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响应面法优化马蹄皮渣中总黄酮的微波提取工艺研究 被引量:3
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作者 黄利华 刘欣 《安徽农业科学》 CAS 2014年第17期5634-5637,共4页
[目的]为更好地利用马蹄加工皮渣中的资源,优化马蹄皮渣中总黄酮的微波提取工艺,得到得率较高的黄酮类化合物。[方法]采用Box-Behnken中心组合响应面法优化马蹄粉加工皮渣中总黄酮的微波提取工艺,建立了不同影响因素与马蹄总黄酮得率之... [目的]为更好地利用马蹄加工皮渣中的资源,优化马蹄皮渣中总黄酮的微波提取工艺,得到得率较高的黄酮类化合物。[方法]采用Box-Behnken中心组合响应面法优化马蹄粉加工皮渣中总黄酮的微波提取工艺,建立了不同影响因素与马蹄总黄酮得率之间的函数关系。[结果]确定最佳提取工艺条件为:乙醇浓度55.4%,料液比1∶30 g/ml,微波功率320 W,微波3 min,在此条件下重复提取2次,理论得率为2.376%,经过验证得到总黄酮得率为2.365%,实测值与理论预测值之间的相对误差为0.461%。[结论]研究结果表明,优化得到的提取工艺可靠,可为马蹄加工废弃物的综合高效利用提供参考依据。 展开更多
关键词 马蹄皮渣 总黄酮 响应面法 微波
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Optimization of Microwave Extraction of Flavonoids from Water Chestnut Skin Dregs with Response Surface Method
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作者 黄利华 《Agricultural Science & Technology》 CAS 2015年第1期187-191,共5页
[Objective] In order to take full advantage of processing by-product of water chestnut, the microwave extraction method of flavonoids from water chestnut skin dregs was optimized. The extracted flavonoids had a relati... [Objective] In order to take full advantage of processing by-product of water chestnut, the microwave extraction method of flavonoids from water chestnut skin dregs was optimized. The extracted flavonoids had a relatively high yield. [Method] The Box-Behnken design-based response surface method was adopted to optimize the microwave extraction of flavonoids from water chestnut skin dregs, a by-product of water chestnut starch. The mathematical relationships between various influencing factors and flavonoids yield were established. [Result] The optimum extraction conditions of flavonoids from water chestnut skin dregs were as follows: ethanol concentration of 55.4%, solid/liquid ratio of 1:30 g/ml, microwave power of 320 W, microwave time of 3 min and microwave time of 2 times. Under the optimum extraction conditions, the theoretical flavonoids yield was 2.376%. However, the actual flavonoids yield under the optimum extraction conditions was 2.365%. The relative error between actual values and theoretically predicted values was 0.461%. [Conclusion] The results showed the optimized extraction method is reliable, and it can provide a reference for the comprehensive and highly efficient utilization of water chestnut processing wastes. 展开更多
关键词 Water chestnut skin dregs FLAVONOIDS Response surface methodology (RSM) MICROWAVE
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