the difference in solubility and corresponding content was obtained by measuring N_(3)-concentration through spectrophotometry.The spectrophotometry method was optimized by studying influencing factors and the recovery rate of different separation methods was studied,ensuring the accuracy and reproducibility of test results.The optimized method is linear in range from 1.0-25.0 mg/L,with a correlation coefficient R^(2)=0.9998,which meets the requirements of CA chips with a milligram-level content test.Compared with the existing ICP method,component analysis results of CA chips obtained by spectrophotometry are closer to real component content in samples and have satisfactory accuracy.Moreover,as its application in miniaturized explosive systems,the ignition ability of CA chips with different component contents for direct ink writing CL-20 and the corresponding mechanism was studied.This study provided a basis and idea for the design and performance evaluation of CA chips in miniaturized explosive systems. 展开更多
关键词 Copper-based azide chips SPECTROPHOTOMETRY Separation method Quantitative analysis Ignition ability
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