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In-flight Energy Calibration of the GECAM Gamma-ray Detectors
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作者 Rui Qiao Dong-Ya Guo +27 位作者 Wen-Xi Peng Yan-Qiu Zhang Shuo Xiao Shao-Lin Xiong Chao Zheng Chao-Yang Li Jia-Cong Liu Wang-Chen Xue Jian-Jian He Zheng-Hua An Da-Li Zhang Xin-Qiao Li Li-Ming Song Shi-Jie Zheng Ke Gong Ya-Qing Liu Xin-Ying Song Xiao-Yun Zhao Xiang-Yang Wen Yan-Bing Xu Xiang Ma Xiao-Bo Li Ping Wang Yue Huang Ce Cai Qi-Bin Yi Yi Zhao Chen-Wei Wang 《Research in Astronomy and Astrophysics》 SCIE CAS CSCD 2024年第10期48-57,共10页
The Gravitational wave high-energy Electromagnetic Counterpart All-sky Monitor(GECAM)mission is designed to monitor the Gamma-Ray Bursts(GRBs)associated with gravitational waves and other high-energy transient sources... The Gravitational wave high-energy Electromagnetic Counterpart All-sky Monitor(GECAM)mission is designed to monitor the Gamma-Ray Bursts(GRBs)associated with gravitational waves and other high-energy transient sources.The mission consists of two microsatellites which are planned to operate at the opposite sides of the Earth.Each GECAM satellite could detect and localize GRBs in about 8 keV-5 MeV with its 25 Gamma-Ray Detectors(GRDs).In this work,we report the in-flight energy calibration of GRDs using the characteristic gamma-ray lines in the background spectra,and show their performance evolution during the commissioning phase.Besides,a preliminary cross-calibration of energy response with Fermi GBM data is also presented,validating the energy response of GRDs. 展开更多
关键词 (stars:)gamma-ray burst:general instrumentation:detectors methods:data analysis
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Electrode Design of Cylindrical Coplanar-grid CdZnTe Detector by Finite Element Methods 被引量:1
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作者 JINWei SANGWen-bin ZHANGQi MINJia-Hua SHENYan 《Semiconductor Photonics and Technology》 CAS 2004年第1期48-52,共5页
Cylindrical coplanar-grid configurations,which offer a lot of advantages over established designs,can effectively overcome the problem of poor hole collection.Finite element analysis is utilized for simulating the pot... Cylindrical coplanar-grid configurations,which offer a lot of advantages over established designs,can effectively overcome the problem of poor hole collection.Finite element analysis is utilized for simulating the potential distribution of the cylindrical coplanar-grid detector under different models by varying the widths of grid and pitch of electrodes. In addition, a modified grid pattern has been discussed to improve the weighting potential match between two grids. In this way, the geometry of electrodes for cylindrical coplanar-grid detectors is optimized. 展开更多
关键词 CDZNTE Finite Element methods Coplanar-grid detector
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Optical fiber positioning based on four-quadrant detector with Gaussian fitting method 被引量:3
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作者 Jin-Sheng Liu Hua Zou +1 位作者 Mei-Ling Zhang Lin-Zheng Wang 《Research in Astronomy and Astrophysics》 SCIE CAS CSCD 2017年第7期115-120,共6页
With the development of large-scale spectral surveys, fiber positioning technology has been developing rapidly. Because of the performance advantages of a four-quadrant(4Q) detector, a fiber positioning and real-tim... With the development of large-scale spectral surveys, fiber positioning technology has been developing rapidly. Because of the performance advantages of a four-quadrant(4Q) detector, a fiber positioning and real-time monitoring system based on the 4Q detector is proposed. The detection accuracy of this system is directly determined by the precision of the center of the spot. A Gaussian fitting algorithm based on the 4Q detector is studied and applied in the fiber positioning process to improve the calculated accuracy of the spot center. The relationship between the center position of the incident spot and the detector output signal is deduced. An experimental platform is built to complete the simulated experiment. Then we use the Gaussian fitting method to process experimental data, compare the fitting value with the theoretical one and calculate the corresponding error. 展开更多
关键词 INSTRUMENTATION detectors - methods data analysis - techniques imaging spectroscopy- telescopes
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A novel method for gamma spectrum analysis of low-level and intermediate-level radioactive waste 被引量:2
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作者 Hui Yang Xin-Yu Zhang +4 位作者 Wei-Guo Gu Bing Dong Xue-Zhi Jiang Wen-Tao Zhou De-Zhong Wang 《Nuclear Science and Techniques》 SCIE EI CAS CSCD 2023年第6期199-213,共15页
The uncertainty of nuclide libraries in the analysis of the gamma spectra of low-and intermediate-level radioactive waste(LILW)using existing methods produces unstable results.To address this problem,a novel spectral ... The uncertainty of nuclide libraries in the analysis of the gamma spectra of low-and intermediate-level radioactive waste(LILW)using existing methods produces unstable results.To address this problem,a novel spectral analysis method is proposed in this study.In this method,overlapping peaks are located using a continuous wavelet transform.An improved quadratic convolution method is proposed to calculate the widths of the peaks and establish a fourth-order filter model to estimate the Compton edge baseline with the overlapping peaks.Combined with the adaptive sensitive nonlinear iterative peak,this method can effectively subtracts the background.Finally,a function describing the peak shape as a filter is used to deconvolve the energy spectrum to achieve accurate qualitative and quantitative analyses of the nuclide without the aid of a nuclide library.Gamma spectrum acquisition experiments for standard point sources of Cs-137 and Eu-152,a segmented gamma scanning experiment for a 200 L standard drum,and a Monte Carlo simulation experiment for triple overlapping peaks using the closest energy of three typical LILW nuclides(Sb-125,Sb-124,and Cs-134)are conducted.The results of the experiments indicate that(1)the novel method and gamma vision(GV)with an accurate nuclide library have the same spectral analysis capability,and the peak area calculation error is less than 4%;(2)compared with the GV,the analysis results of the novel method are more stable;(3)the novel method can be applied to the activity measurement of LILW,and the error of the activity reconstruction at the equivalent radius is 2.4%;and(4)The proposed novel method can quantitatively analyze all nuclides in LILW without a nuclide library.This novel method can improve the accuracy and precision of LILW measurements,provide key technical support for the reasonable disposal of LILW,and ensure the safety of humans and the environment. 展开更多
关键词 HPGe detector Low-level and intermediate-level radioactive waste Gamma spectrum analysis method Deconvolution method Continuous wavelet transform
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CsI-bowl:an ancillary detector for exit channel selection inγ-ray spectroscopy experiments 被引量:1
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作者 Xing-Chi Han Shuo Wang +5 位作者 Hong-Yi Wu Zhi-Huan Li Guo-Zhu Shi Ruo-Fu Chen Yue-Zhao Zhang Shou-Yu Wang 《Nuclear Science and Techniques》 SCIE EI CAS CSCD 2023年第9期32-39,共8页
A particle detector array designed for light-charged particles, known as the CsI-bowl, was built for exit channel selection for in-beam γ-ray spectroscopy experiments. This device is composed of 64 CsI(Tl) detectors,... A particle detector array designed for light-charged particles, known as the CsI-bowl, was built for exit channel selection for in-beam γ-ray spectroscopy experiments. This device is composed of 64 CsI(Tl) detectors, organized in a structure reminiscent of a tea-bowl. High quantum efficiency photodiodes, characterized by their minimal mass, were employed to collect scintillation light. Its design, construction, particle identification resolution, and its effectiveness in relation to exit channel selection are described in this paper. In source tests, the optimal figure of merit for the identification of α-particles and γ-rays using the charge comparison method was found to be 3.3 and 12.1 for CsI detectors coupled to photodiodes and avalanche photodiodes, respectively. The CsI-bowl demonstrated effectiveness in identifying particles, specifically the emission of protons and α-particles in the58Ni(19F, xpyn) fusion–evaporation reaction, thereby enabling the selection of the desired exit channels. 展开更多
关键词 Light charged particle detector array Particle identification Charge comparison method
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乡村振兴背景下脱贫山区乡村韧性演变及影响因素--以陕南秦巴山区为例 被引量:1
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作者 白玉玲 陈佳 +2 位作者 尹莎 李润阳 杨新军 《生态学报》 CAS CSCD 北大核心 2024年第19期8798-8811,共14页
探究乡村振兴背景下乡村韧性动态演变及影响因素,对于脱贫山区推进乡村全面振兴与实现乡村可持续发展具有重要意义。陕南秦巴山区受脆弱生态环境以及薄弱经济基础的双重胁迫,脱贫乡村发展与农户生计仍面临不确定性风险。以陕南秦巴山区2... 探究乡村振兴背景下乡村韧性动态演变及影响因素,对于脱贫山区推进乡村全面振兴与实现乡村可持续发展具有重要意义。陕南秦巴山区受脆弱生态环境以及薄弱经济基础的双重胁迫,脱贫乡村发展与农户生计仍面临不确定性风险。以陕南秦巴山区28个县区为例,将乡村韧性分解为经济、社会、生态以及制度四个维度,构建乡村韧性指标体系并对其进行量化,运用GIS技术和地理探测器探究乡村韧性的时空演变及影响因素。结果显示:(1)陕南秦巴山区2010—2021年乡村韧性整体呈先下降后上升的趋势。社会韧性与经济韧性变化较小,制度韧性逐年上升,生态韧性逐年下降。(2)近10年土地资源利用、文化教育等是乡村韧性分异的主导因子,且制约因子由生态维度转向社会维度,乡村基础教育与农业生产效率影响程度不断加深,土地利用与人口结构的作用不断减弱。(3)依据研究区乡村振兴背景下面临的现实问题,针对各县区乡村韧性提升的短板和关键影响因子,从产业、人才、组织、文化、生态五大振兴出发提出了脱贫山区韧性提升的建设路径及对策。乡村产业振兴方面应打造新兴产业集群,提升农业现代化水平;乡村人才振兴方面应开展农户就业扶持活动,政策吸引人才返乡下乡;乡村文化振兴方面应推进教育新型基础设施建设,建立农民群众文化需求反馈机制;乡村生态振兴方面应优化农业生产结构和区域布局,盘活耕地资源促进绿色生产;乡村组织振兴方面应探索多元组织协作,全面建立健全村务监督委员会,为未来脱贫山区韧性建设提供了参考依据。 展开更多
关键词 乡村振兴 乡村韧性 陕南秦巴山区 地理探测器 变化斜率法
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Calibration and Unfolding of the Pulse Height Spectra of Liquid Scintillator-Based Neutron Detectors Using Photon Sources 被引量:4
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作者 谢旭飞 袁熙 +3 位作者 张兴 樊铁栓 陈金象 李湘庆 《Plasma Science and Technology》 SCIE EI CAS CSCD 2012年第6期553-557,共5页
An accurate energy calibration of a 5"× 2" BC501A liquid scintillator-based neutron detector by means of photon sources and the unfolding of pulse height spectra are described. The photon responses were measure... An accurate energy calibration of a 5"× 2" BC501A liquid scintillator-based neutron detector by means of photon sources and the unfolding of pulse height spectra are described. The photon responses were measured with 22Na, 137Cs and 54Mn photon sources and simulated using the GRESP code, which was developed at the Physiknlisch Technische Bundesanstalt in Germany. Pulse height spectra produced by three different photon sources were employed to investigate the effects of the unfolding techniques. It was found that the four unfolding codes of the HEPRO and UMG3.3 packages, including GRAVEL, UNFANA, MIEKE and MAXED, performed well with the test spectra and produced generally consistent results. They could therefore be used to obtain neutron energy spectra in toknmak experiments. 展开更多
关键词 liquid scintillation detector CALIBRATION pulse height spectra unfolding methods
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Reformatted method for two-dimensional detector arrays measurement data in proton pencil beam scanning 被引量:2
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作者 Meng-Ya Guo Xiu-Fang Li +6 位作者 Jie Wang Qi Liu Xiu-Zhen Deng Man-Zhou Zhang Li-Ren Shen Yue-Hu Pu Zhi-Ling Chen 《Nuclear Science and Techniques》 SCIE EI CAS CSCD 2021年第6期83-93,共11页
The spatial resolution of a commercial two-dimensional(2D)ionization chamber(IC)array is limited by the size of the individual detector and the center-to-center distance between sensors.For dose distributions with are... The spatial resolution of a commercial two-dimensional(2D)ionization chamber(IC)array is limited by the size of the individual detector and the center-to-center distance between sensors.For dose distributions with areas of steep dose gradients,inter-detector dose values are derived by the interpolation of nearby detector readings in the conventional mathematical interpolation of 2D IC array measurements.This may introduce significant errors,particularly in proton spot scanning radiotherapy.In this study,by combining logfile-based reconstructed dose values and detector measurements with the Laplacian pyramid image blending method,a novel method is proposed to obtain a reformatted dose distribution that provides an improved estimation of the delivered dose distribution with high spatial resolution.Meanwhile,the similarity between the measured original data and the downsampled logfilebased reconstructed dose is regarded as the confidence of the reformatted dose distribution.Furthermore,we quantify the performance benefits of this new approach by directly comparing the reformatted dose distributions with 2D IC array detector mathematically interpolated measurements and original low-resolution measurements.The result shows that this new method is better than the mathematical interpolation and achieves gamma pass rates similar to those of the original low-resolution measurements.The reformatted dose distributions generally yield a confidence exceeding 95%. 展开更多
关键词 2D ion chamber array detectors Laplacian pyramid image blending High-resolution reformatted methods Pencil beam scanning Proton therapy
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基于D-D源的三探头中子孔隙度测井探测响应分析
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作者 周悦 王猛 +2 位作者 刘海波 尚修盛 刘志杰 《测井技术》 CAS 2024年第5期595-601,共7页
随着油气勘探进程持续推进,低孔隙度储层越发受到关注,具备更高孔隙度灵敏度的D-D源中子测井存在良好应用前景,为了进一步探索其兼顾中子孔隙度测量灵敏度与化学源测量兼容性的可能性,提出一种基于D-D源的三探头中子孔隙度测井设计并开... 随着油气勘探进程持续推进,低孔隙度储层越发受到关注,具备更高孔隙度灵敏度的D-D源中子测井存在良好应用前景,为了进一步探索其兼顾中子孔隙度测量灵敏度与化学源测量兼容性的可能性,提出一种基于D-D源的三探头中子孔隙度测井设计并开展分析。为探究D-D源中子孔隙度测量响应特征,利用蒙特卡罗方法,基于三探头测井仪器的基本构成,研究了探测器源距设计,并提出利用测量的近远热中子计数比、中远热中子计数比这2组比值分别表征地层孔隙度,同时对D-D源中子孔隙度测井的地层探测能力与地层测量响应进行了综合分析。研究表明:三探头D-D源中子孔隙度测井仪器探测深度稍浅、纵向分辨率较高;近远热中子计数比值响应表现出更高地层孔隙度灵敏度,低孔隙度地层情况下测得的孔隙度变化效果良好;中远热中子计数比值响应泥岩效应较强,虽无法与化学源测量结果兼容,但在纯岩性及含泥质地层与其较高程度接近。该文研究为D-D源中子孔隙度测井仪器测量应用提供了一定参考。 展开更多
关键词 D-D源 中子孔隙度测井 三探头设计 近远热中子计数比值 中远热中子计数比值 蒙特卡罗方法
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A class of fully third-order accurate projection methods for solving the incompressible Navier-Stokes equations 被引量:2
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作者 Yuxin Ren Yuxi Jiang +1 位作者 Miao'er Liu Hanxin Zhang 《Acta Mechanica Sinica》 SCIE EI CAS CSCD 2005年第6期542-549,共8页
In this paper, a fully third-order accurate projection method for solving the incompressible Navier-Stokes equations is proposed. To construct the scheme, a continuous projection procedure is firstly presented. We the... In this paper, a fully third-order accurate projection method for solving the incompressible Navier-Stokes equations is proposed. To construct the scheme, a continuous projection procedure is firstly presented. We then derive a sufficient condition for the continuous projection equations to be temporally third-order accurate approximations of the original Navier-Stokes equations by means of the localtruncation-error-analysis technique. The continuous projection equations are discretized temporally and spatially to third-order accuracy on the staggered grids, resulting in a fully third-order discrete projection scheme. The possibility to design higher-order projection methods is thus demonstrated in the present paper. A heuristic stability analysis is performed on this projection method showing the probability of its being stable. The stability of the present scheme is further verified through numerical tests. The third-order accuracy of the present projection method is validated by several numerical test cases. 展开更多
关键词 Incompressible Navier-Stokes equations Projection methods - Third-order scheme - Local truncation error
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The In-Flight Realtime Trigger and Localization Software of GECAM
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作者 Xiao-Yun Zhao Shao-Lin Xiong +86 位作者 Xiang-Yang Wen Xin-Qiao Li Ce Cai Shuo Xiao Qi Luo Wen-Xi Peng Dong-Ya Guo Zheng-Hua An Ke Gong Jin-Yuan Liao Yan-Qiu Zhang Yue Huang Lu Li Xing Wen Fei Zhang Jing Duan Chen-Wei Wang Dong-Li Shi Peng Zhang Qi-Bin Yi Chao-Yang Li Yan-Bing Xu Xiao-Hua Liang Ya-Qing Liu Da-Li Zhang Xi-Lei Sun Fan Zhang Gang Chen Huan-Yu Wang Sheng Yang Xiao-Jing Liu Min Gao Mao-Shun Li Jin-Zhou Wang Xing Zhou Yi Zhao Wang-Chen Xue Chao Zheng Jia-Cong Liu Xing-Bo Han Jin-Ling Qi Jia Huang Ke-Ke Zhang Can Chen Xiong-Tao Yang Dong-Jie Hou Yu-Sa Wang Rui Qiao Xiang Ma Xiao-Bo Li Ping Wang Xin-Ying Song Li-Ming Song Shi-Jie Zheng Bing Li Hong-Mei Zhang Yue Zhu Wei Chen Jian-Jian He Zhen Zhang Jin Hou Hong-Jun Wang Yan-Chao Hao Xiang-Yu Wang Zong-Yuan Yang Zhi-Long Wen Zhi Chang Yuan-Yuan Du Rui Gao Xiao-Fei Lan Yan-Guo Li Gang Li Xu-Fang Li Fang-Jun Lu Hong Lu Bin Meng Feng Shi Hui Wang Hui-Zhen Wang Yu-Peng Xu Jia-Wei Yang Xue-Juan Yang Shuang-Nan Zhang Chao-Yue Zhang Cheng-Mo Zhang Zhi-Cheng Tang Cheng Cheng 《Research in Astronomy and Astrophysics》 SCIE CAS CSCD 2024年第10期11-24,共14页
Realtime trigger and localization of bursts are the key functions of GECAM,an all-sky gamma-ray monitor launched on 2020 December 10.We developed a multifunctional trigger and localization software operating in the CP... Realtime trigger and localization of bursts are the key functions of GECAM,an all-sky gamma-ray monitor launched on 2020 December 10.We developed a multifunctional trigger and localization software operating in the CPU of the GECAM Electronic Box.This onboard software has the following features:high trigger efficiency for real celestial bursts with a suppression of false triggers caused by charged particle bursts and background fluctuation,dedicated localization algorithm optimized for both short and long bursts,and low time latency of the trigger information which is downlinked through the Global Short Message Communication service of the global BeiDou navigation system.This paper provides a detailed description of the design and development of the trigger and localization software system for GECAM.It covers the general design,workflow,the main functions,and the algorithms used in the system.The paper also includes on-ground trigger tests using simulated gamma-ray bursts generated by a dedicated X-ray tube,as well as an overview of the performance for real celestial bursts during its in-orbit operation. 展开更多
关键词 telescopes instrumentation:detectors methods:observational
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气相色谱-氮磷检测器法测定小麦粉及其制品与小麦粉添加剂中的乙酰氧肟酸 被引量:1
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作者 宁亚萍 武文凯 +3 位作者 石璐 刘璐 李彤辉 谷瑞丽 《粮食与油脂》 北大核心 2024年第3期148-153,共6页
建立了气相色谱-氮磷检测器法测定小麦粉及其制品与小麦粉添加剂中非法添加物乙酰氧肟酸(AHA)的分析方法。以小麦粉、小麦粉添加剂、面皮、面条、馒头为研究基质,优化了色谱条件,并通过向5种空白基质进行加标回收实验优化前处理方法。... 建立了气相色谱-氮磷检测器法测定小麦粉及其制品与小麦粉添加剂中非法添加物乙酰氧肟酸(AHA)的分析方法。以小麦粉、小麦粉添加剂、面皮、面条、馒头为研究基质,优化了色谱条件,并通过向5种空白基质进行加标回收实验优化前处理方法。样品经无水乙醇超声和涡旋振荡提取,高速离心、过滤,采用DB-WAX(60 m×0.32 mm,0.25μm)色谱柱分离,外标法定量。结果表明:AHA溶剂和基质标准曲线在0.60~10.00μg/mL范围内线性关系良好,相关系数均大于0.998,检出限为2 mg/kg,定量限为6 mg/kg;加标回收率为86.19%~109.22%,相对标准偏差(n=6)为1.47%~7.89%。方法适用于小麦粉及其制品与小麦粉添加剂中AHA的测定。 展开更多
关键词 小麦粉 乙酰氧肟酸 气相色谱-氮磷检测器法
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Reflectance conversion methods for the VIS/NIR imaging spectrometer aboard the Chang'E-3 lunar rover: based on ground validation experiment data
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作者 Bin Liu Jian-Zhong Liu +5 位作者 Guang-Liang Zhang Zong-Cheng Ling Jiang Zhang Zhi-Ping He Ben-Yong Yang Yong-Liao Zou 《Research in Astronomy and Astrophysics》 SCIE CAS CSCD 2013年第7期862-874,共13页
The second phase of the Chang'E Program (also named Chang'E-3) has the goal to land and perform in-situ detection on the lunar surface. A VIS/NIR imaging spectrometer (VNIS) will be carded on the Chang'E-3 luna... The second phase of the Chang'E Program (also named Chang'E-3) has the goal to land and perform in-situ detection on the lunar surface. A VIS/NIR imaging spectrometer (VNIS) will be carded on the Chang'E-3 lunar rover to detect the distri-bution of lunar minerals and resources. VNIS is the first mission in history to perform in-situ spectral measurement on the surface of the Moon, the reflectance data of which are fundamental for interpretation of lunar composition, whose quality would greatly affect the accuracy of lunar element and mineral determination. Until now, in-situ de-tection by imaging spectrometers was only performed by rovers on Mars. We firstly review reflectance conversion methods for rovers on Mars (Viking landers, Pathfinder and Mars Exploration rovers, etc). Secondly, we discuss whether these conversion methods used on Mars can be applied to lunar in-situ detection. We also applied data from a laboratory bidirectional reflectance distribution function (BRDF) using simu- lated lunar soil to test the availability of this method. Finally, we modify reflectance conversion methods used on Mars by considering differences between environments on the Moon and Mars and apply the methods to experimental data obtained from the ground validation of VNIS. These results were obtained by comparing reflectance data from the VNIS measured in the laboratory with those from a standard spectrometer obtained at the same time and under the same observing conditions. The shape and amplitude of the spectrum fits well, and the spectral uncertainty parameters for most samples are within 8%, except for the ilmenite sample which has a low albedo. In conclusion, our reflectance conversion method is suitable for lunar in-situ detection. 展开更多
关键词 instrumentation: detectors - lunar in-situ detection: VNIS - re-flectance conversion: BRDF
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Jacobi-Sobolev Orthogonal Polynomialsand Spectral Methods for Elliptic Boundary Value Problems
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作者 Xuhong Yu Zhongqing Wang Huiyuan Li 《Communications on Applied Mathematics and Computation》 2019年第2期283-308,共26页
Generalized Jacobi polynomials with indexes α,β∈ R are introduced and some basic properties are established. As examples of applications,the second- and fourth-order elliptic boundary value problems with Dirichlet ... Generalized Jacobi polynomials with indexes α,β∈ R are introduced and some basic properties are established. As examples of applications,the second- and fourth-order elliptic boundary value problems with Dirichlet or Robin boundary conditions are considered,and the generalized Jacobi spectral schemes are proposed. For the diagonalization of discrete systems,the Jacobi-Sobolev orthogonal basis functions are constructed,which allow the exact solutions and the approximate solutions to be represented in the forms of infinite and truncated Jacobi series. Error estimates are obtained and numerical results are provided to illustrate the effectiveness and the spectral accuracy. 展开更多
关键词 Generalized JACOBI POLYNOMIALS Spectral method - Jacobi-Sobolev ORTHOGONAL BASIS functions ELLIPTIC boundary value problems Error analysis
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不同炮制方法对巴戟天中耐斯糖和甲基异茜草素-1-甲醚含量的影响
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作者 柯颖川 卢海辉 陈继英 《广东药科大学学报》 CAS 2024年第4期48-52,共5页
目的挖掘古籍中的经典炮制方法,考察不同炮制方法对巴戟天中耐斯糖和甲基异茜草素-1-甲醚的质量分数的影响。方法采用高效液相色谱-蒸发光散射检测器(HPLC-ELSD)和高效液相色谱-二极管阵列检测法(HPLC-DAD)分别测定5种炮制方法巴戟天中... 目的挖掘古籍中的经典炮制方法,考察不同炮制方法对巴戟天中耐斯糖和甲基异茜草素-1-甲醚的质量分数的影响。方法采用高效液相色谱-蒸发光散射检测器(HPLC-ELSD)和高效液相色谱-二极管阵列检测法(HPLC-DAD)分别测定5种炮制方法巴戟天中耐斯糖和甲基异茜草素-1-甲醚的质量分数。结果不同炮制方法巴戟天中耐斯糖、甲基异茜草素-1-甲醚的质量分数明显不同:耐斯糖,米炒巴戟天>蒸制巴戟天>甘草制巴戟天>盐制巴戟天>古法巴戟天;甲基异茜草素-1-甲醚,盐制巴戟天>甘草制巴戟天>蒸制巴戟天>米炒巴戟天>古法巴戟天。结论不同炮制方法对巴戟天中耐斯糖以及甲基异茜草素-1-甲醚的质量分数影响较大,其中米炒巴戟天的耐斯糖质量分数较高,盐制巴戟天的甲基异茜草素-1-甲醚质量分数较高。 展开更多
关键词 巴戟天 炮制方法 耐斯糖 甲基异茜草素-1-甲醚 HPLC法 蒸发光散射检测法 二极管阵列检测法
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Soller slits automatic focusing method for multi-element fluorescence detector
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作者 Ya-Yun Yang Qian Gao +3 位作者 Song-Qi Gu Hai-Sheng Yu Rui-You Lu Yu-Ying Huang 《Nuclear Science and Techniques》 SCIE CAS CSCD 2016年第5期179-187,共9页
In X-ray absorption fine structure(XAFS) experiments,Soller slits are widely used as filter devices in order to improve the signal to noise ratio.Performing high accuracy manual focusing operations is a time-consuming... In X-ray absorption fine structure(XAFS) experiments,Soller slits are widely used as filter devices in order to improve the signal to noise ratio.Performing high accuracy manual focusing operations is a time-consuming process;therefore,this work introduces an automatic focusing method for Soller slits in multi-element fluorescence detectors.This method establishes a relation model between the fluorescence intensity distribution and the coordinates of the fluorescence excitation point.According to this relation model,the actual coordinates of the fluorescence excitation point can be deduced from the detected fluorescence intensity distribution and used in focusing operations.This method has proven to be feasible in an XAFS experiment at the BL14W1 beamline of the Shanghai Synchrotron Radiation Facility. 展开更多
关键词 荧光检测器 聚焦方法 狭缝 X射线吸收精细结构 XAFS实验 关系模型 光强度分布 高信噪比
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UPLC-DAD法测定人参再造丸中芦荟大黄素、大黄酸、大黄素、大黄酚、大黄素甲醚5种成分含量
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作者 曾静凯 汤逊尤 +3 位作者 黄晓燕 丁野 孙辉 李文莉 《药品评价》 CAS 2024年第3期286-289,共4页
目的 建立超高效液相色谱-二极管阵列检测器(UPLC-DAD)法测定人参再造丸中芦荟大黄素、大黄酸、大黄素、大黄酚、大黄素甲醚5种成分的含量。方法 采用Waters CORTECS UPLC C18色谱柱(2.1 mm×100 mm,1.6 μm);以甲醇-0.1%磷酸溶液... 目的 建立超高效液相色谱-二极管阵列检测器(UPLC-DAD)法测定人参再造丸中芦荟大黄素、大黄酸、大黄素、大黄酚、大黄素甲醚5种成分的含量。方法 采用Waters CORTECS UPLC C18色谱柱(2.1 mm×100 mm,1.6 μm);以甲醇-0.1%磷酸溶液为流动相,梯度洗脱,流速为0.3 mL/min;检测波长为437 nm;柱温40 ℃。结果 芦荟大黄素、大黄酸、大黄素、大黄酚、大黄素甲醚5种成分分离度良好,在相应范围内线性关系良好,相关系数(r)均不低于0.999 7,平均回收率分别为92.5%、83.5%、94.3%、98.9%、106.8%,RSD(n=6)分别为2.0%、1.2%、2.6%、2.4%、2.4%。结论 UPLC-DAD法准确可靠、重复性好,可用于人参再造丸的质量控制。 展开更多
关键词 人参再造丸 超高效液相色谱-二极管阵列检测器法 芦荟大黄素 大黄酸 大黄素 大黄酚 大黄素甲醚 含量测定
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Usefulness of an Anisotropic Diffusion Method in Cerebral CT Perfusion Study Using Multi-Detector Row CT
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作者 Kenya Murase Takafumi Nanjo +2 位作者 Yoshifumi Sugawara Masaaki Hirata Teruhito Mochizuki 《Open Journal of Medical Imaging》 2015年第3期106-116,共11页
Purpose: To present an application of the anisotropic diffusion (AD) method to improve the accuracy of the functional images of perfusion parameters such as cerebral blood flow (CBF), cerebral blood volume (CBV) and m... Purpose: To present an application of the anisotropic diffusion (AD) method to improve the accuracy of the functional images of perfusion parameters such as cerebral blood flow (CBF), cerebral blood volume (CBV) and mean transit time (MTT) generated from cerebral CT perfusion studies using multi-detector row CT (MDCT). Materials and Methods: Continuous scans (1 sec/rotation ×60 sec) consisting of four 5-mm-thick contiguous slices were acquired after an intravenous injection of iodinated contrast material in 6 patients with cerebrovascular disease using an MDCT scanner with a tube voltage of 80 kVp and a tube current of 200 mA. New image data were generated by thinning out the above original images at an interval of 2 sec or 3 sec. The thinned-out images were then interpolated by linear interpolation to generate the same number of images as originally acquired. The CBF, CBV and MTT images were generated using deconvolution analysis based on singular value decomposition. Results: When using the AD method, the correlation coefficient between the MTT values obtained from the original and thinned-out images was significantly improved. Furthermore, the coefficients of variation of the CBF, CBV and MTT values in the white matter significantly decreased as compared to not using the AD method. Conclusion: Our results suggest that the AD method is useful for improving the accuracy of the functional images of perfusion parameters and for reducing radiation exposure in cerebral CT perfusion studies using MDCT. 展开更多
关键词 ANISOTROPIC Diffusion method CEREBRAL CT PERFUSION STUDY Multi-detector Row CT Radiation Exposure
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HPGPC-RID法测定右旋糖酐20分子量及其分布的可行性研究
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作者 梁姗 王爱秀 +4 位作者 王靖睿 张锦波 李小娟 黄群惠 朱衍志 《现代医药卫生》 2024年第12期1981-1985,共5页
目的 建立高效凝胶渗透色谱-示差折光检测器(HPGPC-RID)测定右旋糖酐20分子量及其分布的方法,并对该方法进行可行性研究。方法 对新建方法进行专属性、准确度、重复性及耐用性验证,并评价新建方法与《中国药典》2020版(二部)收录方法检... 目的 建立高效凝胶渗透色谱-示差折光检测器(HPGPC-RID)测定右旋糖酐20分子量及其分布的方法,并对该方法进行可行性研究。方法 对新建方法进行专属性、准确度、重复性及耐用性验证,并评价新建方法与《中国药典》2020版(二部)收录方法检测结果的等效性。结果 新建方法专属性、准确度、重复性、耐用性良好,且与药典方法等效,可用于右旋糖酐20分子量及其分布的测定。与此同时,新建方法能避免药典方法中硫酸钠(Na_(2)SO_(4))峰对右旋糖酐20峰的干扰。结论 相比于药典方法,新建方法对右旋糖酐20分子量及其分布测定具有更好的适用性。 展开更多
关键词 高效凝胶渗透色谱-示差折光检测器 右旋糖酐20 分子量 分子量分布 等效性
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FITTING CORRECTION METHOD OF RING ARTIFACTS FOR RECONSTRUCTING CONE-BEAM CT IMAGES 被引量:1
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作者 罗守华 吴婧 +1 位作者 张波 陈功 《Transactions of Nanjing University of Aeronautics and Astronautics》 EI 2010年第1期34-38,共5页
In high-resolution cone-beam computed tomography (CBCT) using the flat-panel detector, imperfect or defect detector elements cause ring artifacts due to the none-uniformity of their X-ray response. They often distur... In high-resolution cone-beam computed tomography (CBCT) using the flat-panel detector, imperfect or defect detector elements cause ring artifacts due to the none-uniformity of their X-ray response. They often disturb the image quality. A dedicated fitting correction method for high-resolution micro-CT is presented. The method converts each elementary X-ray response curve to an average one, and eliminates response inconsistency among pixels. Other factors of the method are discussed, such as the correction factor variability by different sampling frames and nonlinear factors over the whole spectrum. Results show that the noise and artifacts are both reduced in reconstructed images 展开更多
关键词 image processing image reconstruction flat-panel detector fitting correction method
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