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热处理气氛和温度对SnO_2∶Sb超细粉的影响
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作者 田甜 张金朝 宋鹂 《硅酸盐通报》 CAS CSCD 北大核心 2005年第3期42-45,共4页
以SnCl4·5H2O和SbCl3为原料,采用共沉淀法分别制得了纳米级的SnO2∶Sb,Sb2O3和SnO2超细粉,并选取工业用Sb2O3粉末作为参比,运用X射线衍射(XRD)、Leitz多功能显微镜、电阻测试等测试方法对粉末进行了表征,比较系统地研究了热处理气... 以SnCl4·5H2O和SbCl3为原料,采用共沉淀法分别制得了纳米级的SnO2∶Sb,Sb2O3和SnO2超细粉,并选取工业用Sb2O3粉末作为参比,运用X射线衍射(XRD)、Leitz多功能显微镜、电阻测试等测试方法对粉末进行了表征,比较系统地研究了热处理气氛和温度对粉末物相和电阻的影响。 展开更多
关键词 SnO2:Sb超细粉 热处理气氛 温度 结构表征 纯锑氧化物 玻璃
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Preparation of Arsenic Oxide and High Purity Ultrafine Antimony Compounds from Flue Dust Containing Arsenic and Antimony 被引量:3
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作者 段学臣 赵天从 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 1999年第3期278-282,共5页
A new hydrometallurgical process of chlorination-distillation at low temperatures about 100 °C was developed for recovery of valuable metal and environmental protection. This process was used to treat flue dust c... A new hydrometallurgical process of chlorination-distillation at low temperatures about 100 °C was developed for recovery of valuable metal and environmental protection. This process was used to treat flue dust containing arsenic and antimony and satisfactory results were obtained. Over 99% of arsenic and antimony were recovered, and high purity As2O3 and SbCl3 were produced. A metallic alcoholate technique was developed and proved to be of significant to the utilization of antimony resources. Using this technique, a number of antimony oxide powders were prepared, such as high purity and ultrafine Sb2O3, ultrafine Sb2O3-Sb2O5 and Sb2O3-SnO2 composite powders. 展开更多
关键词 antimony oxide ultrafine powder composite powder distillation-rectification alcoholate
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