To indirectly investigate the dislocation behavior of Fe-36wt%Ni Invar alloy by the etch pit method,polished Invar specimens were etched by a solution containing 4 g copper sulfate,20 mL hydrochloric acid,and 20 mL de...To indirectly investigate the dislocation behavior of Fe-36wt%Ni Invar alloy by the etch pit method,polished Invar specimens were etched by a solution containing 4 g copper sulfate,20 mL hydrochloric acid,and 20 mL deionized water for 2 min.Etch pits in the etched surfaces were observed.All the etch pits in one specific grain exhibited similar shapes,which are closely related to the grain orientations.These etch pits were characterized as dislocation etch pits.It was observed that etch pits arranged along grain boundaries,gathered at grain tips and strip-like etch pit clusters passed through a number of grains in the pure Invar specimens.After the addition of a small amount of alloying elements,the identification of a single dislocation etch pit is challenging compared with the pure Invar alloy.Thus,the observation of etch pits facilitates the investigation on the dislocation behavior of the pure Invar alloy.In addition,alloying elements may affect the densities and sizes of etch pits.展开更多
In this work,the effects of HNO_3 concentration on the pit morphologies of high-cubic-texture aluminum foil etched in HNO_3-HCl and HNO_3-H_2SO_4-HCl solutions were investigated.When the aluminum foil was etched in HN...In this work,the effects of HNO_3 concentration on the pit morphologies of high-cubic-texture aluminum foil etched in HNO_3-HCl and HNO_3-H_2SO_4-HCl solutions were investigated.When the aluminum foil was etched in HNO_3-HCl solutions,the morphologies of pits transformed from irregular tunnels to typical tunnels(as inverted pyramids) and shallow cuboids as the HNO_3 concentration in the etchant solution was increased.However,as the HCl concentration in the etchant solution was increased,the morphologies of pits transformed from shallow cuboids to typical tunnels(as inverted pyramids) and irregular tunnels.When the aluminum foil was etched in n N HNO_3-(7.2-n) N H_2SO_4-0.8 N HCl solutions,the morphologies of the pits transformed from typical tunnels(i.e.,the number of sub-tunnels formed on the main tunnels increased) to irregular tunnels(corrugated tunnels and polyline tunnels) as the HNO_3 concentration in the etchant solution was increased.These effects are attributed primarily to corrosion on the(100) and(010) faces of pits being accelerated and to the(001) faces being prone to passivation to different degrees when various concentrations of HNO_3 are added to the etchant solutions.展开更多
Experiments were performed to study the pitting corrosion morphology of 304 stainless steel exposed to FeCl 3 environments and SEM micrographs of the pitting corrosion morphology were obtained. The image processing te...Experiments were performed to study the pitting corrosion morphology of 304 stainless steel exposed to FeCl 3 environments and SEM micrographs of the pitting corrosion morphology were obtained. The image processing technique combining with the fractal method was employed to analyze these pitting corrosion images and the self-similarity of pits morphology was observed. It indicates that fractal characteristics exist in pitting corrosion of 304 stainless steel. The self-similarity and complexity of the pitting morphology phenomenon were described in terms of fractal dimension which can also be an important parameter related to characterize pitting morphology qualitatively and quantitatively.展开更多
The pit morphology and growth kinetics of commercially pure aluminium in naturally aerated NaCl solutions were studied using an image processing method based on reflected light microscopy. In order to distinguish betw...The pit morphology and growth kinetics of commercially pure aluminium in naturally aerated NaCl solutions were studied using an image processing method based on reflected light microscopy. In order to distinguish between pits and pre-existing cavities, metallographic examination and statistical analysis were carried out before and after corrosion testing. The results show that the pit shapes and sizes are more dependent on the immersion time than the chloride concentration. Pits are predominantly hemispherical, but they undergo reasonable geometric transitions associated with increased immersion time and occur without significant depth variation. The role of chloride ions is more closely associated with the pit nucleation phenomenon.展开更多
A set of evaluation indicators based on corrosion ratio in theory for assessing the extent of pitting corrosion and performance reduction are proposed. In order to quantify the morphology of pitting corrosion and extr...A set of evaluation indicators based on corrosion ratio in theory for assessing the extent of pitting corrosion and performance reduction are proposed. In order to quantify the morphology of pitting corrosion and extract the evaluation indicators,the 3D profile data obtained by pitting morphology measurement are imported into a special written program to automatically determine the location of each corrosion pit and distill any desired data pertinent to the pitting morphology. The results show that this method seems to be effective to analyze the corroded surface and characterize the pitting morphology.展开更多
Rolling Contact Fatigue(RCF) is a cumulativedamage phenomenon when metals are subjectedto repeated contact stresses. The fomationof pitting on the contact surface is the resultof the rolling contact fatigue. The morph...Rolling Contact Fatigue(RCF) is a cumulativedamage phenomenon when metals are subjectedto repeated contact stresses. The fomationof pitting on the contact surface is the resultof the rolling contact fatigue. The morphologiesof rolling contact fatigue fracture of the har-dened steels (86CrHoV7, 42CrMo) show that strongresemblance in fractuye mechanisms exists betweenrolling contact fatigue and uni-axial fatigue.Since fatigue striations are hardly observedin hardened steels under uni-axial fatigue,it is interesting to note that the state ofstress in rolling contact fatigue is more favor-able to ductile fractures than in uni-axialfatigue.展开更多
Epoxy resin(EP)tends to accumulate a large amount of charge on its surface when exposed to a high-voltage DC electric field,which leads to a reduction in its insulative performance and an increase in potential safety ...Epoxy resin(EP)tends to accumulate a large amount of charge on its surface when exposed to a high-voltage DC electric field,which leads to a reduction in its insulative performance and an increase in potential safety risks in power systems.To suppress charge accumulation,improve the flashover voltage of the EP,and reduce the risk of gas insulated switchgear(GIS)/gas insulated transmission line(GIL)failure,we used two plasma-etching methods,i.e.,atmospheric-pressure dielectric barrier discharge(DBD)and the atmospheric-pressure plasma jet(APPJ),to modify the surface of the EP.The surface morphology and electrical properties of the modified materials were explored as a function of time.The results show that after DBD treatment,the roughness of the sample increases by 103.9 nm,the conductivity increases by3.9×10^(-18)S,and the flashover voltage increases by 14.4%;after APPJ treatment,the roughness of the sample increases by 223.5 nm,the conductivity increases by 3.4×10^(-17)S,and the flashover voltage increases by 18%.This shows that both plasma-etching methods can improve the insulation properties of materials by improving the surface-charge characteristics.The two methods are compared with each other:the APPJ treatment method is better at improving the surface roughness and electrical properties of materials,and this flexible treatment method has greater potential in industrial applications.展开更多
The morphologies of tunnel tips in diferent stages for aluminum foils during DC etching in 1.5 mol/L HCl solution at 90 C were observed by field emission scanning electron microscopy(FE-SEM).A novel model was proposed...The morphologies of tunnel tips in diferent stages for aluminum foils during DC etching in 1.5 mol/L HCl solution at 90 C were observed by field emission scanning electron microscopy(FE-SEM).A novel model was proposed to describe the morphological evolution of tunnel tips throughout the growth processes.In the pit nucleation stage,the pits vary from the hemispherical to half-cubic shapes due to the activation of pit tips from the center to the edge.During the tunnel growth stage,the pits dissolve toward the depth direction and develop into the tunnels,and their tips remain flat.In the tip passivation stage,as the passivation of tunnel tips speeds up from the edge to the center,the tunnel tips change from flat shapes to three-dimensional protrusions.The mechanism may be attributed to the order of activation or passivation on the tunnel tips changed in diferent stages.展开更多
The analysis of threading dislocation density(TDD)in Ge-on-Si layer is critical for developing lasers,light emitting diodes(LEDs),photodetectors(PDs),modulators,waveguides,metal oxide semiconductor field effect transi...The analysis of threading dislocation density(TDD)in Ge-on-Si layer is critical for developing lasers,light emitting diodes(LEDs),photodetectors(PDs),modulators,waveguides,metal oxide semiconductor field effect transistors(MOS-FETs),and also the integration of Si-based monolithic photonics.The TDD of Ge epitaxial layer is analyzed by etching or transmission electron microscope(TEM).However,high-resolution x-ray diffraction(HR-XRD)rocking curve provides an optional method to analyze the TDD in Ge layer.The theory model of TDD measurement from rocking curves was first used in zinc-blende semiconductors.In this paper,this method is extended to the case of strained Ge-on-Si layers.The HR-XRD 2θ/ωscan is measured and Ge(004)single crystal rocking curve is utilized to calculate the TDD in strained Ge epitaxial layer.The rocking curve full width at half maximum(FWHM)broadening by incident beam divergence of the instrument,crystal size,and curvature of the crystal specimen is subtracted.The TDDs of samples A and B are calculated to be 1.41×10~8cm^(-2)and 6.47×10~8cm^(-2),respectively.In addition,we believe the TDDs calculated by this method to be the averaged dislocation density in the Ge epitaxial layer.展开更多
The limiting length of tunnels, llim, of Al foil electro-etched in HCl-H2SO4 solution and the corresponding anodic polarization curves in the same solution were measured. It is found that there is a dependence of llim...The limiting length of tunnels, llim, of Al foil electro-etched in HCl-H2SO4 solution and the corresponding anodic polarization curves in the same solution were measured. It is found that there is a dependence of llim on the potential difference, △φ, between the pitting potential, φpit, and the corrosion potential, φcorr, of Al foil, when the temperature and H2SO4 concentration of HCl-H2SO4 electrolyte are changed. The dynamic equation on the tunnel growing and the linear equation between llim and △φ were deduced by analyzing the relationship among the over-potential on Al foil surface, the transport over-potential in tunnel solution and the over-potential at tunnel tip during the electro-etching. The results show that the growing velocity of tunnels decreases with their extending in length and the changing trend of llim can be judged by measuring △φ, which supplies a convenient access to explore new kinds of etchants.展开更多
AIM:To investigate the foveal pit morphology changes in unaffected carriers and affected Leber’s hereditary optic neuropathy(LHON)patients with the G11778 A mutation from one family.METHODS:This study was a prospecti...AIM:To investigate the foveal pit morphology changes in unaffected carriers and affected Leber’s hereditary optic neuropathy(LHON)patients with the G11778 A mutation from one family.METHODS:This study was a prospective cross-sectional study.Both eyes from 16 family members(age from 9 to 47 y)with the G11778 A mutation were analyzed and compared with 1 eye from 20 normal control subjects.Eleven family members with the G11778 A mutation but without optic neuropathy were classified as unaffected carriers(n=22 eyes).Five family members(n=10 eyes)expressed the LHON phenotype and were classified as affected patients.Retinal images of all the subjects were taken by optical coherence tomography(OCT),and an automatic algorithm was used to segment the retina to eight layers.Horizontal and vertical OCT images centered on the fovea were used to measure intra-retinal layer thicknesses and foveal morphometry.RESULTS:Thicker foveal thickness,thinner foveal pit depth,and flatter foveal slopes were observed in unaffected carriers and affected LHON patients(all P<0.001).Further,the slopes of all four sectors in the LHON were flatter than those in the unaffected carriers(all P<0.001).Compared with the control group,affected LHON patients had a thinner retinal nerve fiber layer(RNFL),ganglion cell layer and inner plexiform layer(GCL+IPL),and total retina(all P<0.01).The retinal nerve fiber layer(RNFL)of affected patients was 38.0%thinner than that of controls while the GCL+IPL was 40.1%thinner.CONCLUSION:The foveal pit morphology shows changes in both unaffected carriers and affects patients.RNFL and GCL+IPL are thinner in affected LHON patients but not in unaffected carriers.展开更多
The morphology of etched aluminum foil was observed using scanning electron microscopy, which led to the establishment of a cylindrical model and two merged models, considering the fixed weight loss of etching. The ma...The morphology of etched aluminum foil was observed using scanning electron microscopy, which led to the establishment of a cylindrical model and two merged models, considering the fixed weight loss of etching. The maximum of specific capacitance and the corresponding optimum values for tunnel sizes at various anodization voltages were predicted. The increased size distribution and taper of tunnels were demonstrated to decrease the specific capacitance, whereas the addition of polymeric additive into the tunnel widening solution was demonstrated to increase the capacitance. The formation of merged tunnels on the etched aluminum surface, irrespective of the presence of row-merged tunnels or cluster-merged tunnels, resulted in a dramatic decrease in the specific capacitance. It is concluded that, enhancing the uniformity of tunnel size and distribution and avoiding the formation of merged tunnels are the effective approach to achieving the higher capacitance for the tunnel etched and formed aluminum foil.展开更多
The {0001} face develops on the habit of self-frequency doubling laser crystal Yb: YAl3(BO3)4 (YbYAB) only under high growth rate condition, and its morphology is rough. To study the growth mechanism of {0001} face, w...The {0001} face develops on the habit of self-frequency doubling laser crystal Yb: YAl3(BO3)4 (YbYAB) only under high growth rate condition, and its morphology is rough. To study the growth mechanism of {0001} face, we have observed the growth morphology on {0001} polishing section by atomic force microscopy (AFM). A series of AFM images captured in different growth durations on the {0001} polishing section reflect the crystal growth process. It is shown that the growth morphology on the {0001} polishing section was rough with many hillocks at the first growth stage, and it can become smooth finally, although the growth morphology on the {0001} face developed naturally on YbYAB crystal habit is always rough. On the smooth {0001} surface formed at the last growth stage, there are some triangular pits. This fact is different from that of hillocks in most crystal growth morphologies. AFM can easily distinguish the pits or hillocks on the surface, but differential interfere contrast microscopy (DIC) can not do. The orientation of the triangular pits is just the opposite to the triangular {0001} faces. The chemical etching pattern is also composed of this kind of triangular pits. These growth morphology and etching pattern of the {0001} faces show 3m symmetry, but the point group of YbYAB crystal is 32. The symmetric contradiction between morphology and point group does not exist for quartz, although which has the same point group as YbYAB. From quartz {0001} surface morphology we can distinguish the right form or left form of the crystal, but from YbYAB {0001} surface morphology we can not do. The reason for the symmetric contradiction between YbYAB {0001} surface morphology and its point group is not known yet.展开更多
文摘To indirectly investigate the dislocation behavior of Fe-36wt%Ni Invar alloy by the etch pit method,polished Invar specimens were etched by a solution containing 4 g copper sulfate,20 mL hydrochloric acid,and 20 mL deionized water for 2 min.Etch pits in the etched surfaces were observed.All the etch pits in one specific grain exhibited similar shapes,which are closely related to the grain orientations.These etch pits were characterized as dislocation etch pits.It was observed that etch pits arranged along grain boundaries,gathered at grain tips and strip-like etch pit clusters passed through a number of grains in the pure Invar specimens.After the addition of a small amount of alloying elements,the identification of a single dislocation etch pit is challenging compared with the pure Invar alloy.Thus,the observation of etch pits facilitates the investigation on the dislocation behavior of the pure Invar alloy.In addition,alloying elements may affect the densities and sizes of etch pits.
基金supported by the Research Project of Guangxi Zhuang Autonomous Region, China (Nos. 1346011-7 and 1298019-11)the Guangxi Hezhou Guidong Electronics Technology Co., Ltd
文摘In this work,the effects of HNO_3 concentration on the pit morphologies of high-cubic-texture aluminum foil etched in HNO_3-HCl and HNO_3-H_2SO_4-HCl solutions were investigated.When the aluminum foil was etched in HNO_3-HCl solutions,the morphologies of pits transformed from irregular tunnels to typical tunnels(as inverted pyramids) and shallow cuboids as the HNO_3 concentration in the etchant solution was increased.However,as the HCl concentration in the etchant solution was increased,the morphologies of pits transformed from shallow cuboids to typical tunnels(as inverted pyramids) and irregular tunnels.When the aluminum foil was etched in n N HNO_3-(7.2-n) N H_2SO_4-0.8 N HCl solutions,the morphologies of the pits transformed from typical tunnels(i.e.,the number of sub-tunnels formed on the main tunnels increased) to irregular tunnels(corrugated tunnels and polyline tunnels) as the HNO_3 concentration in the etchant solution was increased.These effects are attributed primarily to corrosion on the(100) and(010) faces of pits being accelerated and to the(001) faces being prone to passivation to different degrees when various concentrations of HNO_3 are added to the etchant solutions.
文摘Experiments were performed to study the pitting corrosion morphology of 304 stainless steel exposed to FeCl 3 environments and SEM micrographs of the pitting corrosion morphology were obtained. The image processing technique combining with the fractal method was employed to analyze these pitting corrosion images and the self-similarity of pits morphology was observed. It indicates that fractal characteristics exist in pitting corrosion of 304 stainless steel. The self-similarity and complexity of the pitting morphology phenomenon were described in terms of fractal dimension which can also be an important parameter related to characterize pitting morphology qualitatively and quantitatively.
基金This research was supported by FUNDUNESP(process 01258/2008 and 00601/2011-DFP)CNPq(processes 305224/2004-2 and 307271/2007-2).
文摘The pit morphology and growth kinetics of commercially pure aluminium in naturally aerated NaCl solutions were studied using an image processing method based on reflected light microscopy. In order to distinguish between pits and pre-existing cavities, metallographic examination and statistical analysis were carried out before and after corrosion testing. The results show that the pit shapes and sizes are more dependent on the immersion time than the chloride concentration. Pits are predominantly hemispherical, but they undergo reasonable geometric transitions associated with increased immersion time and occur without significant depth variation. The role of chloride ions is more closely associated with the pit nucleation phenomenon.
基金Sponsored by the National Natural Science Foundation of China(Grant No.51378417)Program for Changjiang Scholars and Innovative Research Team in University(IRT13089)PhD Innovation Fund of Xi'an University of Architecture and Technology
文摘A set of evaluation indicators based on corrosion ratio in theory for assessing the extent of pitting corrosion and performance reduction are proposed. In order to quantify the morphology of pitting corrosion and extract the evaluation indicators,the 3D profile data obtained by pitting morphology measurement are imported into a special written program to automatically determine the location of each corrosion pit and distill any desired data pertinent to the pitting morphology. The results show that this method seems to be effective to analyze the corroded surface and characterize the pitting morphology.
文摘Rolling Contact Fatigue(RCF) is a cumulativedamage phenomenon when metals are subjectedto repeated contact stresses. The fomationof pitting on the contact surface is the resultof the rolling contact fatigue. The morphologiesof rolling contact fatigue fracture of the har-dened steels (86CrHoV7, 42CrMo) show that strongresemblance in fractuye mechanisms exists betweenrolling contact fatigue and uni-axial fatigue.Since fatigue striations are hardly observedin hardened steels under uni-axial fatigue,it is interesting to note that the state ofstress in rolling contact fatigue is more favor-able to ductile fractures than in uni-axialfatigue.
基金supported by National Natural Science Foundation of China(Nos.51777076,51507066)the Fundamental Research Funds for the Central Universities(Nos.2019MS083,2018MS084)the Self-topic Fund of State Key Laboratory of Alternate Electrical Power System with Renewable Energy Sources(Nos.LAPS202116,LAPS202103)。
文摘Epoxy resin(EP)tends to accumulate a large amount of charge on its surface when exposed to a high-voltage DC electric field,which leads to a reduction in its insulative performance and an increase in potential safety risks in power systems.To suppress charge accumulation,improve the flashover voltage of the EP,and reduce the risk of gas insulated switchgear(GIS)/gas insulated transmission line(GIL)failure,we used two plasma-etching methods,i.e.,atmospheric-pressure dielectric barrier discharge(DBD)and the atmospheric-pressure plasma jet(APPJ),to modify the surface of the EP.The surface morphology and electrical properties of the modified materials were explored as a function of time.The results show that after DBD treatment,the roughness of the sample increases by 103.9 nm,the conductivity increases by3.9×10^(-18)S,and the flashover voltage increases by 14.4%;after APPJ treatment,the roughness of the sample increases by 223.5 nm,the conductivity increases by 3.4×10^(-17)S,and the flashover voltage increases by 18%.This shows that both plasma-etching methods can improve the insulation properties of materials by improving the surface-charge characteristics.The two methods are compared with each other:the APPJ treatment method is better at improving the surface roughness and electrical properties of materials,and this flexible treatment method has greater potential in industrial applications.
基金the financial support by the Guangxi Hezhou Guidong Electronics Technology Co.Ltd.the Research Project of Guangxi Zhuang Autonomous Region(Nos.1346011-7 and 1298019-11)
文摘The morphologies of tunnel tips in diferent stages for aluminum foils during DC etching in 1.5 mol/L HCl solution at 90 C were observed by field emission scanning electron microscopy(FE-SEM).A novel model was proposed to describe the morphological evolution of tunnel tips throughout the growth processes.In the pit nucleation stage,the pits vary from the hemispherical to half-cubic shapes due to the activation of pit tips from the center to the edge.During the tunnel growth stage,the pits dissolve toward the depth direction and develop into the tunnels,and their tips remain flat.In the tip passivation stage,as the passivation of tunnel tips speeds up from the edge to the center,the tunnel tips change from flat shapes to three-dimensional protrusions.The mechanism may be attributed to the order of activation or passivation on the tunnel tips changed in diferent stages.
基金Project supported by the Research Plan in Shaanxi Province,China(Grant No.2016GY-085)the Opening Project of Key Laboratory of Microelectronic Devices&Integrated Technology,Institute of Microelectronics,Chinese Academy of Sciences(Grant No.90109162905)+1 种基金the Fundamental Research Funds for the Central Universities(Grant No.17-H863-04-ZT-001-019-01)the National Natural Science Foundation of China(Grant Nos.61704130 and 61474085)
文摘The analysis of threading dislocation density(TDD)in Ge-on-Si layer is critical for developing lasers,light emitting diodes(LEDs),photodetectors(PDs),modulators,waveguides,metal oxide semiconductor field effect transistors(MOS-FETs),and also the integration of Si-based monolithic photonics.The TDD of Ge epitaxial layer is analyzed by etching or transmission electron microscope(TEM).However,high-resolution x-ray diffraction(HR-XRD)rocking curve provides an optional method to analyze the TDD in Ge layer.The theory model of TDD measurement from rocking curves was first used in zinc-blende semiconductors.In this paper,this method is extended to the case of strained Ge-on-Si layers.The HR-XRD 2θ/ωscan is measured and Ge(004)single crystal rocking curve is utilized to calculate the TDD in strained Ge epitaxial layer.The rocking curve full width at half maximum(FWHM)broadening by incident beam divergence of the instrument,crystal size,and curvature of the crystal specimen is subtracted.The TDDs of samples A and B are calculated to be 1.41×10~8cm^(-2)and 6.47×10~8cm^(-2),respectively.In addition,we believe the TDDs calculated by this method to be the averaged dislocation density in the Ge epitaxial layer.
基金Project supported by University New Materials Disciplines Construction Program of Beijing, China
文摘The limiting length of tunnels, llim, of Al foil electro-etched in HCl-H2SO4 solution and the corresponding anodic polarization curves in the same solution were measured. It is found that there is a dependence of llim on the potential difference, △φ, between the pitting potential, φpit, and the corrosion potential, φcorr, of Al foil, when the temperature and H2SO4 concentration of HCl-H2SO4 electrolyte are changed. The dynamic equation on the tunnel growing and the linear equation between llim and △φ were deduced by analyzing the relationship among the over-potential on Al foil surface, the transport over-potential in tunnel solution and the over-potential at tunnel tip during the electro-etching. The results show that the growing velocity of tunnels decreases with their extending in length and the changing trend of llim can be judged by measuring △φ, which supplies a convenient access to explore new kinds of etchants.
基金Supported by Wenzhou Technology Program(No.Y20160148).
文摘AIM:To investigate the foveal pit morphology changes in unaffected carriers and affected Leber’s hereditary optic neuropathy(LHON)patients with the G11778 A mutation from one family.METHODS:This study was a prospective cross-sectional study.Both eyes from 16 family members(age from 9 to 47 y)with the G11778 A mutation were analyzed and compared with 1 eye from 20 normal control subjects.Eleven family members with the G11778 A mutation but without optic neuropathy were classified as unaffected carriers(n=22 eyes).Five family members(n=10 eyes)expressed the LHON phenotype and were classified as affected patients.Retinal images of all the subjects were taken by optical coherence tomography(OCT),and an automatic algorithm was used to segment the retina to eight layers.Horizontal and vertical OCT images centered on the fovea were used to measure intra-retinal layer thicknesses and foveal morphometry.RESULTS:Thicker foveal thickness,thinner foveal pit depth,and flatter foveal slopes were observed in unaffected carriers and affected LHON patients(all P<0.001).Further,the slopes of all four sectors in the LHON were flatter than those in the unaffected carriers(all P<0.001).Compared with the control group,affected LHON patients had a thinner retinal nerve fiber layer(RNFL),ganglion cell layer and inner plexiform layer(GCL+IPL),and total retina(all P<0.01).The retinal nerve fiber layer(RNFL)of affected patients was 38.0%thinner than that of controls while the GCL+IPL was 40.1%thinner.CONCLUSION:The foveal pit morphology shows changes in both unaffected carriers and affects patients.RNFL and GCL+IPL are thinner in affected LHON patients but not in unaffected carriers.
基金financially supported by the Research Project of Guangxi Zhuang Autonomous Region,China(Nos.1346011-7 and 1298019-11)the financial support from the Guangxi Hezhou Guidong Electronics Technology Co.,Ltd
文摘The morphology of etched aluminum foil was observed using scanning electron microscopy, which led to the establishment of a cylindrical model and two merged models, considering the fixed weight loss of etching. The maximum of specific capacitance and the corresponding optimum values for tunnel sizes at various anodization voltages were predicted. The increased size distribution and taper of tunnels were demonstrated to decrease the specific capacitance, whereas the addition of polymeric additive into the tunnel widening solution was demonstrated to increase the capacitance. The formation of merged tunnels on the etched aluminum surface, irrespective of the presence of row-merged tunnels or cluster-merged tunnels, resulted in a dramatic decrease in the specific capacitance. It is concluded that, enhancing the uniformity of tunnel size and distribution and avoiding the formation of merged tunnels are the effective approach to achieving the higher capacitance for the tunnel etched and formed aluminum foil.
基金The work was supported by the National Natural Science Foundation of China (grant No. 69890235 and 59823003).
文摘The {0001} face develops on the habit of self-frequency doubling laser crystal Yb: YAl3(BO3)4 (YbYAB) only under high growth rate condition, and its morphology is rough. To study the growth mechanism of {0001} face, we have observed the growth morphology on {0001} polishing section by atomic force microscopy (AFM). A series of AFM images captured in different growth durations on the {0001} polishing section reflect the crystal growth process. It is shown that the growth morphology on the {0001} polishing section was rough with many hillocks at the first growth stage, and it can become smooth finally, although the growth morphology on the {0001} face developed naturally on YbYAB crystal habit is always rough. On the smooth {0001} surface formed at the last growth stage, there are some triangular pits. This fact is different from that of hillocks in most crystal growth morphologies. AFM can easily distinguish the pits or hillocks on the surface, but differential interfere contrast microscopy (DIC) can not do. The orientation of the triangular pits is just the opposite to the triangular {0001} faces. The chemical etching pattern is also composed of this kind of triangular pits. These growth morphology and etching pattern of the {0001} faces show 3m symmetry, but the point group of YbYAB crystal is 32. The symmetric contradiction between morphology and point group does not exist for quartz, although which has the same point group as YbYAB. From quartz {0001} surface morphology we can distinguish the right form or left form of the crystal, but from YbYAB {0001} surface morphology we can not do. The reason for the symmetric contradiction between YbYAB {0001} surface morphology and its point group is not known yet.
