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尿样浓度对尿碘含量的影响 被引量:10
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作者 阎玉芹 陈祖培 《中国地方病学杂志》 CAS CSCD 1997年第4期239-241,共3页
尿样浓度对尿碘含量的影响阎玉芹陈祖培在进行尿碘测定方法标准化的研制过程中,我们严格遵照了国家标准《研制生物样品监测检验方法指南》[1]的要求。《指南》在“样品预处理”一项中明文规定,尿样的浓度按比重进行校正,尿样的标... 尿样浓度对尿碘含量的影响阎玉芹陈祖培在进行尿碘测定方法标准化的研制过程中,我们严格遵照了国家标准《研制生物样品监测检验方法指南》[1]的要求。《指南》在“样品预处理”一项中明文规定,尿样的浓度按比重进行校正,尿样的标准比重为1.020,比重小于1.0... 展开更多
关键词 尿 尿碘 尿样浓度 测定
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UPLC-MS/MS测定大鼠尿样中26-OH-PD浓度的不确定度评定 被引量:1
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作者 林美妤 张楠淇 +3 位作者 王翠竹 朱海林 刘金平 李平亚 《药物评价研究》 CAS 2018年第4期582-588,共7页
目的评定超高液相色谱-串联质谱法(UPLC-MS/MS)测定大鼠尿样中26-OH-PD浓度的不确定度。方法分析UPLC-MS/MS法测定大鼠尿样中26-OH-PD浓度的不确定度来源,根据各分量计算出合成不确定度并进行了扩展。结果大鼠尿样中低浓度(6.16 ng/m L... 目的评定超高液相色谱-串联质谱法(UPLC-MS/MS)测定大鼠尿样中26-OH-PD浓度的不确定度。方法分析UPLC-MS/MS法测定大鼠尿样中26-OH-PD浓度的不确定度来源,根据各分量计算出合成不确定度并进行了扩展。结果大鼠尿样中低浓度(6.16 ng/m L)、中浓度(97.94 ng/m L)和高浓度(398.02ng/m L)26-OH-PD的扩展不确定度分别为1.44、6.97、22.05 ng/m L(P=95%,k=2)。结论 UPLC-MS/MS法测定大鼠尿样中26-OH-PD低浓度样品的不确定度主要分别由线性拟合引入,中、高浓度样品的不确定度主要由仪器允差引入。该法适用于评定UPLC-MS/MS法测定尿样中26-OH-PD的不确定度研究,能为复杂生物样品分析过程的不确定度评定提供一定参考。 展开更多
关键词 不确定度 26-OH-PD UPLC-MS/MS 尿样浓度
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The Relationships Between Milk Constituents and Various Milk Properties in Anatolian Buffaloes
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作者 OEzel. Sekerden Yahya Kemal Avsar 《Journal of Life Sciences》 2012年第8期908-912,共5页
The objectives of this study were to investigate the relationships among milk composition, renneting time, urea concentration, acidity, density and pH of Anatolian Buffaloes' milk. As a total of 115 individual milk s... The objectives of this study were to investigate the relationships among milk composition, renneting time, urea concentration, acidity, density and pH of Anatolian Buffaloes' milk. As a total of 115 individual milk samples from 53 Anatolian buffalo cows that calved in 2004 and 2005 on days of their lactations 30 ± 15, 60 ± 15, 90 ±15, 120 ± 15, 150 ± 15, 180± 15, 210 ±15, 240 ± 15 and 270 ± 15 in 8 units of lhkpmar village were collected in morning milkings in June, September, December and March. Samples were analysed for total dry matter (TDM), fat, protein, ash, density, pH, acidity, renneting time and urea content. Data were classified according to the following environmental factors: lactation stages: (30 ± 15, 60 i 15, 90 ±15 days): 2 (120±15, 150 ± 15, 180 ± 15 days): 3 (210 ± 15, 240 ± 15, 270± 15 days); calving year: 1 (2004), 2 (2005); calving season: 1 (January-May), 2 (September and October); month of samples collection: 1 (June), 2 (September), 3 (December), 4 (March); lactation order: 1 and 2:1, 3 and 4:2, 5 and 6:3. Means and correlation coefficients for the characteristics investigated were calculated. There were negative significant correlations between daily milk yield with TDM, fat and protein percentages, and between pH and all of the milk constituents. Density reduces as TDM, fat and protein contents increase. Relationships between density and coagulation time with milk yield and pH were not significant. Relationships between milk urea concentration with none of milk constituents, milk yield, density, pH and titratable acidity were not significant statistically. It was concluded that genetic selection has to be directed towards increasing fat, protein and total not fat dry matter yields. Under selection programs in which milk yield is taken into consideration, fat and protein yields also increase, but fat and protein concentrations decrease. 展开更多
关键词 Anatolian buffalo MILK COAGULATION renneting UREA pH.
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