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无压烧结Si_3N_4与表面镀钛膜之间的固态化学反应过程 被引量:4
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作者 冼爱平 斯重遥 《金属学报》 SCIE EI CAS CSCD 北大核心 1989年第6期B427-B429,共3页
用X射线衍射技术研究了在Si_3N_4陶瓷与表面镀钛膜之间的固态化学反应过程,当反应温度不超过973K时,Ti与Si_3N_4之间不反应;温度在1073—1123K时,反应产物为Ti_2N和Ti_5Si_3,温度达到1173K时,反应产物为TiN和Ti_5Si_4,温度达到1273K时,... 用X射线衍射技术研究了在Si_3N_4陶瓷与表面镀钛膜之间的固态化学反应过程,当反应温度不超过973K时,Ti与Si_3N_4之间不反应;温度在1073—1123K时,反应产物为Ti_2N和Ti_5Si_3,温度达到1173K时,反应产物为TiN和Ti_5Si_4,温度达到1273K时,反应产物为TiN和Ti_5Si_4。在整个反应过程中,Si_3N_4陶瓷基体相的晶格常数未发生变化,说明Ti原子不能溶入Si_3N_4陶瓷的晶格之中。 展开更多
关键词 烧结 氮化硅 镀钛膜 固态反应
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用化学沉积法在以废碎玻璃瓶为原料制备的玻璃微珠表面镀二氧化钛薄膜 被引量:1
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作者 范利灵 吴建功 +1 位作者 林宝伟 王志强 《大连工业大学学报》 CAS 北大核心 2016年第4期289-292,共4页
采用隔离剂法在煅烧温度为900℃、保温时间为30min条件下对60~80目废碎玻璃粉原料进行煅烧制备微珠样品。制备出的微珠样品经过酸碱处理后,利用化学沉积法在其表面镀二氧化钛膜以增加其表面反射率。镀膜时通过改变TiCl_4浓度、尿素浓度... 采用隔离剂法在煅烧温度为900℃、保温时间为30min条件下对60~80目废碎玻璃粉原料进行煅烧制备微珠样品。制备出的微珠样品经过酸碱处理后,利用化学沉积法在其表面镀二氧化钛膜以增加其表面反射率。镀膜时通过改变TiCl_4浓度、尿素浓度、反应温度等因素,经过偏光显微镜观察、反射率测试、EDS测试确定最佳镀膜条件。最佳镀膜条件为:TiCl_4 0.2mol/L,尿素0.5mol/L,反应温度70℃。镀膜后反射率比镀膜前提高了7%。 展开更多
关键词 玻璃微珠 煅烧条件 镀钛膜 反射率
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镀生物膜镍钛记忆合金支架治疗急性喉气管损伤2例报告
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作者 郭德强 尉爱华 李玉臻 《耳鼻咽喉(头颈外科)》 2001年第5期315-315,共1页
关键词 生物记忆合金支架 治疗 急性喉气管损伤
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Effect of deposition parameters on mechanical properties of TiN films coated on 2A12 aluminum alloys by arc ion plating (AIP) 被引量:1
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作者 AWAD Samir Hamid 《Journal of Chongqing University》 CAS 2005年第1期28-32,共5页
TiN films were deposited on 2A12 aluminum alloy by arc ion plating (AIP). The Vickers hardness of the films deposited at different bias voltages and different nitrogen gas pressures, and that of the substrate were mea... TiN films were deposited on 2A12 aluminum alloy by arc ion plating (AIP). The Vickers hardness of the films deposited at different bias voltages and different nitrogen gas pressures, and that of the substrate were measured. The surface roughness of the TiN films diposited at –30 V and –80 V respectively and at different nitrogen gas pressure was measured also. The mass loss of TiN films deposited at 0 V, –30 V and –80 V respectively were analyzed in dry sand rubber wheel abrasive wear tests and wet ones in comparison with uncoated Al alloy and austenitic stainless steel (AISI 316L). It is revealed that the highest hardness of the TiN film is obtained at a bias voltage of –30 V and a N2 gas pressure of 0.5 Pa. The surface roughness of the film is larger at –80 V than that at –30 V and reduces as the increase of the N2 gas pressure. The mass loss of TiN-film coated 2A12 aluminum alloy is remarkably less than that of uncoated Al alloy and also that of AISI 316L, which indicates that the abrasive wear rate is greatly reduced by the application of TiN coating. TiN coating deposited by arc ion plating (AIP) technique on aluminum alloy can be a potential coating for machine parts requiring preciseness and lightness. 展开更多
关键词 aluminum alloys arc ion plating HARDNESS wear resistance TiN film.
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