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热分析实验教学改革与实践 被引量:1
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作者 李明玲 李宏林 高晓宝 《巢湖学院学报》 2017年第3期137-140,共4页
热分析实验是《材料现代分析方法》课程的重要内容,热分析技术是材料类专业学生必须了解和掌握的技术之一。针对目前热分析实验教学过程中存在的问题和不足,围绕教学方法与手段、教学内容与教学设计等作了改革研究并实践,锻炼了学生的... 热分析实验是《材料现代分析方法》课程的重要内容,热分析技术是材料类专业学生必须了解和掌握的技术之一。针对目前热分析实验教学过程中存在的问题和不足,围绕教学方法与手段、教学内容与教学设计等作了改革研究并实践,锻炼了学生的动手操作能力,培养了学生创新能力和科研素养。 展开更多
关键词 热分析实验 综合分析 教学方法 教学设计
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浅谈热分析实验管理与教学的创新改革 被引量:1
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作者 耿洁婷 华静 《教育教学论坛》 2018年第43期272-273,共2页
本文结合实际,对热分析实验进行了管理和教学的改革,通过培训机制、预约机制的改革和教学方法的创新,丰富并活化了热分析实验管理和教学,以此激发学生的学习兴趣,培养学生的自主学习能力,提高学生的实验技能。
关键词 热分析实验 实验教学改革 实验管理改革
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“双碳”背景下能动类专业实验教学改革与实践——以热重分析实验为例 被引量:2
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作者 张润霞 张瑜 +2 位作者 李娜 周屈兰 顾兆林 《实验室研究与探索》 CAS 北大核心 2023年第12期149-153,213,共6页
在“双碳”战略目标下,能源与动力工程专业应为能源的高效低碳利用,产业的转型升级培养专业素质扎实、创新意识突出、学科交叉能力强的“双碳”人才。能动学院国家级实验教学示范中心面向本科生开设了固体燃料的热重分析实验。通过创新... 在“双碳”战略目标下,能源与动力工程专业应为能源的高效低碳利用,产业的转型升级培养专业素质扎实、创新意识突出、学科交叉能力强的“双碳”人才。能动学院国家级实验教学示范中心面向本科生开设了固体燃料的热重分析实验。通过创新实验内容、实施模式和考核评价方法,加深了学生对固体燃料理化性质和燃烧过程的认知,强化了数据分析能力和科学研究能力,提升了该实验的综合性、挑战性和高阶性。通过建立智能化教学管理平台,高效完成了教学实验,充分发挥了实验平台培养学生实践能力的作用。经过两届学生的教学实践,该实验获得了良好的教学效果和评价。 展开更多
关键词 分析实验 实验创新 教学设计 人才培养
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基于虚拟仿真技术的热分析实验教学探索与实践 被引量:15
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作者 申文竹 安维岳 +2 位作者 刘丽 王平 黄志宇 《化学教育(中英文)》 CAS 北大核心 2020年第22期84-88,共5页
针对热分析实验教学,设计和开发了热分析仪虚拟仿真实训系统,提出了一种新的基于虚拟仿真技术的仪器分析测试类实验课教学模式,并将其应用于实际的实验教学中。对随堂实验教学质量进行了调查,结果表明此种实验教学模式很大程度上提升了... 针对热分析实验教学,设计和开发了热分析仪虚拟仿真实训系统,提出了一种新的基于虚拟仿真技术的仪器分析测试类实验课教学模式,并将其应用于实际的实验教学中。对随堂实验教学质量进行了调查,结果表明此种实验教学模式很大程度上提升了学生自主学习的兴趣,提高了学生的综合实践能力。 展开更多
关键词 虚拟仿真实验 实验教学 大型仪器设备 热分析实验教学
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科技论文有关热分析实验中物理量的规范化表示 被引量:6
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作者 左小青 林琳 《中国科技期刊研究》 CSSCI 北大核心 2007年第3期517-519,共3页
在科技编辑工作中,在化学和材料科学领域,经常碰到有关热分析实验中使用热分析曲线的文章,发现同一种曲线坐标有许多不同的表示方法,存在明显的错误和不规范。本文针对这些问题,查找了热分析方面专业书籍,分别对热分析中的差示扫描量热... 在科技编辑工作中,在化学和材料科学领域,经常碰到有关热分析实验中使用热分析曲线的文章,发现同一种曲线坐标有许多不同的表示方法,存在明显的错误和不规范。本文针对这些问题,查找了热分析方面专业书籍,分别对热分析中的差示扫描量热法(DSC)、差热分析法(DTA)、热重分析法(TG)和微商热重法(DTG)4种方法的曲线坐标的表示进行了对比分析,给出了规范的表示方法,为科技编辑提供参考。 展开更多
关键词 热分析实验 物理量 规范化 单位
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稠油高压火驱氧化特性实验研究 被引量:4
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作者 赵健 张娜 +2 位作者 蒋海岩 赵志龙 焦平格 《油气地质与采收率》 CAS CSCD 北大核心 2023年第3期145-151,共7页
稠油氧化特性研究是火驱提高采收率矿场设计的依据和基础,但截至目前,有关压力对稠油高压火驱的研究相对较少。为了明确压力对稠油火驱氧化特性的影响,并有效减少高压火驱的不利影响,以鲁克沁稠油为例,基于热重实验和差示扫描量热实验,... 稠油氧化特性研究是火驱提高采收率矿场设计的依据和基础,但截至目前,有关压力对稠油高压火驱的研究相对较少。为了明确压力对稠油火驱氧化特性的影响,并有效减少高压火驱的不利影响,以鲁克沁稠油为例,基于热重实验和差示扫描量热实验,研究不同压力下的稠油氧化热失重以及放热等变化特性,首先计算不同压力下的动力学参数,得出各氧化阶段的活化能、反应焓;其次,通过燃烧管实验,评价了不同压力下的火驱燃烧效果及稳定性。研究结果表明:压力升高加快了稠油氧化反应速率,增加了放热量,复杂体系的氧化路径有所改变,反应动力学表征参数需进行高压修正;并且压力升高使火线推进速率加快,燃烧前缘温度较常压火驱升高300℃以上,燃烧稳定性变差;10%减氧高压火驱燃烧稳定,有效抑制高压反应速度过快导致的燃烧不稳定性。 展开更多
关键词 深层稠油 高压火驱 氧化特性 高压动力学表征 热分析实验 高压燃烧管实验 减氧火驱
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AP粒度和包覆层对硼燃烧的影响 被引量:15
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作者 王英红 李葆萱 +1 位作者 胡松起 肖秀友 《固体火箭技术》 EI CAS CSCD 北大核心 2004年第1期50-52,68,共4页
通过对AP和硼及其混合物进行热分析实验,研究了硼在AP分解过程中参与反应的程度;用氧弹式量热计测试含硼富燃料推进剂的爆热,分析硼在推进剂燃烧过程中的放热。结果表明,对各组分含量相同的含硼富燃料推进剂用AP包覆硼粒子和提高超细AP... 通过对AP和硼及其混合物进行热分析实验,研究了硼在AP分解过程中参与反应的程度;用氧弹式量热计测试含硼富燃料推进剂的爆热,分析硼在推进剂燃烧过程中的放热。结果表明,对各组分含量相同的含硼富燃料推进剂用AP包覆硼粒子和提高超细AP含量可促使硼在AP分解过程中参与反应,使AP/B(1∶1)热分解的放热量增加,提高推进剂的爆热,有利于推进剂中硼的燃烧。 展开更多
关键词 AP粒度 包覆层 燃烧 热分析实验 燃料推进剂 固体推进剂
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煤升温氧化动力学阶段性规律 被引量:11
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作者 张辛亥 白亚娥 +1 位作者 李亚清 马腾 《西安科技大学学报》 CAS 北大核心 2017年第4期474-478,共5页
为了研究煤的自燃特性,选取石圪台煤矿22203采煤工作面煤样为研究对象,采用热分析技术,对煤氧化升温过程中质量及动力学参数变化规律进行了探讨。结果表明:煤的失重呈阶段性变化规律,可分为低温失重、吸氧增重、缓慢化学反应和燃烧阶段... 为了研究煤的自燃特性,选取石圪台煤矿22203采煤工作面煤样为研究对象,采用热分析技术,对煤氧化升温过程中质量及动力学参数变化规律进行了探讨。结果表明:煤的失重呈阶段性变化规律,可分为低温失重、吸氧增重、缓慢化学反应和燃烧阶段;通过采用改进的KAS法计算煤升温氧化动力学参数,可知在温度达到燃点前,随着温度升高反应活化能增加,说明不断有难燃结构参与到反应。超过燃点温度,在燃烧阶段初期,活化能基本保持不变,而指前因子出现峰值,表明有大量活性结构被激活,准备参与到燃烧反应中。在燃烧阶段中后期,活化能随温度的增加逐步减小,表明该阶段有芳香环的破坏形成更易于反应的活性结构;动力学参数的补偿效应存在显著分段性,说明在煤氧反应过程中前后反应不同,其整体反应存在不止一个反应机理。研究结果对防治煤自燃提供理论依据。 展开更多
关键词 煤自燃 热分析实验 分段性 活化能 补偿效应
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污泥石灰干化作用机理及应用研究 被引量:6
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作者 曹秀芹 杨华 +3 位作者 甘一萍 胡俊 张辉 梁远 《水工业市场》 2011年第8期44-48,共5页
污泥石灰干化技术具有脱水效果好、投资少、干化后污泥可资源化利用等优点。但污泥成分复杂,污泥石灰干化过程中伴随有大量复杂的化学反应。本研究通过热重实验分析着重探讨了污泥石灰干化过程有机物的转化机理。此外,通过小试和生产试... 污泥石灰干化技术具有脱水效果好、投资少、干化后污泥可资源化利用等优点。但污泥成分复杂,污泥石灰干化过程中伴随有大量复杂的化学反应。本研究通过热重实验分析着重探讨了污泥石灰干化过程有机物的转化机理。此外,通过小试和生产试验研究表明,石灰干化后污泥含水率由80%可降为40%左右;有机物含量由75%可降为14%左右。干化后污泥有用作水泥替代原料、铺路材料和垃圾填埋覆盖土等多种形式的资源化利用途径。 展开更多
关键词 污泥 石灰干化 实验分析 机理 应用
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Theoretical Analysis and Experimental Evidence of Non-Fourier Heat Conduction Behavior 被引量:2
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作者 蒋方明 刘登瀛 蔡睿贤 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2001年第4期359-366,共8页
This paper consists of two parts. (1) For a hollow sphere with sudden temperature changes on its inner and outer surfaces, the hyperbolic heat conduction equation is employed to describe this extreme thermal case and... This paper consists of two parts. (1) For a hollow sphere with sudden temperature changes on its inner and outer surfaces, the hyperbolic heat conduction equation is employed to describe this extreme thermal case and an analytical expression of its temperature distribution is obtained. According to the expression, the non-Fourier heat conduction behavior that will appear in the hollow sphere is studied and some qualitative conditions that will result in distinct non-Fourier behavior in the medium is ultimately attained. (2) A novel experiment to observe non-Fourier heat conduction behavior in porous material (mainly ordinary duplicating paper) heated by a microsecond laser pulse is presented. The conditions for observing distinct non-Fourier heat conduction behavior in the experimental sample agree well with the theoretical results qualitatively. 展开更多
关键词 non-Fourier heat conduction hyperbolic heat conduction thermal wave
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Simulation and experiment analysis on thermal deformation of tool system in single-point diamond turning of aluminum alloy 被引量:4
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作者 ZHANG Yuan-jing DONG Guo-jun ZHOU Ming 《Journal of Central South University》 SCIE EI CAS CSCD 2016年第9期2223-2229,共7页
The aim of this work is to simulate thermal deformation of tool system and investigate the influence of cutting parameters on it in single-point diamond turning(SPDT) of aluminum alloy. The experiments with various cu... The aim of this work is to simulate thermal deformation of tool system and investigate the influence of cutting parameters on it in single-point diamond turning(SPDT) of aluminum alloy. The experiments with various cutting parameters were conducted. Cutting temperature was measured by FLIR A315 infrared thermal imager. Tool wear was measured by scanning electron microscope(SEM). The numerical model of heat flux considering tool wear generated in cutting zone was established. Then two-step finite element method(FEM) simulations matching the experimental conditions were carried out to simulate the thermal deformation. In addition, the tests of deformation of tool system were performed to verify previous simulation results. And then the influence of cutting parameters on thermal deformation was investigated. The results show that the temperature and thermal deformation from simulations agree well with the results from experiments in the same conditions. The maximum thermal deformation of tool reaches to 7 μm. The average flank wear width and cutting speed are the dominant factors affecting thermal deformation, and the effective way to decrease the thermal deformation of tool is to control the tool wear and the cutting speed. 展开更多
关键词 ultra-precision cutting tool wear DIAMOND thermal deformation form accuracy
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Thermo-mechanical and Experimental Analysis of Double Pass Line Heating
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作者 Pankaj Biswas N. R. Mandal +1 位作者 O. P. Sha M. M. Mahapatra 《Journal of Marine Science and Application》 2011年第2期190-198,共9页
The present investigation deals with process analysis of oxy-acetylene flame assisted double pass line heating for varying plate thickness, oxy-acetylene flame as the heat source for multi pass line heating to achieve... The present investigation deals with process analysis of oxy-acetylene flame assisted double pass line heating for varying plate thickness, oxy-acetylene flame as the heat source for multi pass line heating to achieve 3-D bending of plates with varying thicknesses was studied. The oxy-acetylene flame was modeled as the moving heat source in the FEM analysis. The transient thermal histories were predicted taking into account the temperature dependent thermo-mechanical properties. A comparative study between single pass and double pass line heating residual deformation was also carried out. The temperature distribution and residual detbrmations predicted by the numerical model developed in the present work compared fairly well with those of the experimental ones. 展开更多
关键词 double pass thermal history residual defolxnations 3-D FEM transient analysis elasto-plastic analysis oxy-acetylene gas torch
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Comparison of desulfurization kinetics of copper oxide sorbent 被引量:1
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作者 郁青春 邓勇 +4 位作者 王飞 冯跃斌 杨斌 徐宝强 刘大春 《Journal of Central South University》 SCIE EI CAS CSCD 2015年第8期2902-2908,共7页
Desulfurization experiments of CuO, γ-Al2O3 and CuO/γ-Al2O3 were made in simulated flue gas by means of thermogravimetric analysis. It is found that reaction activities of CuO supported on γ-Al2O3 could be highly i... Desulfurization experiments of CuO, γ-Al2O3 and CuO/γ-Al2O3 were made in simulated flue gas by means of thermogravimetric analysis. It is found that reaction activities of CuO supported on γ-Al2O3 could be highly improved. Desulfurization kinetics of CuO/γ-Al2O3 was studied in the temperature range of 250 °C-400 °C and SO2 concentration of 0.1%-0.9%. The experimental data were tested and compared with kinetics models of volume reaction model(VRM), grain size model(GSM), random pore model(RPM) and pore-blocking model(PBM). Correlation analysis shows that VRM and RPM models do not fit experimental data well. GSM contradicts with the changes in the physical and chemical properties of Cu O/γ-Al2O3 as the desulfurization proceeds. It is found that PBM is consistent with the change of pore structure of CuO/γ-Al2O3 sorbent during desulfurization process and predicts the conversion-time curves of the sorbent well. Meanwhile, kinetics parameters are obtained and discussed. 展开更多
关键词 copper oxide DESULFURIZATION KINETICS Γ-AL2O3
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Cooling of Superheated Refrigerants Flowing inside Tubes Filled with Porous Media: Study of Heat Transfer and Pressure Drop, Carbon Dioxide Case Study 被引量:1
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作者 M. Hammad A.S. Alshqirate M. Tarawneh 《Journal of Energy and Power Engineering》 2011年第9期802-810,共9页
In this work an experimental study combined with an analytical investigation for cooling superheated Carbon Dioxide (CO2) gas were carried out. This work is intended to be part of the super critical Gustav Lorentzen... In this work an experimental study combined with an analytical investigation for cooling superheated Carbon Dioxide (CO2) gas were carried out. This work is intended to be part of the super critical Gustav Lorentzen refrigeration cycle of CO2. Experimental and analytical works concentrated on heat transfer and pressure drop for single phase flow during gas cooling inside tubes filled with porous media. Analytical empirical correlations were formulated for the coefficient of convectional heat transfer and for the pressure drop. A comparison between experimental results and that obtained by developed correlations were carried out, and a comparison between these results and literature published ones were carried out too. The results of this research showed that for cooling process the proposed correlations were proved to be acceptably accurate for pressure drop with difference from experimental results of 2%, while for convective heat transfer the difference from experimental results reached about 3%. More than 90% agreement with literature results was obtained. This work can enhance the calculations of heat flux and pressure drop of gases flow inside porous media filled tubes, and can help in the design procedure of heat exchangers and cooling processes. 展开更多
关键词 COOLING porous media convection heat transfer pressure drop R744.
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Heat transfer analysis and experimental verification of cast heat exchanger 被引量:1
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作者 俞洁 董蕾 +1 位作者 张欢 由世俊 《Journal of Central South University》 SCIE EI CAS 2012年第6期1610-1614,共5页
From the viewpoints of environmental conservation and energy efficiency,seawater-source heat pump system(SWHP) to provide district cooling and heating is applied in coastal areas.Based on the system,a heat transfer mo... From the viewpoints of environmental conservation and energy efficiency,seawater-source heat pump system(SWHP) to provide district cooling and heating is applied in coastal areas.Based on the system,a heat transfer model was established for cast heat exchanger(CHE) adopted by SWHP systems.The CHE consists of pipes immersed in the seawater and used for transferring heat between the seawater and the heat exchanger pipes of SWHP system.An experimental study was carried out to test the validity of the model.A program was developed in VB language and the effects of inlet temperature,flow rate of the secondary refrigerant and length of CHE on the results were investigated.The results of the numerical simulation are in consistence with the experiments in both winter and summer conditions.As a result,application of SWHP systems with CHE in coastal areas in China is feasible due to the favorable geographical conditions and environment. 展开更多
关键词 seawater-source heat pump cast heat exchanger mathematical model experimental verification numerical simulation
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Thermal Analyses of Combined Utilization Process of Seawater by Solar Chimney
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作者 王一平 方振雷 朱丽 《Transactions of Tianjin University》 EI CAS 2009年第6期393-399,共7页
It is promising to simultaneously develop multiple products through the combined utilization of seawater by solar chimney technology. A small scale experimental system was set up. The collector temperature, the seawat... It is promising to simultaneously develop multiple products through the combined utilization of seawater by solar chimney technology. A small scale experimental system was set up. The collector temperature, the seawater temperature, and the temperature and humidity of the airflow under the collector were measured. Thermal network analysis of the system was carried out. The results show that the airflow is nearly saturated at the entrance of the chimney, and the mean dry-bulb and wet-bulb temperatures of the airflow have increased by 8.4 ℃ and 9.6 ℃, respectively. The radiation heat transfer between the collector and the sky is the biggest heat loss in the system, which is up to 29.1% on average of the solar energy. However, the water evaporation heat is about 23.6% on average of the solar energy. To reduce the heat loss and enhance the water evaporation, it is necessary to reduce the emissivity and thermal conductivity of the collector and increase the evaporation areas. 展开更多
关键词 solar chimney combined utilization of seawater thermal network enhanced evaporation
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Calculation of phase transformation latent heat based on cooling curves in end-quench test and its application in nickel-based superalloy
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作者 Tian-yang ZHAO Pei FU +2 位作者 Zhuo CHEN Ping ZHOU Chao LI 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2022年第5期1718-1727,共10页
To obtain the phase transformation latent heat corresponding to different cooling rates with low test workload and cost,the Newton thermal analysis method and the improved Newtonian thermal analysis method were discus... To obtain the phase transformation latent heat corresponding to different cooling rates with low test workload and cost,the Newton thermal analysis method and the improved Newtonian thermal analysis method were discussed based on the cooling curve obtained in the end-quench test.The validity of two methods was given by the latent heat calculation of 45^(#) steel.The results show that the relative error of latent heat is 5.20%through the improved Newtonian thermal analysis method,which is more accurate than the Newtonian thermal analysis method.Furthermore,the latent heat release of phase transformation of the self-designed CSU-A1 powder metallurgy nickel-based superalloy increases from 4.3 to 12.29 J/g when the cooling rate decreases from 50.15 to 33.40℃/min,because there is more sufficient time for the alloy microstructure to complete the phase transformation process when the cooling rate is smaller. 展开更多
关键词 cooling curve end-quench test Newtonian thermal analysis method phase transformation latent heat nickel-based superalloy
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部分互溶二组元金属系统相图实验的计算机模拟 被引量:6
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作者 鄢红 郭广生 张常群 《计算机与应用化学》 CAS CSCD 北大核心 2001年第5期515-519,共5页
系统相边界的精确测定 ,特别是复杂的金属系统相边界的测定较为困难 ,并要考虑其测定误差。热分析技术是测定金属固 -液系统相图的一种有效方法。铂 -银二组元金属系统就是较复杂的金属系统的一个典型例子。不仅二组分在固相部分互溶 ,... 系统相边界的精确测定 ,特别是复杂的金属系统相边界的测定较为困难 ,并要考虑其测定误差。热分析技术是测定金属固 -液系统相图的一种有效方法。铂 -银二组元金属系统就是较复杂的金属系统的一个典型例子。不仅二组分在固相部分互溶 ,而且在相图中还出现“转熔点”。本文中 ,以铂 -银系统为例 ,介绍了二组元金属系统热分析实验过程的计算机模拟 ,演示了如何从热分析实验得到该系统的相图 ,研制了相应的多媒体辅助教学课件 ,该课件具有真实。 展开更多
关键词 计算机模拟 多媒体辅助教学课件 固液平衡 二组元金属系统 相图 热分析实验 相平衡
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Analysis of Film-Boiling Heat Transfer on a High Temperature Sphere Immersed into Liquid Sodium
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作者 Alix Le Belguet Georges Berthoud Magali Zabiego 《Journal of Energy and Power Engineering》 2014年第4期628-635,共8页
Film-boiling heat transfer is a key phenomenon governing severe accident sequence in a sodium-cooled fast reactor. Experimental the fuel-coolant interaction process which may occur during a and theoretical work on fil... Film-boiling heat transfer is a key phenomenon governing severe accident sequence in a sodium-cooled fast reactor. Experimental the fuel-coolant interaction process which may occur during a and theoretical work on film-boiling heat transfer in sodium has hardly been carried out in the past. An experiment has been conducted in the early seventies to investigate sodium pool boiling. In this experiment, a hot tantalum sphere was immersed into subcooled liquid sodium. Film boiling was obtained for various sets of parameters: sodium subcooling from 4.1 K to 29. 1 K, initial sphere temperature ranging from 1,802.6 K to 2,633.7 K, sphere diameters of 1.27, 1.91 and 2.54 cm and sodium depths of 7.6 cm and 11.4 cm. In the present work, a simplified analysis based on the boundary layer theory is developed to describe pool film-boiling heat transfer on a hot sphere in liquid sodium. Two extreme cases are considered depending on sodium subcooling. In the case of high subcooling, most of the heat lost by the sphere is used to heat the sodium while for low subcooling, it is used to vaporize the liquid at the liquid-vapor interface. It will be shown that the scaling analysis predicts the heat fluxes within the order of magnitude when compared to the available experimental data. Besides, it allows an estimation of the contribution of these fluxes to the liquid heating and vaporization processes. 展开更多
关键词 Film-boiling heat transfer scale analysis SODIUM sphere.
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The Effects of Voltage and Suction Line Heat Exchanger on a Domestic Refrigerator's Performance
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作者 Xerri Stefan Farrugia Mario 《Journal of Energy and Power Engineering》 2016年第10期606-614,共9页
This experimental analysis shows the measured reduction in energy consumption as well as the effects of voltage on cycle temperatures, pressures, flow rates and also compressor speed (revolutions per minute). The do... This experimental analysis shows the measured reduction in energy consumption as well as the effects of voltage on cycle temperatures, pressures, flow rates and also compressor speed (revolutions per minute). The domestic refrigerator used R134a as refrigerant. Two energy consumption procedures were adapted from the JIS and ISO standards. The biggest difference between two standards is that the fridge is not opened in the ISO test while it is opened a number of times in the JIS test. The tests were carried out between 190 V and 250 V in steps of 10 V. The reduction in energy consumption was of 49.78 W-h per day or 6.27% of the total consumption. The experiments also showed that the voltage drop resulted in only a small rpm drop which in turn did not result in a noticeable refrigerant flow-rate change. Consequently the temperatures and pressures were not affected. 展开更多
关键词 REFRIGERATION voltage optimization energy consumption capillary-tube/suction-line heat exchanger.
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