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石墨电极粉铺垫混合熔剂助熔测定窑渣中主要成分
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作者 马文广 郝选科 关祥忠 《山东冶金》 CAS 2024年第1期45-48,共4页
本法尝试采用滤纸包裹试样,置于预先用石墨电极粉铺垫好的刚玉坩埚中,于900~950℃的高温炉中熔融10~20 min,至熔融物透明,盐酸浸取,过滤掉少量石墨粉,将滤液加热蒸发至干。在浓盐酸中加动物胶使硅酸凝聚沉淀,经过滤、洗涤、灼烧、称量,... 本法尝试采用滤纸包裹试样,置于预先用石墨电极粉铺垫好的刚玉坩埚中,于900~950℃的高温炉中熔融10~20 min,至熔融物透明,盐酸浸取,过滤掉少量石墨粉,将滤液加热蒸发至干。在浓盐酸中加动物胶使硅酸凝聚沉淀,经过滤、洗涤、灼烧、称量,计算SiO_(2)的质量分数。所得滤液以氨水沉淀分离,滤液用EDTA标液滴定,计算CaO和MgO的质量分数。氢氧化物沉淀用盐酸溶解,再在氢氧化钠溶液中沉淀分离Al,分取滤液用氟代盐取代EDTA,用铜标液滴定,计算Al_(2)O_(3)的质量分数。 展开更多
关键词 石墨电极粉 高温熔融 刚玉坩埚 窑渣 硅酸凝聚 滴定
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钼兰光度法测定拜尔赤泥中二氧化硅
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作者 王永惠 贺瑞红 关西安 《山西冶金》 CAS 2003年第2期31-32,共2页
通过研究样品制备时的酸度、时间等引起硅酸凝聚的条件以及光度测定条件的重新试验,确立了拜尔赤泥中二氧化硅的钼兰光度法测定条件。试验结果表明:方法相对标准偏差小于0.75%,加标回收率在98%~101%。
关键词 拜尔法 赤泥 氧化铝 二氧化硅 钼兰光度法 测定 硅酸凝聚
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钼蓝光度法测定拜尔赤泥中二氧化硅 被引量:1
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作者 贺晓东 《山西化工》 2006年第5期42-43,58,共3页
通过研究样品制备时的酸度、时间等引起硅酸凝聚的条件以及光度测定条件的重新实验,确立了拜尔赤泥中二氧化硅的钼蓝光度法测定条件。结果表明:此方法相对标准偏差小于0.75%,回收率98%~101%。
关键词 拜尔赤泥 二氧化硅 硅酸凝聚 酸度 钼蓝光度法
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Study on coagulation property of metal-polysilicate coagulants in low turbidity water treatment 被引量:9
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作者 杨海燕 崔福义 +1 位作者 赵庆良 马超 《Journal of Zhejiang University Science》 EI CSCD 2004年第6期721-726,共6页
In order to remove the low turbidity present in surface water, a novel metal-polysilicate coagulant was used to treat the raw water taken from Tanjiang River in Guangdong Province. This study on the effects of Al/Fe ... In order to remove the low turbidity present in surface water, a novel metal-polysilicate coagulant was used to treat the raw water taken from Tanjiang River in Guangdong Province. This study on the effects of Al/Fe molar ratio on the performance of a complex compound formed by polysilicic acid, aluminium and ferric salt (PAFS) showed that PAFS with Al/Fe ratio of 10:3 seemed to have the best coagulation performance in removing turbidity and color. Experimental results showed that under the conditions of polymerization time of 15 d, sedimentation time of 12 min, and pH of 6?8, PAFS with Al/Fe molar ratio of 10:3 had the best coagulation efficiency and lowest residual Al concentration. The turbid- ity decreased from 23.8 NTU to 3.23 NTU and the residual Al concentration was only 0.165 mg/L in the product water. It could be speculated that colloidal impurities and particulate Al were removed by adsorption bridging and electrical neu- tralization of long chain inorganic polymer coagulants. 展开更多
关键词 Potable water treatment Metal-polysilicate coagulant Coagulation property Residual aluminum
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Preparation of New Poly Silicate Iron Coagulants and Their Coagulation Property on Micro-polluted Water 被引量:6
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作者 L.P. Wang X.F. Yan +4 位作者 X. XU A.B. Xu H. Qi Z.D. Zou N.Y. Gao 《Journal of Environmental Science and Engineering》 2011年第1期1-4,共4页
The sodium silicate, ferric chloride, ferrous sulfate, sodium chlorate and other common inorganic materials were used to synthesize two new poly silicate iron coagulants: Polysilicate Ferric Chloride (PFSiC) and Po... The sodium silicate, ferric chloride, ferrous sulfate, sodium chlorate and other common inorganic materials were used to synthesize two new poly silicate iron coagulants: Polysilicate Ferric Chloride (PFSiC) and Polymeric Ferric Silicate Sulfate (PFSiS). Their coagulation effect on micro-polluted water was compared with the poly ferric choride (PFC) saled in the market. The results showed that turbidity, organic matter, total phosphorus, total nitrogen removal rate ofPFSiC, PFSiS coagulant were better than PFC on micro-polluted water treatment at the same dosage. The coagulation effect of PFSiC was the best. The surface morphology of three coagulants was observed by scanning electron microscopy (SEM), and the coagulation mechanism was discussed preliminarily. 展开更多
关键词 Poly silicate iron PREPARATION micro-polluted water coagulation mechanism
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Pilot study on binding of bovine salivary proteins to grit silicates and plant phytoliths
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作者 Marcus MAU Thomas M.KAISER Karl-Heinz SüDEKUM 《Zoological Research》 CAS CSCD 北大核心 2013年第3期I0013-I0018,共6页
Mostly fed with grass in fresh or conserved form, cattle and other livestock have to cope with silicate defence bodies from plants (phytoliths) and environmental silicates (grit), which abrade tooth enamel and cou... Mostly fed with grass in fresh or conserved form, cattle and other livestock have to cope with silicate defence bodies from plants (phytoliths) and environmental silicates (grit), which abrade tooth enamel and could additionally interact with various salivary proteins. To detect potential candidates for silicate-binding proteins, bovine whole saliva was incubated with grass-derived phytoliths and silicates. Interactions of salivary proteins with pulverized bovine dental enamel and dentine were additionally analysed. After intense washing, the powder fractions were loaded onto 1D-polyacrylamide gels, most prominent adhesive protein bands were cut out and proteins were identified by mass spectrometry within three independent replicates. All materials were mainly botmd by bovine odorant-binding protein, bovine salivary protein 30× 10^3 and carbonic anhydrase VI. The phytolith/silicate fraction showed additional stronger interaction with haemoglobin β and lactoperoxidase. Conceivably, the binding of these proteins to the surfaces may contribute to biological processes occurring on them. 展开更多
关键词 Bovine salivary proteins Mass spectrometry PHYTOLITHS SILICATES Tooth enamel
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