In order to expand the application of steel 20 in precision device,fast multiple rotation rolling( FMRR) is applied to fabricate a nanostructured layer on the surface of steel 20. The FMRR samples are then Cr-Rare ear...In order to expand the application of steel 20 in precision device,fast multiple rotation rolling( FMRR) is applied to fabricate a nanostructured layer on the surface of steel 20. The FMRR samples are then Cr-Rare earth-boronized under low-temperature. The microstructure of the top surface layer is characterized by transmission electron microscopy( TEM). Microhardness of the top surface is measured by a Vickers microhardness tester. The boride layer is characterized by using scanning electron microscopy( SEM).Experimental results show that a nanostructured layer with their grain size range from 200 to 400 nm is obtained in the top surface layer. The microhardness of FMRR sample changes gradiently along the depth from about274 HV in the top surface layer to about 159 HV in the matrix,which is nearly 1.7 times harder than that of the original sample. The penetrating rate is enhanced significantly when the FMRR samples are Cr-Rare earthboronized at 600 ℃ for 6 h. Thickness of the boride layer increases to around 20 μm,which is nearly twice thicker than that of the original sample.展开更多
Using fast multiple rotation rolling(FMRR),a nanostructure layer was fabricated on the surface of Ti6Al4V alloy.The microstructure of the surface layer was investigated using optical microscopy,transmission electron m...Using fast multiple rotation rolling(FMRR),a nanostructure layer was fabricated on the surface of Ti6Al4V alloy.The microstructure of the surface layer was investigated using optical microscopy,transmission electron microscopy,scanning electron microscopy,and X-ray diffraction.The results indicated that a nanostructured layer,with an average grain size of 72—83 nm,was obtained in the top surface layer,when the FMRR duration was 15 min.And the average grain size further reduced to 24—37 nm when the treatment duration increased to 45 min.High density dislocations,twins,and stacking faults were observed in the top surface layer.The microhardness of FMRR specimen,compared with original specimen,was significantly increased.A uniform,continuous and thicker compound layer was obtained in the top surface of FMRR sample,and the diffusion speed of N atom in the top surface layer was accelerated.FMRR treatment provides corrosion improvement.展开更多
文摘In order to expand the application of steel 20 in precision device,fast multiple rotation rolling( FMRR) is applied to fabricate a nanostructured layer on the surface of steel 20. The FMRR samples are then Cr-Rare earth-boronized under low-temperature. The microstructure of the top surface layer is characterized by transmission electron microscopy( TEM). Microhardness of the top surface is measured by a Vickers microhardness tester. The boride layer is characterized by using scanning electron microscopy( SEM).Experimental results show that a nanostructured layer with their grain size range from 200 to 400 nm is obtained in the top surface layer. The microhardness of FMRR sample changes gradiently along the depth from about274 HV in the top surface layer to about 159 HV in the matrix,which is nearly 1.7 times harder than that of the original sample. The penetrating rate is enhanced significantly when the FMRR samples are Cr-Rare earthboronized at 600 ℃ for 6 h. Thickness of the boride layer increases to around 20 μm,which is nearly twice thicker than that of the original sample.
基金National Key Research and Development Program of China(No.2016YFB0300700)Education and Scientific Research Project of Shanghai(No.19SG46)+2 种基金Natural Science Foundation of Shanghai(No.17ZR1440900)International Science and Technology Cooperation Program(No.CU03-29)Project of Shandong Province Higher Educational Science and Technology Program(No.J17KA017)。
文摘Using fast multiple rotation rolling(FMRR),a nanostructure layer was fabricated on the surface of Ti6Al4V alloy.The microstructure of the surface layer was investigated using optical microscopy,transmission electron microscopy,scanning electron microscopy,and X-ray diffraction.The results indicated that a nanostructured layer,with an average grain size of 72—83 nm,was obtained in the top surface layer,when the FMRR duration was 15 min.And the average grain size further reduced to 24—37 nm when the treatment duration increased to 45 min.High density dislocations,twins,and stacking faults were observed in the top surface layer.The microhardness of FMRR specimen,compared with original specimen,was significantly increased.A uniform,continuous and thicker compound layer was obtained in the top surface of FMRR sample,and the diffusion speed of N atom in the top surface layer was accelerated.FMRR treatment provides corrosion improvement.