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电子天平在现场的使用及定量包装商品净含量的不确定度评定
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作者 杜红 卢文利 刘明江 《内蒙古科技与经济》 2012年第17期87-87,89,共2页
介绍了电子天平在现场检验定量包装商品时的注意事项,以及以质量标注的定量包装商品净含量计量检验时不同方法的不确定度的评定与说明。
关键词 电子天平 注意事项 定量包装计量检验不确定评定
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基于β-容度容忍区间的血塞通注射液近红外定量分析不确定度评估 被引量:8
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作者 徐冰 薛忠 +3 位作者 罗赣 李建宇 史新元 乔延江 《中草药》 CAS CSCD 北大核心 2015年第6期832-839,共8页
目的建立基于β-容度容忍区间(β-CTI)的血塞通注射液近红外(NIR)定量分析不确定度评估方法。方法采用"I×J×K"型析因实验设计法获取NIR分析校正和验证实验数据,通过PLS算法建立NIR定量模型,通过β-CTI估计NIR定量... 目的建立基于β-容度容忍区间(β-CTI)的血塞通注射液近红外(NIR)定量分析不确定度评估方法。方法采用"I×J×K"型析因实验设计法获取NIR分析校正和验证实验数据,通过PLS算法建立NIR定量模型,通过β-CTI估计NIR定量分析不确定度,并与常规β-期望容忍区间(β-ETI)进行比较。采用ln U=a+b ln Y模型对相对扩展不确定度(U)与相应质量浓度(Y)之间的关系进行拟合,设置不确定度可接受限(λ)=20%,并绘制不确定度决策曲线。结果在考察的7个质量浓度水平中,除1.485 mg/m L外,由β-ETI估计的不确定度均低于由β-CTI估计的不确定度。由β-ETI和β-CTI确定的临界可接受不确定度质量浓度分别为4.867、5.686 mg/m L。结论β-CTI可充分估计NIR定量不确定度,可用于NIR定量结果准确性和可靠性评价。 展开更多
关键词 近红外 定量不确定度 β-容容忍区间 β-期望容忍区间 血塞通注射液 三七总皂苷
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Uncertainty Calculation of Roundness Assessment by Automatic Differentiation in Coordinate Metrology
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作者 林家春 Michael Krystek 石照耀 《Journal of Measurement Science and Instrumentation》 CAS 2010年第3期224-227,共4页
Reomtly, Coordinate bieasuring Machines (CMMs) are widely used to measure roundness errors. Roundness is calculated from a large number of points collected from the profiles of the parts. According to the Guide to t... Reomtly, Coordinate bieasuring Machines (CMMs) are widely used to measure roundness errors. Roundness is calculated from a large number of points collected from the profiles of the parts. According to the Guide to the Expression of Uncertainty in Measta- meat (GUM), all measurement results must have a stated uncertainty associated the titan. However, no CMMs give the uncertainty value of the roundness, because no suitable measrement uncertainty calculation procedure exists. In the case of roundness raeasurement in coordinate metrology, this paper suggests the algorithms for the calculation of the measurement uncertainty of the roudness deviation based on the two mainly used association criteria, LSC and MZC. The calculation of the sensitivity coefficients for the uncertainty calculatiion can be done by autnatic differentiation, in order to avoid introducing additional emars by the traditional difference quotient approxima- tions. The proposed methods are exact and need input data only as the nrasured coordinates of the data points and their associated un- certainties. 展开更多
关键词 raeasurement uncertainty ROUNDNESS automatic diferentiation
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Clearance Effects in Parallel Manipulators: Position Error Discontinuities and Inertial Effects Influence 被引量:1
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作者 Oscar Altuzarra Jokin Aginaga +1 位作者 Charles Pinto Xabier Iriarte 《Journal of Mechanics Engineering and Automation》 2012年第1期41-51,共11页
Clearances at joints cause an uncertainty in the actual posture of the end-effector of any mechanism. This uncertainty relays on the clearance dimension and the way these clearances are taken up by the mechanism under... Clearances at joints cause an uncertainty in the actual posture of the end-effector of any mechanism. This uncertainty relays on the clearance dimension and the way these clearances are taken up by the mechanism under the load and the inertial effects at every instant. As a matter of fact, the actual measure of the pose error is often replaced by an uncertainty measure. However, a side effect of the existence of clearances is that they can cause sudden changes in the posture of the mechanism as a motion is performed. Such discontinuities in the position produce task defects and impacts. In this work a tool to determine the pose error due to clearances is presented together with a discontinuity analysis. In addition, effects of mass distribution and inertial effects on such discontinuities are expounded, taking a 3-PRS robot as example. 展开更多
关键词 Parallel manipulator CLEARANCE position error discontinuity.
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Some Peculiarities of the Preprocessing of Spectral Data and Images
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作者 Valentin Atanassov Georgi Jelev Lubomira Kraleva 《Journal of Shipping and Ocean Engineering》 2013年第1期55-60,共6页
Remotely sensed spectral data and images are acquired under significant additional effects accompanying their major formation process, which greatly determine measurement accuracy. In order to be used in subsequent qu... Remotely sensed spectral data and images are acquired under significant additional effects accompanying their major formation process, which greatly determine measurement accuracy. In order to be used in subsequent quantitative analysis and assessment, this data should be subject to preliminary processing aiming to improve its accuracy and credibility. The paper considers some major problems related with preliminary processing of remotely sensed spectral data and images. The major factors are analyzed, which affect the occurrence of data noise or uncertainties and the methods for reduction or removal thereof. Assessment is made of the extent to which available equipment and technologies may help reduce measurement errors. 展开更多
关键词 SPECTROMETRY spectral data and images preliminary processing.
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Uncertainty Estimation for the Determination of Trace Heavy Metals in Human Hair by Flame and Electrothermal Atomic Absorption Spectrometry
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作者 Fariba Tadayon Mohammad Saber-Tehrani Azam Ghorbani 《Journal of Chemistry and Chemical Engineering》 2010年第8期26-34,共9页
Trace element analysis on hair samples has been widely used to assess wildlife and human exposure to different contaminants present in the environment or at the workplace. Pollutants due to the presence of toxic metal... Trace element analysis on hair samples has been widely used to assess wildlife and human exposure to different contaminants present in the environment or at the workplace. Pollutants due to the presence of toxic metals in environment not only enter the body by breading, water, and foodstuff accumulates in hair, but they could be adsorbed directly on the hair from environment. In order to remove adsorbed elements and thus determine the internally bound elements correctly, hair sample must be washed. In the present work, we propose uncertainty estimation for the analytical results that are obtained from determination of cadmium, lead, copper, iron, manganese and nickel in human hair by flame and electrothermal atomic absorption spectrometry (FAAS and ETAAS). To estimate the uncertainty of analytical result obtained, two types of bias are calculated in the assessment of trueness: a proportional bias and a constant bias. Nested design was applied for calculating proportional bias and Youden method to calculate the constant bias. The results we obtained for proportional bias are calculated from spiked samples. In this case, the concentration found is plotted against the concentration added and the slop of standard addition curve is an estimate of the method recovery. Estimated method of average recovery in human hair is: (1.019 ±0.026), (0.918 ±0.014), (1.073±0.016), (1.0597± 0.017), (1.073± 0.020) and (0.934± 0.117) for Cd, Pb, Mn, Ni, Fe and Cu respectively. 展开更多
关键词 UNCERTAINTY hair analysis trace elements atomic absorption spectrometry.
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Evaluation of measurement uncertainty based on grey system theory for small samples from an unknown distribution 被引量:18
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作者 HAN LianFu TANG WenYan +2 位作者 LIU YongMeng WANG Jun FU ChangFeng 《Science China(Technological Sciences)》 SCIE EI CAS 2013年第6期1517-1524,共8页
To evaluate measurement uncertainty for small sample size and measurement data from an unknown distribution, we propose a grey evaluation method of measurement uncertainty based on the grey relation coefficient. The u... To evaluate measurement uncertainty for small sample size and measurement data from an unknown distribution, we propose a grey evaluation method of measurement uncertainty based on the grey relation coefficient. The uncertainty of measurement is analyzed using grey system theory, and the defects of the grey evaluation model of measurement uncertainty (GEMU) are studied. We then establish an improved grey evaluation model of measurement uncertainty (IGEMU). Simulations show that the precision of IGEMU is greater than that of GEMU, and that sample size has only a small effect on the precision of IGEVU. In particular, IGEMU is applied to evaluating measurement uncertainty for small sample size and measurement data from an unknown distribution. The measurement uncertainty of total profile deviation, which is measured by the CNC gear measuring center, can be evaluated by a combination of IGEMU and the Monte Carlo method. 展开更多
关键词 grey system theory grey relational coefficient measurement uncertainty tooth profile gear measuring center
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