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Use of Magic Angle Spinning ~1H NMR Spectroscopy to Monitor Reactions in Solid-Phase Synthesis 被引量:1
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作者 Ai Ming YU Hua Zheng YANG(The State Key Laboratory of Elemento-Organic Chemistry, Nankai University, Tianjin 300071)Ping Chuan SUN +1 位作者 Zhen Pu ZHANG Ming LI(The State Key Laboratory of Functional Polymeric Materials for Adsorption and Separation,Nankai Uni 《Chinese Chemical Letters》 SCIE CAS CSCD 1997年第12期0-0,共2页
Proton NMR-spectra of Wang resin bound compounds were obtained using the magic angle spinning 1HNMR technique with standard equipment. It was possible to analyse the spectra to evaluate their utility in solid-phase ch... Proton NMR-spectra of Wang resin bound compounds were obtained using the magic angle spinning 1HNMR technique with standard equipment. It was possible to analyse the spectra to evaluate their utility in solid-phase chernistry. A typical example was presented, which could directly monitor solid-phase reactions 展开更多
关键词 NMR Spectroscopy to Monitor Reactions in Solid-Phase synthesis Use of Magic Angle Spinning DCC DCM
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