The contents ofMg, Al, Si, Ti, Cr, Mn, Fe, Co, Cu, Ga, As, Se, Cd, Sb, Pb and Bi in high purity nickel were determined by high resolution inductively coupled plasma mass spectrometry （HR-ICP-MS）. The sample was diss...The contents ofMg, Al, Si, Ti, Cr, Mn, Fe, Co, Cu, Ga, As, Se, Cd, Sb, Pb and Bi in high purity nickel were determined by high resolution inductively coupled plasma mass spectrometry （HR-ICP-MS）. The sample was dissolved in HNO3 and HCI by microwave digestion. Most of the spectral interferences could be avoided by measuring in the high resolution mode. The matrix effects because of the presence of excess HC1 and nickel were evaluated. Correction for matrix effects was made using Sc, Rh and T1 as internal standards. The optimum conditions for the determination were tested and discussed. The detection limits range from 0.012 to 1.76 ~tg/g depending on the type of elements. The applicability of the proposed method is also validated by the analysis of high purity nickel reference material （NIST SRM 671）. The relative standard deviation （RSD） is less than 3.3%. Results for determination of trace elements in high purity nickel were presented.展开更多
In this paper, we conduct research on the project-driven alliance between the college and enterprise teaching mode and the applications on the contemporary vocational education. To achieve the aim of higher education ...In this paper, we conduct research on the project-driven alliance between the college and enterprise teaching mode and the applications on the contemporary vocational education. To achieve the aim of higher education popularization in our country, to vigorously develop vocational education is the important way. Higher vocational education for national and local economic development is the purpose of training the production, construction, management and service first line need to cultivate high quality personnel. Higher vocational education is the social demand as the primary guidance of employment education, cultivate the students should be a technology applied talents with skills. Our research proposes the novel guideline to deal with the mentioned issues which is applicable.展开更多
基金Project(21075138) supported by the National Natural Science Foundation of ChinaProject(cstc2011jjA0780) supported by Natural Science Foundation of Chongqing City,ChinaProject(KJ121311) supported by Educational Commission of Chongqing City of China
文摘The contents ofMg, Al, Si, Ti, Cr, Mn, Fe, Co, Cu, Ga, As, Se, Cd, Sb, Pb and Bi in high purity nickel were determined by high resolution inductively coupled plasma mass spectrometry （HR-ICP-MS）. The sample was dissolved in HNO3 and HCI by microwave digestion. Most of the spectral interferences could be avoided by measuring in the high resolution mode. The matrix effects because of the presence of excess HC1 and nickel were evaluated. Correction for matrix effects was made using Sc, Rh and T1 as internal standards. The optimum conditions for the determination were tested and discussed. The detection limits range from 0.012 to 1.76 ~tg/g depending on the type of elements. The applicability of the proposed method is also validated by the analysis of high purity nickel reference material （NIST SRM 671）. The relative standard deviation （RSD） is less than 3.3%. Results for determination of trace elements in high purity nickel were presented.
文摘In this paper, we conduct research on the project-driven alliance between the college and enterprise teaching mode and the applications on the contemporary vocational education. To achieve the aim of higher education popularization in our country, to vigorously develop vocational education is the important way. Higher vocational education for national and local economic development is the purpose of training the production, construction, management and service first line need to cultivate high quality personnel. Higher vocational education is the social demand as the primary guidance of employment education, cultivate the students should be a technology applied talents with skills. Our research proposes the novel guideline to deal with the mentioned issues which is applicable.
