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低浓度六价铬样品回收率测定中加标量问题的探讨 被引量:1
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作者 刘瑞芹 贾立军 罗爱民 《承德石油高等专科学校学报》 CAS 2001年第3期18-20,共3页
通过对大量低浓度环境样品六价铬的加标回收率测定表明 :加标量控制在方法测定下限的 4倍时 ,加标回收率样品能达到 1 0 0 %合格 ,加标量在测定下限的 3倍时 ,合格率可达 85 .7% ,如果加标量过低 。
关键词 低浓度六价铬 环境样品 标回收率 测定 加标量
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低浓度样品加标回收测定中的加标量问题
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作者 刘瑞芹 《中国环境监测》 CAS CSCD 北大核心 2002年第1期5-5,共1页
关键词 低浓度样品 标回收测定 加标量
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化学需氧量检测的标准方法及加标回收率的测定 被引量:3
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作者 王红 张威 范丹 《辽宁师专学报(自然科学版)》 2015年第2期99-101,108,共4页
用重铬酸钾法对化学需氧量进行分析并进行加标回收.建立水质化学需氧量分析的加标方案和方法,提高了分析准确度.加标量一般是待测物含量的0.5~2.0倍.加标物以浓度高、体积小为好,加标物的体积不超过原始试样体积的1%,加标后总含量不超... 用重铬酸钾法对化学需氧量进行分析并进行加标回收.建立水质化学需氧量分析的加标方案和方法,提高了分析准确度.加标量一般是待测物含量的0.5~2.0倍.加标物以浓度高、体积小为好,加标物的体积不超过原始试样体积的1%,加标后总含量不超过方法的线性范围最大值.化学需氧量分析的加标回收率为100.3%. 展开更多
关键词 化学需氧量 加标量 标回收率
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加标回收法在环境水质低浓度样品分析过程中的应用 被引量:4
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作者 李德春 傅凯文 +1 位作者 李雅妍 张静 《中国高新技术企业》 2016年第27期83-85,共3页
文章对加标回收法在环境水质低浓度样品监测分析过程中出现的问题进行了论述,从低浓度样品的加标量和回收率的限值范围问题入手,分别对加标回收率测定时的测量方法、操作手法、试验试剂、水质温度及仪器设备等实验方面的系统误差,测定... 文章对加标回收法在环境水质低浓度样品监测分析过程中出现的问题进行了论述,从低浓度样品的加标量和回收率的限值范围问题入手,分别对加标回收率测定时的测量方法、操作手法、试验试剂、水质温度及仪器设备等实验方面的系统误差,测定的精密度问题和计算方面带来的误差问题进行了分析,确立了相应对策。 展开更多
关键词 标回收法 环境水质 低浓度样品监测 加标量 回收率
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大气监测中氮氧化物加标回收与质量控制
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作者 周炜 管小梅 +1 位作者 陈静 曹红俊 《江汉大学学报》 2001年第3期34-35,共2页
探讨大气监测中氮氧化物全程加标回收测定的方法,总结做好加标回收实验的主要条件及影响因素.
关键词 氮氧化物 全程标回收 质量控制 大气监测 加标量 回收率
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高效液相色谱法分析海水中的氯霉素 被引量:14
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作者 胡莹莹 叶赛 +3 位作者 李爱 徐恒振 王菊英 马德毅 《环境化学》 CAS CSCD 北大核心 2005年第4期481-482,共2页
在海水养殖中,氯霉素被认为是抑制对虾病原弧菌作用最强的药物.由于氯霉素存在严重的副作用,能引起人的再生障碍性贫血、粒状白细胞缺乏症等疾病,许多发达国家相继禁止或严格限制使用氯霉素.因此,有必要对养殖环境中残留的氯霉素进行监... 在海水养殖中,氯霉素被认为是抑制对虾病原弧菌作用最强的药物.由于氯霉素存在严重的副作用,能引起人的再生障碍性贫血、粒状白细胞缺乏症等疾病,许多发达国家相继禁止或严格限制使用氯霉素.因此,有必要对养殖环境中残留的氯霉素进行监测.目前,有关海洋环境介质中痕量氯霉素检测方法的研究报道不多,在相关的实验室加标试验中,由于加标量较大,水样中的氯霉素采取直接进样. 展开更多
关键词 氯霉素 高效液相色谱法 再生障碍性贫血 海水养殖 病原弧菌 限制使用 发达国家 养殖环境 检测方法 环境介质 直接进样 副作用 缺乏症 白细胞 实验室 加标量 对虾 残留
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水质检验中回收率的校正问题 被引量:1
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作者 郎碧玲 《内蒙古石油化工》 CAS 1999年第4期53-54,58,共3页
水质检验中计算回收率时,加标量与定容总体积之比有关。
关键词 水质检验 回收率 校正 加标量 定容总体积
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肉制品中亚硝酸盐国标测定方法的探讨 被引量:10
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作者 谭燕 庄松娟 《肉类工业》 2005年第7期26-28,共3页
为了对肉制品中亚硝酸盐含量实施有效的监督,我们分别利用GB/T5009.33-1996,GB/T5009.33-2003两版国标方法对同一样品进行了检测和比较,进行了高、中、低3种浓度的加标试验,结果表明:两版国标方法对肉类亚硝酸盐检测的精密度均较高;添... 为了对肉制品中亚硝酸盐含量实施有效的监督,我们分别利用GB/T5009.33-1996,GB/T5009.33-2003两版国标方法对同一样品进行了检测和比较,进行了高、中、低3种浓度的加标试验,结果表明:两版国标方法对肉类亚硝酸盐检测的精密度均较高;添加高标量亚硝酸钠时,两版回收率都较高,无明显差别,但随加标量的降低,1996版的回收率逐渐明显低于2003版,说明2003版的灵敏度高于1996版。两版国标方法的交叉实验表明两版的差异主要来自于样品前处理的不同,同时我们建议在GB/T5009.33-2003版格里斯试剂比色法测定肉制品亚硝酸盐的样品处理过程于沸水中加热15min应延长至30min。 展开更多
关键词 肉制品 国标 测定方法 2003版 亚硝酸盐含量 样品前处理 比色法测定 格里斯试剂 亚硝酸钠 处理过程 回收率 GB 精密度 加标量 灵敏度 检测 肉类 沸水
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冷饮中糖精钠的简捷测定法
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作者 项丹 李质华 《吉林医学院学报》 1998年第2期54-55,共2页
目的:建立糖精钠的快速测定。方法:碳酸氢钠比色法。结果:方法操作简单、检测迅速、重现性较好,灵敏度较高。结论:此方法测定冷饮中糖精钠较准确、可靠。
关键词 糖精钠 加标量 碳酸氢钠 冷饮
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Fast and secure elliptic curve scalar multiplication algorithm based on special addition chains
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作者 刘双根 胡予濮 《Journal of Southeast University(English Edition)》 EI CAS 2008年第1期29-32,共4页
To resist the side chaimel attacks of elliptic curve cryptography, a new fast and secure point multiplication algorithm is proposed. The algorithm is based on a particular kind of addition chains involving only additi... To resist the side chaimel attacks of elliptic curve cryptography, a new fast and secure point multiplication algorithm is proposed. The algorithm is based on a particular kind of addition chains involving only additions, providing a natural protection against side channel attacks. Moreover, the new addition formulae that take into account the specific structure of those chains making point multiplication very efficient are proposed. The point multiplication algorithm only needs 1 719 multiplications for the SAC260 of 160-bit integers. For chains of length from 280 to 260, the proposed method outperforms all the previous methods with a gain of 26% to 31% over double-and add, 16% to22% over NAF, 7% to 13% over4-NAF and 1% to 8% over the present best algorithm--double-base chain. 展开更多
关键词 scalar multiplication algorithm special addition chains side channel attacks double base chain
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Energy increment criteria for evaluation of train derailment 被引量:2
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作者 向俊 曾庆元 《Journal of Central South University of Technology》 2005年第2期233-238,共6页
The criteria for evaluation of train derailment were studied. The worldwide commonly used evaluation criteria for wheel derailment were summarized and their main problems were pointed out. The mechanism of train derai... The criteria for evaluation of train derailment were studied. The worldwide commonly used evaluation criteria for wheel derailment were summarized and their main problems were pointed out. The mechanism of train derailment was expounded on the basis of system dynamics stability concept. And the energy increment criteria were proposed to evaluate train derailment. By applying the criteria, the calculated results concerning 6 cases of freight train derailment on tangent railway line and 6 cases of freight train derailment on bridge were obtained, which are all in agreement with the practical situation. The safety, comfort and stability results concerning 3 cases of freight train running on bridge were analyzed. In addition, the running speed limits of freight train on the Yanconggou and Donggou bridge in the Beijing-Tonghua railway line of 50km/h and 60km/h, respectively, were proposed. And the running speed of freight train on the Nanjing Yangtze River Bridge can reach 70km/h. 展开更多
关键词 train derailment derailment mechanism energy increment criterion EVALUATION
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Novel Frequency Hopping Sequences Generator Based on AES Algorithm 被引量:2
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作者 李振荣 庄奕琪 +1 位作者 张博 张超 《Transactions of Tianjin University》 EI CAS 2010年第1期22-27,共6页
A novel frequency hopping(FH) sequences generator based on advanced encryption standard(AES) iterated block cipher is proposed for FH communication systems.The analysis shows that the FH sequences based on AES algorit... A novel frequency hopping(FH) sequences generator based on advanced encryption standard(AES) iterated block cipher is proposed for FH communication systems.The analysis shows that the FH sequences based on AES algorithm have good performance in uniformity, correlation, complexity and security.A high-speed, low-power and low-cost ASIC of FH sequences generator is implemented by optimizing the structure of S-Box and MixColumns of AES algorithm, proposing a hierarchical power management strategy, and applying ... 展开更多
关键词 frequency hopping sequences advanced encryption standard LOW-POWER LOW-COST application specific integrated circuit
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Effective Way of Finding Common Eigenvectors of Center-of-Mass Coordinate and Mass-Weighted Relative Momenta of Multi-Partite via IWOP Technique
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作者 刘述光 范洪义 《Communications in Theoretical Physics》 SCIE CAS CSCD 2010年第3期455-461,共7页
We present a convenient approach to finding multi-partite entangled state with continuum variables, which is the common eigenvectors of center-of-mass coordinate and mass-weighted relative momenta, by decomposing the ... We present a convenient approach to finding multi-partite entangled state with continuum variables, which is the common eigenvectors of center-of-mass coordinate and mass-weighted relative momenta, by decomposing the normally ordered Gaussian-form operator expressing the completeness relation which is constructed by analyzing the eigenvector equations. The whole derivation is based on the technique of integration within an ordered product of operators. 展开更多
关键词 multi-partite entangled state IWOP technique
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Simulation Study on a Heat Pump System Using R744/R290 as Refrigerant 被引量:3
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作者 Xiaowei Fan Xianping Zhang Fengkun Wang 《Journal of Civil Engineering and Architecture》 2013年第2期220-226,共7页
Based on the Chinese National Standards involving heat pump water heater and space heating system, performances of the R744/R290 subcritical heat pump system have been discussed and compared with those of the R22 syst... Based on the Chinese National Standards involving heat pump water heater and space heating system, performances of the R744/R290 subcritical heat pump system have been discussed and compared with those of the R22 system, which is widely used in heat pump systems in China nowadays. It can be indicated that R744/R290 mixture can work efficiently as a refrigerant for heat pumps with a large heat-sink temperature rise. When mass fraction of R290 is increased, discharge pressure is reduced. Under the nominal working condition, there is an optimum mixture mass fraction of 20/80 for R744/R290 under conventional condensation pressure. Both the heating COPhs (coefficient of performance) and volumetric heating capacity are increased by about 12.62% and 34.24% respectively compared with those of R22 based system. But for the heat sink with a small temperature rise, R744/R290 system has poorer performances than R22 system. When heat transfer pinch point in evaporator and condensation processes is considered, the degree of superheat has a negative influence upon system performances under the given conditions. 展开更多
关键词 Carbon dioxide PROPANE subcritical heat pump pinch point COP.
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Multiple dependent reliability estimation of large range MEMS accelerometers in high temperature environment
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作者 QIN Li HE Cheng +2 位作者 YU Li-xia WANG Wei QIN Li-jun 《Journal of Measurement Science and Instrumentation》 CAS CSCD 2019年第1期9-15,共7页
In the past,only one performance parameter was considered in the reliability estimation of micro-electro-mechanical system (MEMS) accelerometers,resulting in a one-sided reliability evaluation. Aiming at the failure c... In the past,only one performance parameter was considered in the reliability estimation of micro-electro-mechanical system (MEMS) accelerometers,resulting in a one-sided reliability evaluation. Aiming at the failure condition of large range MEMS accelerometers in high temperature environment,the corresponding accelerated degradation test is designed. According to the degradation condition of zero bias and scale factor,multiple dependent reliability estimation of large range MEMS accelerometers is carried out. The results show that the multiple dependent reliability estimation of the large range MEMS accelerometers can improve the accuracy of the estimation and get more accurate results. 展开更多
关键词 large range MEMS accelerometers zero bias scale factor multiple dependent reliability estimation accelerated degradation test
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Non-Maximal Tripartite Entanglement Degradation of Dirac and Scalar Fields in Non-Inertial Frames 被引量:1
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作者 Salman Khan Niaz Ali Khan M.K.Khan 《Communications in Theoretical Physics》 SCIE CAS CSCD 2014年第3期281-288,共8页
The π-tangle is used to study the behavior of entanglement of a nonmaximal tripartite state of both Dirac and scMar fields in accelerated frame. For Dirac fields, the degree of degradation with acceleration of both o... The π-tangle is used to study the behavior of entanglement of a nonmaximal tripartite state of both Dirac and scMar fields in accelerated frame. For Dirac fields, the degree of degradation with acceleration of both one-tangle of accelerated observer and π-tangle, for the same initial entanglement, is different by just interchanging the values of probability amplitudes. A fraction of both one-tangles and the π-tangle always survives for any choice of acceleration and the degree of initial entanglement. For scalar field, the one-tangle of accelerated observer depends on the choice of values of probability amplitudes and it vanishes in the range of infinite acceleration, whereas for 1r-tangle this is not always true. The dependence of π-tangle on probability amplitudes varies with acceleration. In the lower range of acceleration, its behavior changes by switching between the values of probability amplitudes and for larger values of acceleration this dependence on probability amplitudes vanishes. Interestingly, unlike bipartite entanglement, the degradation of π-tangle against acceleration in the case of sca/ar fields is slower than for Dirac fields. 展开更多
关键词 tripartite entanglement noninertial frame
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