Waxy crude oil exhibits complex rheological behavior below the pour point temperature, such as viscoelasticity, yield stress, and thixotropy, owing to the formation of a three-dimensional spongelike interlock network ...Waxy crude oil exhibits complex rheological behavior below the pour point temperature, such as viscoelasticity, yield stress, and thixotropy, owing to the formation of a three-dimensional spongelike interlock network structure. This viscoelasto-thixotropic behavior is an important rheologieal behavior of waxy crude oils, determining the flow recovery and safe restart of crude oil pipelines. Up to now, the thixotropic models for waxy crude have been all viscoplastic models, without considering the viscoelastic part before the yield point. In this work, based on analyzing the variation of the elastic stress and viscous stress in the Mujumbar model, a new viscoelasto-plastic model is proposed, whose shear stress is separated into an elastic component and a viscous component. The elastic stress is the product of the shear modulus and elastic strain; the shear modulus is proportional to the structural parameter. For the elastic strain, we followed the line of Zhu and his coauthors and assumed that it may be expressed by an algebraic equation. The model is validated by stepwise shear rate tests and hysteresis loop tests on Daqing and Zhongyuan waxy crude. The results show that the model's fitting and predictive capability is satisfactory.展开更多
Using a circular incremental step load and unload method, a set of rheological experiments were performed to study the viscoelasto-plastic properties of amphibolite in Jinchuan No.2 diggings under different environmen...Using a circular incremental step load and unload method, a set of rheological experiments were performed to study the viscoelasto-plastic properties of amphibolite in Jinchuan No.2 diggings under different environments. Based on the scientific analysis on rheological experimental data, the viscoelasto-plastic properties of amphibolite under different environments were studied. The results show that the instantaneous elastic modulus and viscoplastic properties of amphibolite are affected little, the viscoelastic properties of amphibolite are significantly affected. Based on the experimental results and characteristics of recovered rock specimen, a generalized Kelvin model was chosen to simulate rheological properties of amphibolites and key parameters were obtained. It is found that the creep deformation modulus E1 is significantly influenced by the water, while the instant elastic modulus E2 is not significantly affected. The discreteness of the viscosity coefficient η is large, the influence of water on η is not clear and needs to be further studied.展开更多
A creep experiment of preformed molding coal under different confining pressures were carried out using self-developed 3-triaxial creep loading device for gas-containing coal, which loaded by Shimadzu AGI-250 kN elect...A creep experiment of preformed molding coal under different confining pressures were carried out using self-developed 3-triaxial creep loading device for gas-containing coal, which loaded by Shimadzu AGI-250 kN electrical servo-controlled stiffness testing machine. Based on the experimental results, the variation trend of axial deformation under different stress states was studied, and creep failure characteristics of gas-containing coal under different confining pressures were analyzed. The experimental results were identified with seven-component nonlinear viscoelasto-plastic creep model (Hohai model), and the creep material parameters were obtained. The experimental result complies well with the theoretical value of this model. It indicates that creep constitutive relation of gas-containing coal can be expressed by nonlinear viscoelasto-plastic creep model correctly.展开更多
基金the financial support from the National Natural Science Foundation of China (Grant No.51134006)Science Foundation of China University of Petroleum (Beijing) (Grant No.LLYJ-2011-55)
文摘Waxy crude oil exhibits complex rheological behavior below the pour point temperature, such as viscoelasticity, yield stress, and thixotropy, owing to the formation of a three-dimensional spongelike interlock network structure. This viscoelasto-thixotropic behavior is an important rheologieal behavior of waxy crude oils, determining the flow recovery and safe restart of crude oil pipelines. Up to now, the thixotropic models for waxy crude have been all viscoplastic models, without considering the viscoelastic part before the yield point. In this work, based on analyzing the variation of the elastic stress and viscous stress in the Mujumbar model, a new viscoelasto-plastic model is proposed, whose shear stress is separated into an elastic component and a viscous component. The elastic stress is the product of the shear modulus and elastic strain; the shear modulus is proportional to the structural parameter. For the elastic strain, we followed the line of Zhu and his coauthors and assumed that it may be expressed by an algebraic equation. The model is validated by stepwise shear rate tests and hysteresis loop tests on Daqing and Zhongyuan waxy crude. The results show that the model's fitting and predictive capability is satisfactory.
基金Project (10972238) supported by the National Natural Science Foundation of ChinaProject (2009bsxt061) supported by the Thesis Innovation Funds for the Central South University, ChinaProject (2009) supported by Hunan Administration of Work Safety Fund, China
文摘Using a circular incremental step load and unload method, a set of rheological experiments were performed to study the viscoelasto-plastic properties of amphibolite in Jinchuan No.2 diggings under different environments. Based on the scientific analysis on rheological experimental data, the viscoelasto-plastic properties of amphibolite under different environments were studied. The results show that the instantaneous elastic modulus and viscoplastic properties of amphibolite are affected little, the viscoelastic properties of amphibolite are significantly affected. Based on the experimental results and characteristics of recovered rock specimen, a generalized Kelvin model was chosen to simulate rheological properties of amphibolites and key parameters were obtained. It is found that the creep deformation modulus E1 is significantly influenced by the water, while the instant elastic modulus E2 is not significantly affected. The discreteness of the viscosity coefficient η is large, the influence of water on η is not clear and needs to be further studied.
基金National Basic Research Program of China (973 program)(2005CB221502) National Natural Science Foundation of China(50534080) National Natural Science Foundation of China(50604021 )
文摘A creep experiment of preformed molding coal under different confining pressures were carried out using self-developed 3-triaxial creep loading device for gas-containing coal, which loaded by Shimadzu AGI-250 kN electrical servo-controlled stiffness testing machine. Based on the experimental results, the variation trend of axial deformation under different stress states was studied, and creep failure characteristics of gas-containing coal under different confining pressures were analyzed. The experimental results were identified with seven-component nonlinear viscoelasto-plastic creep model (Hohai model), and the creep material parameters were obtained. The experimental result complies well with the theoretical value of this model. It indicates that creep constitutive relation of gas-containing coal can be expressed by nonlinear viscoelasto-plastic creep model correctly.