针对 X 射线衍射分析设备应用于压力管道腐蚀检测过程中的价值进行分析,能够缩短检测的速度,分析腐蚀诱发的原因,为压力管道腐蚀的预防及管道的科学维护奠定基础。通过实验研究的方式,具体分析压力管道常见的腐蚀物及成分,为承压类特种...针对 X 射线衍射分析设备应用于压力管道腐蚀检测过程中的价值进行分析,能够缩短检测的速度,分析腐蚀诱发的原因,为压力管道腐蚀的预防及管道的科学维护奠定基础。通过实验研究的方式,具体分析压力管道常见的腐蚀物及成分,为承压类特种设备的事故原因调查提供重要数据支撑。展开更多
Pitting and stress corrosion cracking(SCC) studies on the 316 N stainless steel(SS) weldments in aswelded(AW) and thermally aged(solution annealing(SA), 550C/4 h and 750C/1 h) conditions were carried out in acidic and...Pitting and stress corrosion cracking(SCC) studies on the 316 N stainless steel(SS) weldments in aswelded(AW) and thermally aged(solution annealing(SA), 550C/4 h and 750C/1 h) conditions were carried out in acidic and acidic chloride media. Pitting corrosion and SCC resistance was the highest for SA weldment, which was attributed to homogenization of microstructural and microchemical heterogeneities during solution annealing. SA specimen showed the most stable passive film as compared to AW weldment because of higher amount of delta-ferrite in AW weld metal, which resulted in an increased heterogeneity and inferior SCC resistance in AW. Stability of passive film was found to be adversely affected due to heat treatments(at 550C/4 h and 750C/1 h) because of the precipitation of carbide and sigma phases.展开更多
Capability of a novel severe plastic deformation(SPD)method of hydrostatic cyclic extrusion compression(HCEC)for processing of hcp metallic rods with high length to diameter ratios was investigated.The process was con...Capability of a novel severe plastic deformation(SPD)method of hydrostatic cyclic extrusion compression(HCEC)for processing of hcp metallic rods with high length to diameter ratios was investigated.The process was conducted in two consecutive cycles on the AZ91 magnesium alloy,and microstructural evolution,mechanical properties and corrosion behavior were investigated.The results showed that the HCEC process was successively capable of producing ultrafine-grained long magnesium rods.Its ability in improving strength and ductility simultaneously was also shown.The ultimate tensile strength and elongation to failure of the sample after the second cycle of the process were improved to be 2.46 and 3.8 times those of the as-cast specimen,respectively.Distribution of the microhardness after the second cycle was uniform and its average value was increased by 116%.The potentials derived from the polarization curves were high and the currents were much low for the processed samples.Also,the diameter of the capacitive arcs derived from the Nyquist curves was large in the HCEC processed samples.The finite element analysis indicated the independency of HCEC load from the length in comparison to the conventional CEC.HCEC is a unique SPD method,which can produce long ultrafine-grained rods with a combination of superior mechanical and corrosion properties.展开更多
The effects of single-stage solution treatment(SST),enhanced solution treatment(EST),high-temperature pre-precipitation(HTPP)and multi-stage solution treatment(MST)on the microstructure,mechanical properties and corro...The effects of single-stage solution treatment(SST),enhanced solution treatment(EST),high-temperature pre-precipitation(HTPP)and multi-stage solution treatment(MST)on the microstructure,mechanical properties and corrosion resistance of the as-extruded 7055 aluminium alloy(AA7055)helical profile were investigated using differential scanning calorimetry(DSC),optical microscopy(OM),scanning electron microscopy(SEM),electron back-scattered diffraction(EBSD)and transmission electron microscopy(TEM).It was observed that EST and MST could promote the dissolution of the second-phase particles compared with the traditional SST,and the intergranular phases were distinctly discontinuously distributed after HTPP and MST.There was obvious difference in the main texture type and texture strength for the alloy after different solid solution treatments.HTPP could improve the corrosion resistance of the alloy by regulating the intergranular phases,but the mechanical properties were severely weakened.While the good corrosion resistance of the alloy could be obtained by MST without obvious strength loss.As a result,the MST is an ideal solid solution treatment scheme for AA7055.展开更多
During the whole operation life of Bratsk and Ust-Ilimsk hydroelectric plants, chemical analysis of water filtering through the pressure front of the concrete dams was under systematic monitoring by sampling in places...During the whole operation life of Bratsk and Ust-Ilimsk hydroelectric plants, chemical analysis of water filtering through the pressure front of the concrete dams was under systematic monitoring by sampling in places of concemrated outcome in the inspection galleries of a dam. Long-term cumulative observations made up a basis for study of the indicated dams concrete corrosion caused by the Angara water in the process of its filtration through the cracks formed in the period of the dam erection, through construction joims and other defects. Mathematical-statistical analysis allowed the classification the processes of corrosion from the point of view of their time dynamics and divided them correspondingly into stationary （stable） and non-stationary. On the basis of a calculation of the cement stone componem removal along with the ideas of the process dynamics the pressure from filtration developmem forecast has been made and their danger level has been estimated. The developed conception is of rather a general character and can be used when analyzing the state of concrete dams of the Angara cascade and other similar cases.展开更多
文摘Pitting and stress corrosion cracking(SCC) studies on the 316 N stainless steel(SS) weldments in aswelded(AW) and thermally aged(solution annealing(SA), 550C/4 h and 750C/1 h) conditions were carried out in acidic and acidic chloride media. Pitting corrosion and SCC resistance was the highest for SA weldment, which was attributed to homogenization of microstructural and microchemical heterogeneities during solution annealing. SA specimen showed the most stable passive film as compared to AW weldment because of higher amount of delta-ferrite in AW weld metal, which resulted in an increased heterogeneity and inferior SCC resistance in AW. Stability of passive film was found to be adversely affected due to heat treatments(at 550C/4 h and 750C/1 h) because of the precipitation of carbide and sigma phases.
文摘Capability of a novel severe plastic deformation(SPD)method of hydrostatic cyclic extrusion compression(HCEC)for processing of hcp metallic rods with high length to diameter ratios was investigated.The process was conducted in two consecutive cycles on the AZ91 magnesium alloy,and microstructural evolution,mechanical properties and corrosion behavior were investigated.The results showed that the HCEC process was successively capable of producing ultrafine-grained long magnesium rods.Its ability in improving strength and ductility simultaneously was also shown.The ultimate tensile strength and elongation to failure of the sample after the second cycle of the process were improved to be 2.46 and 3.8 times those of the as-cast specimen,respectively.Distribution of the microhardness after the second cycle was uniform and its average value was increased by 116%.The potentials derived from the polarization curves were high and the currents were much low for the processed samples.Also,the diameter of the capacitive arcs derived from the Nyquist curves was large in the HCEC processed samples.The finite element analysis indicated the independency of HCEC load from the length in comparison to the conventional CEC.HCEC is a unique SPD method,which can produce long ultrafine-grained rods with a combination of superior mechanical and corrosion properties.
基金the financial supports from the National Natural Science Foundation of China(No.51975330)Science Fund for Distinguished Young Scholars of Shandong Province,China(No.JQ201810)the Key Research and Development Program of Shandong Province,China(No.2019JZZY010360).
文摘The effects of single-stage solution treatment(SST),enhanced solution treatment(EST),high-temperature pre-precipitation(HTPP)and multi-stage solution treatment(MST)on the microstructure,mechanical properties and corrosion resistance of the as-extruded 7055 aluminium alloy(AA7055)helical profile were investigated using differential scanning calorimetry(DSC),optical microscopy(OM),scanning electron microscopy(SEM),electron back-scattered diffraction(EBSD)and transmission electron microscopy(TEM).It was observed that EST and MST could promote the dissolution of the second-phase particles compared with the traditional SST,and the intergranular phases were distinctly discontinuously distributed after HTPP and MST.There was obvious difference in the main texture type and texture strength for the alloy after different solid solution treatments.HTPP could improve the corrosion resistance of the alloy by regulating the intergranular phases,but the mechanical properties were severely weakened.While the good corrosion resistance of the alloy could be obtained by MST without obvious strength loss.As a result,the MST is an ideal solid solution treatment scheme for AA7055.
文摘During the whole operation life of Bratsk and Ust-Ilimsk hydroelectric plants, chemical analysis of water filtering through the pressure front of the concrete dams was under systematic monitoring by sampling in places of concemrated outcome in the inspection galleries of a dam. Long-term cumulative observations made up a basis for study of the indicated dams concrete corrosion caused by the Angara water in the process of its filtration through the cracks formed in the period of the dam erection, through construction joims and other defects. Mathematical-statistical analysis allowed the classification the processes of corrosion from the point of view of their time dynamics and divided them correspondingly into stationary （stable） and non-stationary. On the basis of a calculation of the cement stone componem removal along with the ideas of the process dynamics the pressure from filtration developmem forecast has been made and their danger level has been estimated. The developed conception is of rather a general character and can be used when analyzing the state of concrete dams of the Angara cascade and other similar cases.
