BL10U2 is an undulator-based macromolecular crystallography(MX)beamline located at the 3.5-GeV Shanghai Synchrotron Radiation Facility.BL10U2 is specifically designed for conducting routine and biosafety level-2(BSL-2...BL10U2 is an undulator-based macromolecular crystallography(MX)beamline located at the 3.5-GeV Shanghai Synchrotron Radiation Facility.BL10U2 is specifically designed for conducting routine and biosafety level-2(BSL-2)MX experiments utilizing high-flux tunable X-rays with energies from 7 to 18 keV,providing a beam spot size of 20μm(horizontal)×10μm(vertical)at the sample point.Certification by the Shanghai Pudong Municipal Health Commission confirmed the capability to perform BSL-2 MX experiments.The beamline is currently equipped with an Eiger X 16 M detector and two newly developed in-house high-precision diffractometers that can be switched to perform conventional or in situ crystal diffraction experiments.An automatic sample changer developed in-house allows fast sample exchange in less than 30 s,supporting high-throughput MX experimentation and rapid crystal screening.Data collection from both the diffractometer and detector was controlled by an in-house developed data collection software(Finback)with a user-friendly interface for convenient operation.This study presents a comprehensive overview of the facilities,experimental methods,and performance characteristics of the BL10U2 beamline.展开更多
Macromolecular crystallography beamline BL17U1 at the Shanghai Synchrotron Radiation Facility has been relocated,upgraded,and given a new ID(BL02U1).It now delivers X-rays in the energy range of 6–16 keV,with a focus...Macromolecular crystallography beamline BL17U1 at the Shanghai Synchrotron Radiation Facility has been relocated,upgraded,and given a new ID(BL02U1).It now delivers X-rays in the energy range of 6–16 keV,with a focused beam of 11.6μm×4.8μm and photon flux greater than 1012 phs/s.The high credibility and stability of the beam and good timing synchronization of the equipment significantly improve the experimental efficiency.Since June 2021,when it officially opened to users,over 4200 h of beamtime have been provided to over 200 research groups to collect data at the beamline.Its good performance and stable operation have led to the resolution of several structures based on data collected at the beamline.展开更多
From a safety point of view, it is important to study the damages and reliability of molten salt reactor structural alloy materials, which are subjected to extreme environments due to neutron irradiation, molten salt ...From a safety point of view, it is important to study the damages and reliability of molten salt reactor structural alloy materials, which are subjected to extreme environments due to neutron irradiation, molten salt corrosion, fission product attacks, thermal stress, and even combinations of these. In the past few years, synchrotron radiation-based materials characterization techniques have proven to be effective in revealing the microstructural evolution and failure mechanisms of the alloys under surrogating operation conditions. Here, we review the recent progress in the investigations of molten salt corrosion,tellurium(Te) corrosion, and alloy design. The valence states and distribution of chromium(Cr) atoms, and the diffusion and local atomic structure of Te atoms near the surface of corroded alloys have been investigated using synchrotron radiation techniques, which considerably deepen the understandings on the molten salt and Te corrosion behaviors. Furthermore, the structure and size distribution of the second phases in the alloys have been obtained, which are helpful for the future development of new alloy materials.展开更多
A new X-ray imaging and biomedical application beamline(BL13HB)has been implemented at the Shanghai Radiation Synchrotron Facility(SSRF)as an upgrade to the old X-ray imaging and biomedical application beamline(BL13W1...A new X-ray imaging and biomedical application beamline(BL13HB)has been implemented at the Shanghai Radiation Synchrotron Facility(SSRF)as an upgrade to the old X-ray imaging and biomedical application beamline(BL13W1).This is part of the Phase II construction project of the SSRF.The BL13HB is dedicated to 2D and 3D static and dynamic X-ray imaging,with a field of view of up to 48.5 mm×5.2 mm and spatial resolution as high as 0.8μm.A super-bending magnet is used as the X-ray source in BL13HB,which has a maximum magnetic field of 2.293 T.The energy range of monochromatic X-ray photons from a double-multiplayer monochromator was 8–40 keV,and the white beam mode was provided on the beamline for dynamic X-ray imaging and dynamic X-ray micro-CT.While maintaining the previous experimental setup of BL13W1,new equipment was added to the beamline experimental station.The beamline is equipped with different sets of X-ray imaging detectors for several experimental methods such as micro-CT,dynamic micro-CT,and pair distribution function.The experimental station of BL13HB is designed specifically for various in situ dynamic experiments,and BL13HB has been open to users since June 2021.展开更多
New-generation synchrotron light sources are being designed and operated worldwide to provide brighter radiation by reducing the beam emittance to X-ray diffraction limits.Intra-beam scattering(IBS)and Touschek scatte...New-generation synchrotron light sources are being designed and operated worldwide to provide brighter radiation by reducing the beam emittance to X-ray diffraction limits.Intra-beam scattering(IBS)and Touschek scattering in such facilities are significant and require attention because of their ultra-low emittance.Therefore,cure strategies need to be carefully studied to obtain highquality photon beams.For the Shanghai Synchrotron Radiation Facility Upgrade(SSRF-U),a candidate lattice of the storage ring,reaching the soft X-ray diffraction limit,was designed and presented for the first time in this study.The emittance growth and beam lifetime in the SSRF-U storage ring were studied using particle simulations for a series of different machine configurations.The gains with RF frequencies of 100 MHz and 500 MHz were compared.Along with a better filling pattern,a more suitable RF frequency was adopted in the SSRF-U.The variations in the equilibrium beam emittance with beam coupling and bunch-lengthening were identified using simulations.Optimal beam coupling and required bunch-lengthening for the SSRF-U storage ring were thus determined.The fitness of the beam energy in the SSRF-U was subsequently assessed using the obtained parameters.Additionally,the Touschek scattering and beam lifetime were calculated,and an acceptable total beam lifetime was obtained.展开更多
The lattice of the Shanghai Synchrotron Radiation Facility(SSRF) storage ring was upgraded in the Phase-II beamline project, and thus far, 18 insertion devices(IDs) have been installed. The IDs cause closed-orbit dist...The lattice of the Shanghai Synchrotron Radiation Facility(SSRF) storage ring was upgraded in the Phase-II beamline project, and thus far, 18 insertion devices(IDs) have been installed. The IDs cause closed-orbit distortions, tune drift, and coupling distortions in the SSRF storage ring, all of which are significant issues that require solutions. In this study, an ID orbit feedforward compensation system based on a response matrix using corrector coils was developed, and it was applied to all commissioned IDs in the SSRF storage ring. After correction, the maximum ID-induced horizontal and vertical orbit distortions were less than 5.0 and 3.5 μm, respectively. Some interesting phenomena observed during the measurement process were explained. Additionally, optical and coupling feedforward systems were developed using quadrupole and skew quadrupole magnets installed on the front and back of elliptically polarizing undulators(EPUs). Moreover, over nearly four months of operation, the developed strategy delivered a satisfactory performance in the SSRF storage ring.展开更多
The BL19U2 at the Shanghai Synchrotron Radiation Facility is a small-angle X-ray scattering beamline dedicated to structural studies pertaining to biological macromolecules in solution.The beamline has been officially...The BL19U2 at the Shanghai Synchrotron Radiation Facility is a small-angle X-ray scattering beamline dedicated to structural studies pertaining to biological macromolecules in solution.The beamline has been officially opened to users in March 2015,and since then,a series of technological innovations has been developed to optimize beamline performance,thereby significantly improving the data collection efficiency and broadening the application scope of biological small-angle X-ray scattering.BL19U2 is ideal for the high-throughput screening of weakly scattered proteins,protein assemblies,nucleic acids,inorganic nanomaterials,and organic drug molecules.This paper describes the design and overview of the BL19U2 beamline.Versatile sample environments at the experimental station and some recent scientific highlights are presented.展开更多
基金supported by the SSRF Phase-II projectNatural Science Foundation of Shanghai(Nos.21ZR1471800 and 23ZR1471200)National Natural Science Foundation of China(No.12005281)。
文摘BL10U2 is an undulator-based macromolecular crystallography(MX)beamline located at the 3.5-GeV Shanghai Synchrotron Radiation Facility.BL10U2 is specifically designed for conducting routine and biosafety level-2(BSL-2)MX experiments utilizing high-flux tunable X-rays with energies from 7 to 18 keV,providing a beam spot size of 20μm(horizontal)×10μm(vertical)at the sample point.Certification by the Shanghai Pudong Municipal Health Commission confirmed the capability to perform BSL-2 MX experiments.The beamline is currently equipped with an Eiger X 16 M detector and two newly developed in-house high-precision diffractometers that can be switched to perform conventional or in situ crystal diffraction experiments.An automatic sample changer developed in-house allows fast sample exchange in less than 30 s,supporting high-throughput MX experimentation and rapid crystal screening.Data collection from both the diffractometer and detector was controlled by an in-house developed data collection software(Finback)with a user-friendly interface for convenient operation.This study presents a comprehensive overview of the facilities,experimental methods,and performance characteristics of the BL10U2 beamline.
基金supported by the National Key Research and Development Program of China(No.2021YFC2301405)the National Natural Science Foundation of China(No.31971121)Shanghai Science and Technology Plan Project(No.21ZR14718)。
文摘Macromolecular crystallography beamline BL17U1 at the Shanghai Synchrotron Radiation Facility has been relocated,upgraded,and given a new ID(BL02U1).It now delivers X-rays in the energy range of 6–16 keV,with a focused beam of 11.6μm×4.8μm and photon flux greater than 1012 phs/s.The high credibility and stability of the beam and good timing synchronization of the equipment significantly improve the experimental efficiency.Since June 2021,when it officially opened to users,over 4200 h of beamtime have been provided to over 200 research groups to collect data at the beamline.Its good performance and stable operation have led to the resolution of several structures based on data collected at the beamline.
基金supported by the National key research and development program of China(Nos.2016YFB0700401 and 2016YFB0700404)Natural Science Foundation of Shanghai(Nos.19ZR1468200 and 18ZR1448000)+2 种基金National Natural Science Foundation of China(Nos.51671154,51601213 and 51671122)Strategic Priority Research Program of the Chinese Academy of Sciences(No.XDA02004210)Youth Innovation Promotion Association,Chinese Academy of Science(No.2019264)
文摘From a safety point of view, it is important to study the damages and reliability of molten salt reactor structural alloy materials, which are subjected to extreme environments due to neutron irradiation, molten salt corrosion, fission product attacks, thermal stress, and even combinations of these. In the past few years, synchrotron radiation-based materials characterization techniques have proven to be effective in revealing the microstructural evolution and failure mechanisms of the alloys under surrogating operation conditions. Here, we review the recent progress in the investigations of molten salt corrosion,tellurium(Te) corrosion, and alloy design. The valence states and distribution of chromium(Cr) atoms, and the diffusion and local atomic structure of Te atoms near the surface of corroded alloys have been investigated using synchrotron radiation techniques, which considerably deepen the understandings on the molten salt and Te corrosion behaviors. Furthermore, the structure and size distribution of the second phases in the alloys have been obtained, which are helpful for the future development of new alloy materials.
基金supported by the National Major Scientific Instruments and Equipment Development Project of China(No.11627901)the National Key Research and Development Program of China(Nos.2021YFF0701202 and 2021YFA1600703)the National Natural Science Foundation of China(Nos.U1932205,12275343)。
文摘A new X-ray imaging and biomedical application beamline(BL13HB)has been implemented at the Shanghai Radiation Synchrotron Facility(SSRF)as an upgrade to the old X-ray imaging and biomedical application beamline(BL13W1).This is part of the Phase II construction project of the SSRF.The BL13HB is dedicated to 2D and 3D static and dynamic X-ray imaging,with a field of view of up to 48.5 mm×5.2 mm and spatial resolution as high as 0.8μm.A super-bending magnet is used as the X-ray source in BL13HB,which has a maximum magnetic field of 2.293 T.The energy range of monochromatic X-ray photons from a double-multiplayer monochromator was 8–40 keV,and the white beam mode was provided on the beamline for dynamic X-ray imaging and dynamic X-ray micro-CT.While maintaining the previous experimental setup of BL13W1,new equipment was added to the beamline experimental station.The beamline is equipped with different sets of X-ray imaging detectors for several experimental methods such as micro-CT,dynamic micro-CT,and pair distribution function.The experimental station of BL13HB is designed specifically for various in situ dynamic experiments,and BL13HB has been open to users since June 2021.
基金The authors would like to thank Dr.Na Wang and Sai-Ke Tian in IHEP for their useful discussions.
文摘New-generation synchrotron light sources are being designed and operated worldwide to provide brighter radiation by reducing the beam emittance to X-ray diffraction limits.Intra-beam scattering(IBS)and Touschek scattering in such facilities are significant and require attention because of their ultra-low emittance.Therefore,cure strategies need to be carefully studied to obtain highquality photon beams.For the Shanghai Synchrotron Radiation Facility Upgrade(SSRF-U),a candidate lattice of the storage ring,reaching the soft X-ray diffraction limit,was designed and presented for the first time in this study.The emittance growth and beam lifetime in the SSRF-U storage ring were studied using particle simulations for a series of different machine configurations.The gains with RF frequencies of 100 MHz and 500 MHz were compared.Along with a better filling pattern,a more suitable RF frequency was adopted in the SSRF-U.The variations in the equilibrium beam emittance with beam coupling and bunch-lengthening were identified using simulations.Optimal beam coupling and required bunch-lengthening for the SSRF-U storage ring were thus determined.The fitness of the beam energy in the SSRF-U was subsequently assessed using the obtained parameters.Additionally,the Touschek scattering and beam lifetime were calculated,and an acceptable total beam lifetime was obtained.
基金supported by the Key Program of Shanghai Science and Technology Innovation Center(No.1174000565)。
文摘The lattice of the Shanghai Synchrotron Radiation Facility(SSRF) storage ring was upgraded in the Phase-II beamline project, and thus far, 18 insertion devices(IDs) have been installed. The IDs cause closed-orbit distortions, tune drift, and coupling distortions in the SSRF storage ring, all of which are significant issues that require solutions. In this study, an ID orbit feedforward compensation system based on a response matrix using corrector coils was developed, and it was applied to all commissioned IDs in the SSRF storage ring. After correction, the maximum ID-induced horizontal and vertical orbit distortions were less than 5.0 and 3.5 μm, respectively. Some interesting phenomena observed during the measurement process were explained. Additionally, optical and coupling feedforward systems were developed using quadrupole and skew quadrupole magnets installed on the front and back of elliptically polarizing undulators(EPUs). Moreover, over nearly four months of operation, the developed strategy delivered a satisfactory performance in the SSRF storage ring.
基金the National Natural Science Foundation of China(Nos.U1832215 and U1832144)the Youth Innovation Promotion Association of Chinese Academy Science(No.2017319).
文摘The BL19U2 at the Shanghai Synchrotron Radiation Facility is a small-angle X-ray scattering beamline dedicated to structural studies pertaining to biological macromolecules in solution.The beamline has been officially opened to users in March 2015,and since then,a series of technological innovations has been developed to optimize beamline performance,thereby significantly improving the data collection efficiency and broadening the application scope of biological small-angle X-ray scattering.BL19U2 is ideal for the high-throughput screening of weakly scattered proteins,protein assemblies,nucleic acids,inorganic nanomaterials,and organic drug molecules.This paper describes the design and overview of the BL19U2 beamline.Versatile sample environments at the experimental station and some recent scientific highlights are presented.
