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光化学制备纳米银溶胶及其灭菌性能表征 被引量:3
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作者 杨胜科 费晓华 +2 位作者 杜双田 赵有林 蒋丽娟 《功能材料》 EI CAS CSCD 北大核心 2004年第z1期2383-2385,共3页
采用紫外光化学制备了胶态纳米银,用透射电镜、吸收光谱对该纳米银进行了表征.发现纳米银的颗粒呈球形均匀分布,平均粒经为10nm,吸收峰位于426nm处.利用悬液法对纳米银胶的杀灭细菌性能进行了研究,结果表明,在20~22℃条件下,5mg/L纳米... 采用紫外光化学制备了胶态纳米银,用透射电镜、吸收光谱对该纳米银进行了表征.发现纳米银的颗粒呈球形均匀分布,平均粒经为10nm,吸收峰位于426nm处.利用悬液法对纳米银胶的杀灭细菌性能进行了研究,结果表明,在20~22℃条件下,5mg/L纳米银胶与细菌作用10min,能将98.98%的金黄色葡萄球菌和99.30%大肠杆菌杀灭.纳米银浓度在3~20mg/L范围内,灭菌效率变化不大. 展开更多
关键词 纳米银胶粒 光化学制备 灭菌作用
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Green synthesis of silver nanoneedles using shallot and apricot tree gum
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作者 Mohammad Mahdi TAHERI Mohammed Rafiq ABDUL KADIR +3 位作者 Noor Kamila AHMAD SHAFIAI Tolou SHOKUHFAR Mahtab ASSADIAN Mostafa Rezazadeh SHIRDAR 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2015年第10期3286-3290,共5页
A green synthesis method to produce silver nanoneedles was described using shallot and apricot tree gum(ATG).A fast,simple,and low cost method was used to synthesize silver with nanoparticle and nanoneedle shape fro... A green synthesis method to produce silver nanoneedles was described using shallot and apricot tree gum(ATG).A fast,simple,and low cost method was used to synthesize silver with nanoparticle and nanoneedle shape from the silver nitrate solution.Shallot as a reducing agent and apricot tree gum(ATG) as a stabilizer and a capping agent were utilized to reduce and form silver ions into silver atoms with needle and particle shape.Moreover,high crystalline structures of silver nanoparticles(AgNPs) with diameters of 8-20 nm and silver nanoneedles with average diameters of 50-60 nm and lengths of 5-10 μm were consequently synthesized by shallot and the mixture of shallot and ATG.A self-assembly mechanism was proposed to indicate the formation of needle-like structures of spherical Ag NPs via carbon chains of ATG.The results indicate that the presence of ATG with shallot can transfer the reduced Ag NPs into the silver nanoneedle.The findings were characterized using X-ray diffraction(XRD),ultra violet visible(UV-Vis) spectrometry,field emission scanning electron microscopy(FESEM),and transmission electron microscopy(TEM) techniques. 展开更多
关键词 green synthesis SILVER NANONEEDLE nanoparticle SHALLOT apricot tree gum self-assembly
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Sol-Gel Synthesis and Structure-Property Relations in Silver Nanoparticles-Dispersed in GeO2 Matrix
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作者 Bidhu Bhusan Das Jubin Jose Murugesan Yogapriya 《Journal of Chemistry and Chemical Engineering》 2010年第6期58-62,共5页
Synthesis of Ag nanoparticles dispersed in germanium dioxide (GeO2) matrix was performed via sol-gel route. Analysis of the powder X-ray diffraction (XRD) pattern shows fcc cubic unit cell of Ag with lattice param... Synthesis of Ag nanoparticles dispersed in germanium dioxide (GeO2) matrix was performed via sol-gel route. Analysis of the powder X-ray diffraction (XRD) pattern shows fcc cubic unit cell of Ag with lattice parameters: a = 4.0884 A, space group Fm-3m. Energy dispersive analysis of X-rays (EDAX) results show the presence of only GeO2 and Ag in the sample. The average crystallite sizes of Ag particles determined by Scherrer's relation are found to be i 8-47 nm. Observed sharp electron paramagnetic resonance (EPR) lineshapes at 8, 70 and 300 K with g-values of 2.004, 2.004, and 2.004, respectively, show that the Ag (5s~) electrons are localized in the Ag nanoparticles. The calculated value of the magnetic susceptibility is 1.014~ 10-5 emu/gG from the observed magnetic moments data at 300 K, which shows fairly strong paramagnetic nature of the material. Refinement of Ag crystal structure in space group Fm-3m with Ag atoms in 4(a) position shows the agreement bond length as 2.8909 ,&. Calculated density of states below Fermi factors Rp= 67.22%, Rwp= 75.7%, Rexp= 0.06%, Z = 4 and Ag-Ag energy, EF, from -2 to -8 eV are due to valence d orbitals of Ag. 展开更多
关键词 Sol-gel method powder XRD Ag nanoparticles EPR.
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玻璃Te/Pb对晶硅太阳能电池电性能的影响
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作者 陆建鑫 曹秀华 +2 位作者 何峰 杜静仪 黄子怀 《武汉理工大学学报》 CAS 北大核心 2015年第9期7-13,共7页
通过熔体冷却法制备得到不同Te/Pb的碲酸盐玻璃,研究了不同Te/Pb对碲酸盐玻璃的结构、性能和晶硅太阳能电池电性能的影响。采用傅里叶变换红外光谱仪和X射线衍射仪分析了玻璃的结构,通过热分析测试玻璃的热学性能,采用分选仪测试太阳能... 通过熔体冷却法制备得到不同Te/Pb的碲酸盐玻璃,研究了不同Te/Pb对碲酸盐玻璃的结构、性能和晶硅太阳能电池电性能的影响。采用傅里叶变换红外光谱仪和X射线衍射仪分析了玻璃的结构,通过热分析测试玻璃的热学性能,采用分选仪测试太阳能电池的电性能,利用场发射扫描电镜观察太阳能电池正面电极Ag/Si接触界面的微观结构。研究结果表明:随着Te/Pb的降低,玻璃的网络结构增强,但玻璃化转变温度(Tg)不断下降,太阳能电池的串联电阻(R_s)先降低后升高,与短路电流(I_(sc))、填充因子(FF)和光电转换效率(Eff)的变化规律相反;玻璃的Te/Pb不宜过高或过低,当Te/Pb为1.4时,Ag/Si界面的玻璃层中和硅发射极表面存在大量纳米银胶粒子,有利于银硅之间进行光电子传导,从而降低了太阳能电池的R_s,获得最佳的E_(ff)。 展开更多
关键词 碲酸盐玻璃 玻璃化转变温度 银硅接触 纳米银胶粒 太阳能电池
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