研究了Cu Al Be B形状记忆合金的成分、微观组织和相结构与阻尼和力学性能的关系 ,通过扫描电镜原位观察合金在单向拉伸应力作用下裂纹萌生和扩展的特征。结果表明 :应力诱发马氏体变体的转变使Cu Al Be B合金具有较高的阻尼性能 ;弹性...研究了Cu Al Be B形状记忆合金的成分、微观组织和相结构与阻尼和力学性能的关系 ,通过扫描电镜原位观察合金在单向拉伸应力作用下裂纹萌生和扩展的特征。结果表明 :应力诱发马氏体变体的转变使Cu Al Be B合金具有较高的阻尼性能 ;弹性各向异性和相变应变差引发晶界应力集中 ,导致合金在拉伸条件下发生晶间断裂 ;18R与 2H马氏体混合程度大时 ,会增加相变应变差引起的晶界应力集中和可能萌生的晶界裂纹源 ,大大减小合金的塑性和强度。展开更多
采用扫描电镜、X射线衍射分析等手段 ,研究了正火处理对Cu Al Be B合金组织、相结构及阻尼和力学性能的影响 ,并原位观察拉伸应力作用下裂纹的萌生和扩展过程。研究结果表明 ,Cu Al Be B合金具有较高的阻尼性能 (S D C =17%～ 19% ) ,...采用扫描电镜、X射线衍射分析等手段 ,研究了正火处理对Cu Al Be B合金组织、相结构及阻尼和力学性能的影响 ,并原位观察拉伸应力作用下裂纹的萌生和扩展过程。研究结果表明 ,Cu Al Be B合金具有较高的阻尼性能 (S D C =17%～ 19% ) ,正火处理可抑制α相的析出 ,并减少γ1′的混杂程度 ,从而进一步提高阻尼能力。各向弹性异性和相变应变差引起的晶界集中应力 ,导致Cu A1 Be B合金在拉伸条件下发生晶间断裂。正火处理不但纯净晶界 ,形成马氏体共格晶界 ,而且减小晶内γ1′马氏体与 β1′马氏体的混合程度 ,有利于减少晶界应力集中和可能萌生的晶界裂纹源 ,从而有效改善合金的塑性和强度。展开更多
The morphology and formation mechanism of the substructure of martensite in TC21 alloy was investigated by XRD and TEM. The results showed that the martensitic transformation from β to α＂ occurs upon quenching afte...The morphology and formation mechanism of the substructure of martensite in TC21 alloy was investigated by XRD and TEM. The results showed that the martensitic transformation from β to α＂ occurs upon quenching after solution treatment between 960-1000 ℃. The antiphase boundary （APB）-like structure was observed clearly in the α＂ martensite plates. The APB-like contrasts exist along the （001） and （020） planes of α＂ martensite. This APB-like structure of α＂ martensite was identified as a kind of stacking fault with an APB-like morphology induced by martensitic transformation and not by order/disorder transition. During martensitic transformation, martensitic domains nucleate and grow, eventually encounter each other, resulting in the formation of the APBdike contrast.展开更多
Heat treatment of Ti-50.9%Ni （mole fraction） alloy was studied by differential scanning calorimetry, X-ray diffraction, scanning electron microscopey and energy dispersive X-ray analysis to investigate the influence...Heat treatment of Ti-50.9%Ni （mole fraction） alloy was studied by differential scanning calorimetry, X-ray diffraction, scanning electron microscopey and energy dispersive X-ray analysis to investigate the influence of cooling rate on transformation behavior and microstructures of NiTi shape memory alloy. The experimental results show that three-stage phase transformation can be induced at a very low cooling rate such as cooling in furnace. The cooling rate also has a great influence on the phase transformation temperatures. Both martensitic start transformation temperature （Ms） and martensitic finish transformation temperature （Mf） decrease with the decrease of the cooling rate, and decreasing the cooling rate contributes to enhancing the M→A austenite transformation temperature. The phase transformation hysteresis （Af-Mf） increases with the decrease of the cooling rate. Heat treatment is unable to eliminate the textures formed in hot working of NiTi sample, but can weaken the intensity of them. The cooling rate has little influence on the grain size.展开更多
Effect of tempering temperature on the microstructure and mechanical properties of AISI 6150 steel was investigated. All samples were austenitized at 870 ℃ for 45 min followed by oil quenching, and then tempered at t...Effect of tempering temperature on the microstructure and mechanical properties of AISI 6150 steel was investigated. All samples were austenitized at 870 ℃ for 45 min followed by oil quenching, and then tempered at temperatures between 200 and 600 ℃ for 60 min. The results show that the microstructure of tempered sample at 200 ℃ mainly consists of tempered martensite. With increasing the tempered temperature, the martensite transforms to the ferrite and carbides. The ultimate tensile strength, the hardness and the retained austenite decrease with increasing tempered temperature, and 0.2% yield strength increases when the temperature increases from 200 to 300 ℃ and then decreases with increasing the temperature, but the elongation and impact energy increase with increasing the tempering temperature.展开更多
On-line thermo mechanical controlled processing(TMCP) was conducted to develop the third generation high strength low alloy(HSLA) steel with high toughness economically.The ultra-low carbon content ensured a high leve...On-line thermo mechanical controlled processing(TMCP) was conducted to develop the third generation high strength low alloy(HSLA) steel with high toughness economically.The ultra-low carbon content ensured a high level of upper shelf energy while ultrafine lath martensitic structure transformed from super-thin pancaked austenite during controlled rolling and cooling.The reduction of martensite block size decreased ductile-to-brittle transition temperature(DBTT) and compensated the strength loss due to carbon reduction.Consequently,the excellent balance of strength and toughness values was obtained as 950-1060 MPa for yield strength,180 J for Charpy V-notch impact absorbed energy at 30℃,which is much superior to that of traditional martensitic steel.Two mechanisms for the refinement of lath martensite block were proposed:One is the austenite grain refinement in the direction of thickness,and the other is the reduction in the fraction of sub-block boundaries with small misorientation and the increase in the fraction of block boundaries with large misorientation,possibly due to austenite hardening.展开更多
文摘研究了Cu Al Be B形状记忆合金的成分、微观组织和相结构与阻尼和力学性能的关系 ,通过扫描电镜原位观察合金在单向拉伸应力作用下裂纹萌生和扩展的特征。结果表明 :应力诱发马氏体变体的转变使Cu Al Be B合金具有较高的阻尼性能 ;弹性各向异性和相变应变差引发晶界应力集中 ,导致合金在拉伸条件下发生晶间断裂 ;18R与 2H马氏体混合程度大时 ,会增加相变应变差引起的晶界应力集中和可能萌生的晶界裂纹源 ,大大减小合金的塑性和强度。
文摘采用扫描电镜、X射线衍射分析等手段 ,研究了正火处理对Cu Al Be B合金组织、相结构及阻尼和力学性能的影响 ,并原位观察拉伸应力作用下裂纹的萌生和扩展过程。研究结果表明 ,Cu Al Be B合金具有较高的阻尼性能 (S D C =17%～ 19% ) ,正火处理可抑制α相的析出 ,并减少γ1′的混杂程度 ,从而进一步提高阻尼能力。各向弹性异性和相变应变差引起的晶界集中应力 ,导致Cu A1 Be B合金在拉伸条件下发生晶间断裂。正火处理不但纯净晶界 ,形成马氏体共格晶界 ,而且减小晶内γ1′马氏体与 β1′马氏体的混合程度 ,有利于减少晶界应力集中和可能萌生的晶界裂纹源 ,从而有效改善合金的塑性和强度。
基金Project (2011AA030101) supported by the High-tech Research and Development Program of China
文摘The morphology and formation mechanism of the substructure of martensite in TC21 alloy was investigated by XRD and TEM. The results showed that the martensitic transformation from β to α＂ occurs upon quenching after solution treatment between 960-1000 ℃. The antiphase boundary （APB）-like structure was observed clearly in the α＂ martensite plates. The APB-like contrasts exist along the （001） and （020） planes of α＂ martensite. This APB-like structure of α＂ martensite was identified as a kind of stacking fault with an APB-like morphology induced by martensitic transformation and not by order/disorder transition. During martensitic transformation, martensitic domains nucleate and grow, eventually encounter each other, resulting in the formation of the APBdike contrast.
基金Project (51071056) supported by the National Natural Science Foundation of ChinaProjects (HEUCFR1132, HEUCF121712) supported by the Fundamental Research Funds for the Central Universities of China
文摘Heat treatment of Ti-50.9%Ni （mole fraction） alloy was studied by differential scanning calorimetry, X-ray diffraction, scanning electron microscopey and energy dispersive X-ray analysis to investigate the influence of cooling rate on transformation behavior and microstructures of NiTi shape memory alloy. The experimental results show that three-stage phase transformation can be induced at a very low cooling rate such as cooling in furnace. The cooling rate also has a great influence on the phase transformation temperatures. Both martensitic start transformation temperature （Ms） and martensitic finish transformation temperature （Mf） decrease with the decrease of the cooling rate, and decreasing the cooling rate contributes to enhancing the M→A austenite transformation temperature. The phase transformation hysteresis （Af-Mf） increases with the decrease of the cooling rate. Heat treatment is unable to eliminate the textures formed in hot working of NiTi sample, but can weaken the intensity of them. The cooling rate has little influence on the grain size.
基金Project(2011BAE13B03) supported by the National Key Technology R&D Program of China
文摘Effect of tempering temperature on the microstructure and mechanical properties of AISI 6150 steel was investigated. All samples were austenitized at 870 ℃ for 45 min followed by oil quenching, and then tempered at temperatures between 200 and 600 ℃ for 60 min. The results show that the microstructure of tempered sample at 200 ℃ mainly consists of tempered martensite. With increasing the tempered temperature, the martensite transforms to the ferrite and carbides. The ultimate tensile strength, the hardness and the retained austenite decrease with increasing tempered temperature, and 0.2% yield strength increases when the temperature increases from 200 to 300 ℃ and then decreases with increasing the temperature, but the elongation and impact energy increase with increasing the tempering temperature.
基金supported by the National Basic Research Program of China ("973" Program) (Grant No. 2010CB630805)the National Natural Science Foundation of China (Grant No. 51071089)
文摘On-line thermo mechanical controlled processing(TMCP) was conducted to develop the third generation high strength low alloy(HSLA) steel with high toughness economically.The ultra-low carbon content ensured a high level of upper shelf energy while ultrafine lath martensitic structure transformed from super-thin pancaked austenite during controlled rolling and cooling.The reduction of martensite block size decreased ductile-to-brittle transition temperature(DBTT) and compensated the strength loss due to carbon reduction.Consequently,the excellent balance of strength and toughness values was obtained as 950-1060 MPa for yield strength,180 J for Charpy V-notch impact absorbed energy at 30℃,which is much superior to that of traditional martensitic steel.Two mechanisms for the refinement of lath martensite block were proposed:One is the austenite grain refinement in the direction of thickness,and the other is the reduction in the fraction of sub-block boundaries with small misorientation and the increase in the fraction of block boundaries with large misorientation,possibly due to austenite hardening.
