<div style="text-align:justify;"> In view of the serious lack and lag of the test and evaluation technology of non-metallic composite continuous pipe, and focusing on the characteristics of the applica...<div style="text-align:justify;"> In view of the serious lack and lag of the test and evaluation technology of non-metallic composite continuous pipe, and focusing on the characteristics of the application of non-metallic composite continuous pipe in oil field, this paper discusses a series of new full-scale test and evaluation technologies for accurately evaluating the product quality and practical application performance of non-metallic composite continuous pipe, which effectively solves the major technical problem that the new products of non-metallic pipe cannot be accurately evaluated. Based on the characteristics of the application of non-metallic composite continuous pipe in oil field, a series of new full-scale test evaluation technologies which can accurately evaluate the product quality and practical application performance of non-metallic pipe are designed through a large number of tests. The test and evaluation technology can accurately evaluate the key performance of high and low pressure cycle, high and low temperature cycle, gas permeability resistance, minimum bending radius etc. It provides a scientific evaluation basis for the standardized application of non-metallic continuous pipe and a reliable quality control method for the selection of products in oil field. </div>展开更多
Y 2O 3 nanoparticles organosol coated with DBS was prepared by microemulsion method. The optimum preparative conditions of Y 2O 3 nanoparticles organosol were obtained. TEM analysis indicates that the prepared Y ...Y 2O 3 nanoparticles organosol coated with DBS was prepared by microemulsion method. The optimum preparative conditions of Y 2O 3 nanoparticles organosol were obtained. TEM analysis indicates that the prepared Y 2O 3 nanoparticles are spherical in shape. The size is about 5 nm. The size distribution is in the narrow range and no agglomerates are observed. Y 2O 3 nanoparticles coated with DBS are easy to dissolve in weak polar solvents.展开更多
The generation of hydrogen through the electrolysis of water has attracted attention as a promising way to produce and store energy using renewable energy sources.In this process,a catalyst is very important to achiev...The generation of hydrogen through the electrolysis of water has attracted attention as a promising way to produce and store energy using renewable energy sources.In this process,a catalyst is very important to achieve a high‐energy conversion efficiency for the electrolysis of water.A good catalyst for water electrolysis should exhibit high catalytic activity,good stability,low cost and good scalability.Much research has been devoted to developing efficient catalysts for both the hydrogen evolution reaction(HER)and oxygen evolution reaction(OER).Traditionally,it has been accepted that a material with high crystallinity is important to serve as a good catalyst for HER and/or OER.Recently,catalysts for HER and/or OER in the electrolysis of water splitting based on amorphous materials have received much interest in the scientific community owing to the abundant unsaturated active sites on the amorphous surface,which form catalytic centers for the reaction of the electrolysis of water.We summarize the recent advances of amorphous catalysts for HER,OER and overall water splitting by electrolysis and the related fundamental chemical reactions involved in the electrolysis of water.The current challenges confronting the electrolysis of water and the development of more efficient amorphous catalysts are also discussed.展开更多
Proton exchange membrane fuel cells suffer from the sluggish kinetics of the oxygen reduction reaction(ORR)and the high cost of Pt catalysts.In the present work,a high‐performance ORR catalystbased on Fe,N,S‐doped p...Proton exchange membrane fuel cells suffer from the sluggish kinetics of the oxygen reduction reaction(ORR)and the high cost of Pt catalysts.In the present work,a high‐performance ORR catalystbased on Fe,N,S‐doped porous carbon(FeNS‐PC)was synthesized using melamine formaldehyderesin as C and N precursors,Fe(SCN)3as Fe and S precursors,and CaCl2as a template via a two‐stepheat treatment without a harsh template removal step.The results show that the catalyst treated at900℃(FeNS‐PC‐900)had a high surface area of775m2/g,a high mass activity of10.2A/g in anacidic medium,and excellent durability;the half‐wave potential decreased by only20mV after10000potential cycles.The FeNS‐PC‐900catalyst was used as the cathode in a proton exchangemembrane fuel cell and delivered a peak power density of0.49W/cm2.FeNS‐PC‐900therefore hasgood potential for use in practical applications.展开更多
This paper deals with the reconstruction and innovation of an ordinary magnetostriction apparatus for cavitation erosion tests of non metallic materials. It aims at making testing specimen to be independent of amplit...This paper deals with the reconstruction and innovation of an ordinary magnetostriction apparatus for cavitation erosion tests of non metallic materials. It aims at making testing specimen to be independent of amplitude amplifier rod, thus overcoming the difficulties of fixing tightly the non metallic specimen to the vibrating rod. Such approach makes the exposure area greatly increased and effectively mitigates the effect of non homogeneity of non metallic specimen on the testing results, thus extending the application of magnetostriction apparatus to carry out cavitation erosion tests to larger size of non metallic and non homogeneous materials. It will render a set of new innovative apparatus and recently developed method to conduct fast and simple cavitation erosion test in days to come. Simultaneously, several tests on non metallic materials have been made by means of such new apparatus, yielding satisfactory results and witnessing the availability of new methods.展开更多
Glutamic acid and gamma-aminobutyric acid （GABA） influence iron content in the substantia nigra and globus pallidus, although the mechanisms of action remain unclear. The present study measured iron content and chan...Glutamic acid and gamma-aminobutyric acid （GABA） influence iron content in the substantia nigra and globus pallidus, although the mechanisms of action remain unclear. The present study measured iron content and changes in divalent metal transporter 1 （DMT1） and hephaestin expression in the substantia nigra and caudate putamen, and explored the effects of GABA and glutamic acid on iron metabolism. Results demonstrated that iron content and DMT1 non iron response element [DMT1 （-IRE）] expression were significantly greater but hephaestin expression was significantly lower in the caudate putamen of the monosodium glutamate group compared with the control group. No significant difference in iron content was detected between the GABA and control groups. DMT1 （-IRE） expression was significantly reduced, but hephaestin expressiori was significantly increased in the GABA group compared with the control group. In addition, there was no significant difference in tyrosine hydroxylase expression between monosodium glutamate and GABA groups and the control group. These results suggested that glutamate affected iron metabolism in the caudate putamen by increasing DMTI（-IRE） and decreasing hephaestin expression. In addition, GABA decreased DMT1 （-IRE） expression in the caudate putamen.展开更多
The comprehensive utilization of abundant high-boron iron concentrate is of particular significance to Chi- na, and the high-boron iron concentrate has not yet been utilized as a source for boron at an industrial scal...The comprehensive utilization of abundant high-boron iron concentrate is of particular significance to Chi- na, and the high-boron iron concentrate has not yet been utilized as a source for boron at an industrial scale due to its complex mineralogy and fine mineral dissemination. An innovative method was proposed for recovery of boron and iron from high-boron iron concentrate by reduction roasting and magnetic sepa- ration. The effects of reduction temperature and roasting time were investigated and their optimum condi- tions were determined. The mineralogical changes during roasting were characterized by X-ray diffraction （XRD） and scanning electron microscopy （SEM）. The results showed that the pyrrhotite （FeS） contained in the high-boron iron concentrate and the new-formed FeS-Fe solid solution softened or melted at high temperatures owing to their low melting points, and then decreased the metallic iron ratio and accelerated the growth of metallic iron particles. Meanwhile, the magnetite and szaibelyite were converted into metal- lic iron and suanite, respectively. Consequently, boron was readily enriched into the non-magnetic product and the metallic iron was aggregated to the magnetic concentrate by magnetic separation. Boron recovery of 88.6% with corresponding B2O3 content of 14.5% and iron recovery of 95.1% with an iron grade of 92.7% were achieved when high-boron iron concentrate was reduced at 1 125℃ for 150 min. Besides, the boron reactivity of the boron-rich non-magnetic product was up to 80.8%.展开更多
文摘<div style="text-align:justify;"> In view of the serious lack and lag of the test and evaluation technology of non-metallic composite continuous pipe, and focusing on the characteristics of the application of non-metallic composite continuous pipe in oil field, this paper discusses a series of new full-scale test and evaluation technologies for accurately evaluating the product quality and practical application performance of non-metallic composite continuous pipe, which effectively solves the major technical problem that the new products of non-metallic pipe cannot be accurately evaluated. Based on the characteristics of the application of non-metallic composite continuous pipe in oil field, a series of new full-scale test evaluation technologies which can accurately evaluate the product quality and practical application performance of non-metallic pipe are designed through a large number of tests. The test and evaluation technology can accurately evaluate the key performance of high and low pressure cycle, high and low temperature cycle, gas permeability resistance, minimum bending radius etc. It provides a scientific evaluation basis for the standardized application of non-metallic continuous pipe and a reliable quality control method for the selection of products in oil field. </div>
文摘Y 2O 3 nanoparticles organosol coated with DBS was prepared by microemulsion method. The optimum preparative conditions of Y 2O 3 nanoparticles organosol were obtained. TEM analysis indicates that the prepared Y 2O 3 nanoparticles are spherical in shape. The size is about 5 nm. The size distribution is in the narrow range and no agglomerates are observed. Y 2O 3 nanoparticles coated with DBS are easy to dissolve in weak polar solvents.
基金the financial support from Chinese Scholarship Council (CSC)the support from Australian Research Council (ARC) Future Fellowship scheme
文摘The generation of hydrogen through the electrolysis of water has attracted attention as a promising way to produce and store energy using renewable energy sources.In this process,a catalyst is very important to achieve a high‐energy conversion efficiency for the electrolysis of water.A good catalyst for water electrolysis should exhibit high catalytic activity,good stability,low cost and good scalability.Much research has been devoted to developing efficient catalysts for both the hydrogen evolution reaction(HER)and oxygen evolution reaction(OER).Traditionally,it has been accepted that a material with high crystallinity is important to serve as a good catalyst for HER and/or OER.Recently,catalysts for HER and/or OER in the electrolysis of water splitting based on amorphous materials have received much interest in the scientific community owing to the abundant unsaturated active sites on the amorphous surface,which form catalytic centers for the reaction of the electrolysis of water.We summarize the recent advances of amorphous catalysts for HER,OER and overall water splitting by electrolysis and the related fundamental chemical reactions involved in the electrolysis of water.The current challenges confronting the electrolysis of water and the development of more efficient amorphous catalysts are also discussed.
基金supported by the National Basic Research Program of China (973 Program,2015CB932303)the National Natural Science Founda-tion of China (21373175,21621091)~~
文摘Proton exchange membrane fuel cells suffer from the sluggish kinetics of the oxygen reduction reaction(ORR)and the high cost of Pt catalysts.In the present work,a high‐performance ORR catalystbased on Fe,N,S‐doped porous carbon(FeNS‐PC)was synthesized using melamine formaldehyderesin as C and N precursors,Fe(SCN)3as Fe and S precursors,and CaCl2as a template via a two‐stepheat treatment without a harsh template removal step.The results show that the catalyst treated at900℃(FeNS‐PC‐900)had a high surface area of775m2/g,a high mass activity of10.2A/g in anacidic medium,and excellent durability;the half‐wave potential decreased by only20mV after10000potential cycles.The FeNS‐PC‐900catalyst was used as the cathode in a proton exchangemembrane fuel cell and delivered a peak power density of0.49W/cm2.FeNS‐PC‐900therefore hasgood potential for use in practical applications.
文摘This paper deals with the reconstruction and innovation of an ordinary magnetostriction apparatus for cavitation erosion tests of non metallic materials. It aims at making testing specimen to be independent of amplitude amplifier rod, thus overcoming the difficulties of fixing tightly the non metallic specimen to the vibrating rod. Such approach makes the exposure area greatly increased and effectively mitigates the effect of non homogeneity of non metallic specimen on the testing results, thus extending the application of magnetostriction apparatus to carry out cavitation erosion tests to larger size of non metallic and non homogeneous materials. It will render a set of new innovative apparatus and recently developed method to conduct fast and simple cavitation erosion test in days to come. Simultaneously, several tests on non metallic materials have been made by means of such new apparatus, yielding satisfactory results and witnessing the availability of new methods.
基金the National Natural Science Foundation of China, No. 30570957the Natural Science Foundation of Hebei Province, No. C2006000152, C2007000251
文摘Glutamic acid and gamma-aminobutyric acid （GABA） influence iron content in the substantia nigra and globus pallidus, although the mechanisms of action remain unclear. The present study measured iron content and changes in divalent metal transporter 1 （DMT1） and hephaestin expression in the substantia nigra and caudate putamen, and explored the effects of GABA and glutamic acid on iron metabolism. Results demonstrated that iron content and DMT1 non iron response element [DMT1 （-IRE）] expression were significantly greater but hephaestin expression was significantly lower in the caudate putamen of the monosodium glutamate group compared with the control group. No significant difference in iron content was detected between the GABA and control groups. DMT1 （-IRE） expression was significantly reduced, but hephaestin expressiori was significantly increased in the GABA group compared with the control group. In addition, there was no significant difference in tyrosine hydroxylase expression between monosodium glutamate and GABA groups and the control group. These results suggested that glutamate affected iron metabolism in the caudate putamen by increasing DMTI（-IRE） and decreasing hephaestin expression. In addition, GABA decreased DMT1 （-IRE） expression in the caudate putamen.
基金the financial support from the National Natural Science Foundation of China (51134002)the Fundamental Research Funds for the Central Universities of China (N140108001 and N150106003)
文摘The comprehensive utilization of abundant high-boron iron concentrate is of particular significance to Chi- na, and the high-boron iron concentrate has not yet been utilized as a source for boron at an industrial scale due to its complex mineralogy and fine mineral dissemination. An innovative method was proposed for recovery of boron and iron from high-boron iron concentrate by reduction roasting and magnetic sepa- ration. The effects of reduction temperature and roasting time were investigated and their optimum condi- tions were determined. The mineralogical changes during roasting were characterized by X-ray diffraction （XRD） and scanning electron microscopy （SEM）. The results showed that the pyrrhotite （FeS） contained in the high-boron iron concentrate and the new-formed FeS-Fe solid solution softened or melted at high temperatures owing to their low melting points, and then decreased the metallic iron ratio and accelerated the growth of metallic iron particles. Meanwhile, the magnetite and szaibelyite were converted into metal- lic iron and suanite, respectively. Consequently, boron was readily enriched into the non-magnetic product and the metallic iron was aggregated to the magnetic concentrate by magnetic separation. Boron recovery of 88.6% with corresponding B2O3 content of 14.5% and iron recovery of 95.1% with an iron grade of 92.7% were achieved when high-boron iron concentrate was reduced at 1 125℃ for 150 min. Besides, the boron reactivity of the boron-rich non-magnetic product was up to 80.8%.
