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Microstructure and Properties of W-15Cu Alloys Prepared by Mechanical Alloying and Spark Plasma Sintering Process 被引量:2
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作者 章桥新 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2008年第3期399-402,共4页
W-15Cu composite powders prepared by mechanical alloying (MA) of raw powders were consolidated by spark plasma sintering (SPS) process at temperature ranged 1 230-1 300 ℃ for 10 min and under a pressure of 30 MPa... W-15Cu composite powders prepared by mechanical alloying (MA) of raw powders were consolidated by spark plasma sintering (SPS) process at temperature ranged 1 230-1 300 ℃ for 10 min and under a pressure of 30 MPa. By using high energy milling, particles containing very fine tungsten grains embedded in copper, called composite particles, could be produced. The W grains were homogeneously dispersed in copper phase, which was very important to obtain W-Cu alloy with high mechanical properties, fine and homogeneous microstructure. The microstructure and properties of W-15Cu alloys prepared by SPS processes at different temperature were researched. The results show that W-15Cu alloys consolidated by SPS can reach 99.6 % relative density, and transverse rupture strength (TRS) is 1 400.9 MPa, Rockwell C hardness (HRC) is 45.2, the thermal conductivity is 196 W/m-K at room temperature, the average grain size is less than 2 μm, and W-15Cu alloy with excellent properties, homogeneous and fine microstructure is obtained. 展开更多
关键词 w-15cu mechanical alloying spark plasma sintering (SPS)
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Effects of Activated Sintering Process on Properties and Microstructure of W-15Cu Alloy
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作者 史晓亮 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2010年第6期909-913,共5页
The effects of activated sintering technology of H2 atmosphere sintering on the microstructure and properties of W-15Cu alloy using ultrafine W-15Cu composite powder fabricated by spray drying calcining-continuous red... The effects of activated sintering technology of H2 atmosphere sintering on the microstructure and properties of W-15Cu alloy using ultrafine W-15Cu composite powder fabricated by spray drying calcining-continuous reduction technology were investigated.The experimental results showed that W-15Cu alloy,consolidated by activated sintering technology of H2 atmosphere sintering for 1 h at 1300 ℃,with 98.5 % relative density,transverse rupture strength 1218 MPa,Vickers hardness HV0.5 378,average grain size about 1.2 μm and thermal conductivity 192 W/m·K,was obtained.In comparison to the normal sintering process,activated sintering process to W-15Cu alloy could be achieved at lower sintering temperature.Furthermore,better properties in activated sintered compacts were obtained,and activated sintering process resulted in finer microstructure and excellent properties. 展开更多
关键词 ultrafine composite powder w-15cu alloy activated sintering process MICROSTRUCTURE PROPERTIES
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W-15Cu合金制备中钨骨架孔隙控制的研究 被引量:6
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作者 姜国圣 王志法 吴泓 《粉末冶金技术》 EI CAS CSCD 北大核心 2007年第2期126-128,144,共4页
钨铜复合材料是由高温烧结钨骨架经渗铜制成的两相假合金,钨骨架中的孔隙形态和大小将直接影响材料的性能。本文分别以添加硬脂酸和诱导铜的方法对钨粉进行处理,W-15Cu骨架孔隙在压制成形过程中得到了精确控制,钨骨架经熔渗后制成W-15C... 钨铜复合材料是由高温烧结钨骨架经渗铜制成的两相假合金,钨骨架中的孔隙形态和大小将直接影响材料的性能。本文分别以添加硬脂酸和诱导铜的方法对钨粉进行处理,W-15Cu骨架孔隙在压制成形过程中得到了精确控制,钨骨架经熔渗后制成W-15Cu合金。用扫描电镜观察材料的显微结构,并测出材料的密度、气密性,研究了钨粉成形性与钨铜合金密度的关系。结果表明,添加硬脂酸和诱导铜不会带入杂质,能改善钨粉的成形性能,可以获得组织均匀、致密度高的W-15Cu复合材料。 展开更多
关键词 w-15cu合金 钨骨架 成形性能 孔隙度 致密度
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钨粉粒径对W-15Cu导热性能的影响 被引量:9
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作者 陈德欣 王志法 +1 位作者 张行健 张瑾瑾 《稀有金属与硬质合金》 CAS CSCD 2005年第2期16-18,共3页
采用不同粒径的钨粉,用熔渗法制取钨铜两相假合金,分别测量其热导率,并在扫描电镜下观察熔渗后铜网络的分布,分析了钨粉粒径的大小对W-15Cu烧结行为的影响及其导热性能的影响。
关键词 w-15cu 钨粉粒径 热导率
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熔体保温和超声振动对Al-Cu-Mn合金组织与性能的协同作用 被引量:1
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作者 张天阳 方晓刚 +4 位作者 原紫云 张迪 黄中月 严峰 祖方遒 《铸造》 CAS 2024年第8期1109-1115,共7页
含特定Cu/Mn比的铝合金能够形成稳定的二十面体准晶相(I-Al_(65)Cu_(20)Mn_(15)),但是在常规凝固组织中准晶含量较低且尺寸粗大。本文以Al-Cu-Mn准晶合金为研究对象,研究在准晶I相形成温度区间进行熔体保温和超声振动对I相形貌与尺寸的... 含特定Cu/Mn比的铝合金能够形成稳定的二十面体准晶相(I-Al_(65)Cu_(20)Mn_(15)),但是在常规凝固组织中准晶含量较低且尺寸粗大。本文以Al-Cu-Mn准晶合金为研究对象,研究在准晶I相形成温度区间进行熔体保温和超声振动对I相形貌与尺寸的影响规律。结果表明,随着熔体保温时间的延长,准晶I相尺寸呈先减小后增大的趋势,特别是保温时间为20 min时,准晶颗粒呈细小的花瓣状;对保温20 min后的合金熔体施加600 W功率的超声振动,准晶尺寸发生细化,但继续增大功率会导致I相粗化。 展开更多
关键词 AL-cu-MN合金 Al_(65)cu_(20)Mn_(15)准晶 熔体保温 超声振动
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Microwave Sintering of W-15Cu Ultrafine Composite Powder Prepared by Spray Drying & Calcining-continuous Reduction Technology
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作者 舒敬萍 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2011年第2期281-284,共4页
The effects of microwave sintering and conventional H2 sintering on the microstructure and properties of W-15Cu alloy using ultrafine W-15Cu composite powder fabricated by spray drying & calcining-continuous reductio... The effects of microwave sintering and conventional H2 sintering on the microstructure and properties of W-15Cu alloy using ultrafine W-15Cu composite powder fabricated by spray drying & calcining-continuous reduction technology were investigated. In comparison to the conventional HE sintering processing, microwave sintering to W-15Cu can be achieved at lower sintering temperature and shorter sintering time. Furthermore, higher performances in microwave sintered compacts were obtained, but high microwave sintering temperature or long microwave sintering time could result in coarser microstructures. 展开更多
关键词 w-15cu ultrafine composite powder spray drying calcining continuous reduction microwave sintering
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时效对Cu-2.0Ni-0.5Si-0.15Ag合金组织和性能的影响 被引量:2
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作者 张毅 刘平 +2 位作者 田保红 陈小红 贾淑果 《金属热处理》 CAS CSCD 北大核心 2008年第8期120-123,共4页
研究了时效温度和时效时间对不同冷变形条件下Cu-2.0Ni-0.5Si-0.15Ag合金组织和性能的影响。结果表明,Cu-2.0Ni-0.5Si-0.15Ag合金经900℃×1h固溶处理和不同预冷变形,在450℃和500℃时效处理,第二相呈弥散分布,能获得较高的显微硬... 研究了时效温度和时效时间对不同冷变形条件下Cu-2.0Ni-0.5Si-0.15Ag合金组织和性能的影响。结果表明,Cu-2.0Ni-0.5Si-0.15Ag合金经900℃×1h固溶处理和不同预冷变形,在450℃和500℃时效处理,第二相呈弥散分布,能获得较高的显微硬度与导电率,析出相为Ni2Si相。当变形量为80%、时效温度达到500℃时,其显微硬度达到252HV0.1,导电率达到45%IACS;合金经40%变形、450℃×4h时效处理后,其抗拉强度达到680MPa。 展开更多
关键词 cu-2.0Ni-0.5Si-0.15Ag合金 时效 冷变形 显微硬度 导电率
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Effect of ageing temperature on precipitation of A1-Cu-Li-Mn-Zr alloy 被引量:4
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作者 DENG Yan-jun HUANG Guang-jie +2 位作者 CAO Ling-fei WU Xiao-dong HUANG Li 《Journal of Central South University》 SCIE EI CAS CSCD 2018年第6期1340-1349,共10页
The precipitation behaviors of an A1-Cu-Li-Mn-Zr alloy at different ageing temperatures (120, 160 and 200 ~C) were investigated using Vickers hardness measurements and transmission electron microscopy (TEM) charac... The precipitation behaviors of an A1-Cu-Li-Mn-Zr alloy at different ageing temperatures (120, 160 and 200 ~C) were investigated using Vickers hardness measurements and transmission electron microscopy (TEM) characterization. Age hardening curves show an increase in precipitation kinetics with increasing ageing temperature. The results of TEM show that for the samples peak aged at 120 ~C, the amount of g' (A13Li), GP zones/0' (A12Cu) and Z (A15Cu6Li2) phases is obviously higher than that of T1 (A12CuLi) precipitates; while the samples peak aged at 160 and 200 ~C are usually dominated by T1 phase with a minor fraction of GP zones/0' and g', and the Z phase almost does not form. In addition, quantitative analysis on the T1 platelets demonstrates that the samples peak aged at 200 ~C have larger plate diameter and smaller area fraction of T1, as compared to the samples peak aged at 160 ~C. Correspondingly, the possible reasons for such phenomena are discussed. 展开更多
关键词 ageing temperature PRECIPITATION A1-cu-Li-Mn-Zr alloy T1 phase Z (A15cu6Li2) phase
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Estimation of thermal expansion properties of quasicrystalline alloys
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作者 齐育红 张占平 黑祖昆 《中国有色金属学会会刊:英文版》 CSCD 2004年第1期152-155,共4页
By investigating the thermal expansion properties of three quasicrystalline alloys Al 65 Cu 20 Cr 15 quenched, Al 65 Cu 20 Cr 15 cast and Al 65 Cu 20 Fe 15 cast particles reinforced Al matrix composites from 25 ℃ to ... By investigating the thermal expansion properties of three quasicrystalline alloys Al 65 Cu 20 Cr 15 quenched, Al 65 Cu 20 Cr 15 cast and Al 65 Cu 20 Fe 15 cast particles reinforced Al matrix composites from 25 ℃ to 500 ℃, the thermal expansion coefficients of three quasicrystalline alloys were theoretically estimated. The results show that the thermal expansion coefficients of the composites are much lower than that of pure Al, and the thermal expansion coefficients of the composites reinforced by Al Cu Cr quasicrystalline particles are lower than those of the composites reinforced by Al Cu Fe quasicrystalline particles. According to estimating, quasicrystalline alloys have negative thermal expansion coefficients, and the thermal expansion coefficients of Al Cu Cr quasicrystalline alloys are lower than those of Al Cu Fe quasicrystalline alloys. In the alloys, the more the qusicrystalline content, the lower the thermal expansion coefficient. 展开更多
关键词 Al-cu-Cr合金 准晶 热膨胀系数 热分析 铝合金
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化学镀和粉末冶金法制备W-15Cu复合材料及性能研究(英文) 被引量:2
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作者 罗来马 谭晓月 +4 位作者 卢泽龙 罗广南 昝祥 程继贵 吴玉程 《稀有金属材料与工程》 SCIE EI CAS CSCD 北大核心 2015年第12期3005-3008,共4页
用化学镀和粉末冶金的方法制备出W-15Cu复合材料。首先用化学方法对W粉表面预处理,然后在其表面化学镀铜。得到的复合粉末用图谱进行表征。发现用化学镀的方法制备出的W-15Cu复合粉末纯度非常高,且W颗粒均匀、被Cu致密的包覆着。呈现出... 用化学镀和粉末冶金的方法制备出W-15Cu复合材料。首先用化学方法对W粉表面预处理,然后在其表面化学镀铜。得到的复合粉末用图谱进行表征。发现用化学镀的方法制备出的W-15Cu复合粉末纯度非常高,且W颗粒均匀、被Cu致密的包覆着。呈现出包状结构。这种复合粉末表现出优异的压制性能,压坯分别在300,400,500,600 MPa的压制压力下成形。压坯在1250℃温度下保温90min烧结后,从其断口形貌可以发现W颗粒没有明显的长大,且W颗粒表面特征并没有发生改变,仍然表现出预处理后的表面特征。对烧结体的相对密度、硬度、抗弯强度和电导率同样进行了表征。 展开更多
关键词 w-15cu复合材料 化学镀 显微结构
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Microstructures, mechanical properties, and grease-lubricated sliding wear behavior of Cu–15Ni–8Sn–0.8Nb alloy with high strength and toughness 被引量:2
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作者 Jinjuan CHENG Mincong MAO +3 位作者 Xueping GAN Qian LEI Zhou LI Kechao ZHOU 《Friction》 SCIE EI CAS CSCD 2021年第5期1061-1076,共16页
Alloys used as bearings in aircraft landing gear are required to reduce friction and wear as well as improve the load‐carrying capability due to the increased aircraft weights.Cu–15Ni–8Sn–0.8Nb alloy is well known... Alloys used as bearings in aircraft landing gear are required to reduce friction and wear as well as improve the load‐carrying capability due to the increased aircraft weights.Cu–15Ni–8Sn–0.8Nb alloy is well known for possessing good mechanical and wear properties that satisfy such requirements.In this study,the microstructure,mechanical properties,and grease‐lubricated sliding wear behavior of Cu–15Ni–8Sn–0.8Nb alloy with 0.8 wt%Nb are investigated.The nanoscale NbNi3 and NbNi2Sn compounds can strengthen the alloy through the Orowan strengthening mechanism.A Stribeck‐like curve is plotted to illustrate the relationship among friction coefficient,normal load,and sliding velocity and to analyze the grease‐lubricated mechanism.The wear rate increases with normal load and decreases with sliding velocity,except at 2.58 m/s.A wear mechanism map has been developed to exhibit the dominant wear mechanisms under various friction conditions.When the normal load is 700 N and the sliding velocity is 2.58 m/s,a chemical reaction between the lubricating grease and friction pairs occurs,resulting in the failure of lubricating grease and an increase in wear. 展开更多
关键词 cu15Ni–8Sn–0.8Nb alloy MICROSTRUCTURE mechanical properties grease‐lubricated wear behavior
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高Zr含量Cu-1.0%Zr-0.15%Y合金高温变形行为 被引量:1
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作者 田卡 田保红 +2 位作者 刘勇 张毅 宋克兴 《稀有金属材料与工程》 SCIE EI CAS CSCD 北大核心 2018年第4期1143-1148,共6页
利用Gleeble-1500D热模拟试验机对Cu-1.0%Zr-0.15%Y合金进行等温热压缩实验。分析了合金变形温度为550~900℃,应变速率为0.001~10 s^(-1)条件下的真应力-真应变特征、热压缩过程中的组织演变和热变形机制。结果表明:在550~750℃时具有... 利用Gleeble-1500D热模拟试验机对Cu-1.0%Zr-0.15%Y合金进行等温热压缩实验。分析了合金变形温度为550~900℃,应变速率为0.001~10 s^(-1)条件下的真应力-真应变特征、热压缩过程中的组织演变和热变形机制。结果表明:在550~750℃时具有典型的动态回复特征,在850~900℃时具有动态再结晶热变形特征。变形温度和应变速率对Cu-1.0%Zr-0.15%Y合金有显著影响。在真应力-真应变曲线的基础上,建立等温压缩变形过程中的流变应力与应变速率和变形温度之间的本构方程,得到合金的热变形激活能Q为379.16 kJ/mol,与纯铜相比,高Zr含量Cu-1.0%Zr-0.15%Y合金热变形激活能提高了81%。添加稀土元素Y,可以细化Cu-Zr合金晶粒,促进动态结晶。 展开更多
关键词 高Zr含量 cu-1.0%Zr-0.15%Y合金 高温变形 本构方程 动态再结晶
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