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Prediction of loess soil-water characteristic curve by mercury intrusion porosimetry 被引量:4
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作者 LI Hua LI Tong-lu +1 位作者 LI Ping ZHANG Ya-guo 《Journal of Mountain Science》 SCIE CSCD 2020年第9期2203-2213,共11页
Mercury intrusion porosimetry(MIP)is a simple and fast way to obtain the pore distribution of soil and can be used to estimate the soil-water characteristic curve(SWCC).In previous studies,soil was assumed to be a per... Mercury intrusion porosimetry(MIP)is a simple and fast way to obtain the pore distribution of soil and can be used to estimate the soil-water characteristic curve(SWCC).In previous studies,soil was assumed to be a perfect wettability material,and the contact angle(CA)of the soil-water interface was taken as zero in the SWCC prediction method.However,the CA has proved to be much greater than zero even for hydrophilic soils according to some soil wettability experiments,and it has a significant effect on predicting the SWCC.In this research,a method for predicting the SWCC by MIP,which takes the CA as a fitting coefficient,is proposed.The pore size distribution curves are measured by MIP,and the SWCCs of two loess soils are measured by pressure plate and filter paper tests.When the CA is taken as70°and 50°for the wetting and drying process,respectively,the SWCCs predicted by the pore size distribution curves agree well with the measured SWCCs.The predicted suction range of the proposed method is 0-105 k Pa.The consistency of the results suggests that utilizing the MIP test to predict the SWCC with a proper CA is effective for loess. 展开更多
关键词 Soil-water characteristic curve mercury intrusion porosimetry Contact angle LOESS
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Determining the soil-water retention curve using mercury intrusion porosimetry test in consideration of soil volume change 被引量:5
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作者 Wen-Jing Sun Yu-Jun Cui 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2020年第5期1070-1079,共10页
It is well-known that a close link exists between soil-water retention curve(SWRC)and pore size distribution(PSD).Theoretically,mercury intrusion porosimetry(MIP)test simulates a soil drying path and the test results ... It is well-known that a close link exists between soil-water retention curve(SWRC)and pore size distribution(PSD).Theoretically,mercury intrusion porosimetry(MIP)test simulates a soil drying path and the test results can be used to deduce the SWRC(termed SWRCMIP).However,SWRCMIP does not include the effect of volume change,compared with the conventional SWRC that is directly determined by suction measurement or suction control techniques.For deformable soils,there is a significant difference between conventional SWRC and SWRCMIP.In this study,drying test was carried out on a reconstituted silty soil,and the volume change,suction,and PSD were measured on samples with different water contents.The change in the deduced SWRCMIP and its relationship with the conventional SWRC were analyzed.The results showed that the volume change of soil is the main reason accounting for the difference between conventional SWRC and SWRCMIP.Based on the test results,a transformation model was then proposed for conventional SWRC and SWRCMIP,for which the soil state with no volume change is taken as a reference.Comparison between the experimental and predicted SWRCs showed that the proposed model can well consider the influence of soil volume change on its water retention property. 展开更多
关键词 Soil-water retention curve(SWRC) mercury intrusion porosimetry(MIP) Pore size distribution(PSD) Deformable soils
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Comparison of the Pore Structure of Ultralow-Permeability Reservoirs Between the East and West Subsags of the Lishui Sag Using Constant-Rate Mercury Injection 被引量:2
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作者 WANG Jinkai ZHANG Jinliang +1 位作者 SHEN Wenlong LIU Hengyi 《Journal of Ocean University of China》 SCIE CAS CSCD 2021年第2期315-328,共14页
In this study, the differences in reservoir parameters, such as pore radius, throat radius, and pore-throat ratio, between the east and west subsags of the Lishui Sag are analyzed by using data obtained from a constan... In this study, the differences in reservoir parameters, such as pore radius, throat radius, and pore-throat ratio, between the east and west subsags of the Lishui Sag are analyzed by using data obtained from a constant-rate mercury injection experiment. Furthermore, the quality of the reservoirs in the two subsags is systematically evaluated. Results show that the throat radius of the Lishui west subsag is larger than that of the east subsag, and this parameter has a positive correlation with reservoir quality. However, the pore-throat ratio of the east subsag is larger than that of the west subsag, which has an inverse relationship with reservoir quality. The main reasons for this reservoir difference can be attributed to sedimentation and diagenesis. The sedimentary facies types of the Lishui east subsag are the fan delta, shore lake, shallow lake, and shore shallow lake;their sandstone composition maturity is low;the clay mineral content is high;and the rock has undergone strong diagenesis. Therefore, the physical conditions of the reservoir are poor. However, the sandstones in the Lishui west subsag have weak cementation and compaction, mainly with an intergranular pore structure type, which leads to good connectivity between pores. Therefore, the storage performance and seepage capacity of the Lishui west subsag are better than those of the east subsag;the west subsag is the main area of oil and gas accumulation, as confirmed in the process of exploration and development. 展开更多
关键词 Lishui Sag constant-rate mercury injection sedimentary facies DIAGENESIS rock pore structure
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Influence of Dry Density on Soil-Water Retention Curve of Unsaturated Soils and Its Mechanism Based on Mercury Intrusion Porosimetry
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作者 李博 陈宇龙 《Transactions of Tianjin University》 EI CAS 2016年第3期268-272,共5页
The soil-water retention curve(SWRC)can be used to evaluate the ability of unsaturated soils to attract water at various water contents and suctions. In this study, drying SWRCs for a kind of sandy soil were obtained ... The soil-water retention curve(SWRC)can be used to evaluate the ability of unsaturated soils to attract water at various water contents and suctions. In this study, drying SWRCs for a kind of sandy soil were obtained in the laboratory by using self-modified SWRC apparatus. In addition, the porosity and the pore size distribution of the samples were investigated by a mercury porosimetry test in order to analyze the effect of dry density. Results showed that the soil-water retention of the soil specimens was strongly dependent on the dry density. Under zero suction, soil specimens with a higher dry density exhibited lower initial volumetric water content. The higher the dry density of soil, the more slowly the volumetric water content decreased with the increase of suction. There was a general and consistent trend for a soil specimen to possess a larger air-entry value and residual suction, while smaller slope of SWRC when it had a higher density. This was probably attributed to the presence of smaller interconnected pores in the soil specimen with a higher dry density. The proportion of large diameter pores decreased in comparison to pores with small diameters in the soil tested. The measured total pore volume of the soil specimen, which had a larger dry density, was lower than that of the relatively loose specimens. 展开更多
关键词 土壤水分特征曲线 土壤干密度 非饱和土 压汞法 土壤样品 土壤含水量 体积含水量 机制
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A Secure Hardware Implementation for Elliptic Curve Digital Signature Algorithm
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作者 Mouna Bedoui Belgacem Bouallegue +4 位作者 Abdelmoty M.Ahmed Belgacem Hamdi Mohsen Machhout Mahmoud M.Khattab 《Computer Systems Science & Engineering》 SCIE EI 2023年第3期2177-2193,共17页
Since the end of the 1990s,cryptosystems implemented on smart cards have had to deal with two main categories of attacks:side-channel attacks and fault injection attacks.Countermeasures have been developed and validat... Since the end of the 1990s,cryptosystems implemented on smart cards have had to deal with two main categories of attacks:side-channel attacks and fault injection attacks.Countermeasures have been developed and validated against these two types of attacks,taking into account a well-defined attacker model.This work focuses on small vulnerabilities and countermeasures related to the Elliptic Curve Digital Signature Algorithm(ECDSA)algorithm.The work done in this paper focuses on protecting the ECDSA algorithm against fault-injection attacks.More precisely,we are interested in the countermeasures of scalar multiplication in the body of the elliptic curves to protect against attacks concerning only a few bits of secret may be sufficient to recover the private key.ECDSA can be implemented in different ways,in software or via dedicated hardware or a mix of both.Many different architectures are therefore possible to implement an ECDSA-based system.For this reason,this work focuses mainly on the hardware implementation of the digital signature ECDSA.In addition,the proposed ECDSA architecture with and without fault detection for the scalar multiplication have been implemented on Xilinxfield programmable gate arrays(FPGA)platform(Virtex-5).Our implementation results have been compared and discussed.Our area,frequency,area overhead and frequency degradation have been compared and it is shown that the proposed architecture of ECDSA with fault detection for the scalar multiplication allows a trade-off between the hardware overhead and the security of the ECDSA. 展开更多
关键词 Elliptic curve cryptography(ECC) Montgomery ladder fault detection method fault injection attack digital signature ECDSA FPGA
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致密砂岩气藏微观孔隙结构多尺度联合表征
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作者 甯波 任大忠 +6 位作者 王虎 张瀚澎 郭建林 付宁海 李俊键 李天 李启晖 《断块油气田》 CAS CSCD 2024年第1期34-41,共8页
致密砂岩的微观孔隙结构对气藏的开发至关重要。文中以临兴地区下石盒子组盒8段为研究对象,采用多种实验方法对致密砂岩孔隙结构进行精确表征。研究结果显示:致密砂岩主要孔隙类型为长石溶孔和岩屑溶孔,其次为粒间孔、晶间孔和微裂隙;... 致密砂岩的微观孔隙结构对气藏的开发至关重要。文中以临兴地区下石盒子组盒8段为研究对象,采用多种实验方法对致密砂岩孔隙结构进行精确表征。研究结果显示:致密砂岩主要孔隙类型为长石溶孔和岩屑溶孔,其次为粒间孔、晶间孔和微裂隙;高压压汞、CO_(2)吸附、N_(2)吸附以及渗吸-核磁等实验结果均反映了研究区致密砂岩孔隙结构具有较好的连通性;多尺度联合法表征的致密砂岩孔径分布以微孔为主,介孔次之,大孔最少;微孔的大量分布为比表面积做出主要贡献,介孔、大孔贡献较少,孔容主要由微孔、介孔贡献,大孔贡献较少;核磁共振计算的孔径分布比例与多尺度联合法的计算值在介孔、大孔阶段具有较好一致性,在微孔阶段,多尺度联合法的计算值大于核磁共振法,表明微孔为气藏的主要气体储集空间,而介孔和大孔为气体运移的主要通道,多尺度联合法在致密砂岩储层孔隙结构精细表征方面更具特色。 展开更多
关键词 致密砂岩气藏 气体吸附 高压压汞 核磁共振 孔隙表征
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牛东地区砂砾岩储层测井层内非均质性评价
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作者 周军 边会媛 +3 位作者 陈文安 张迪 刘国良 王飞 《物探与化探》 CAS 2024年第1期142-150,共9页
牛东地区砂砾岩储层具有低孔、低渗等特征,储层结构复杂,非均质性较强,常规测井对储层类型划分困难,影响了储层评价精度。岩心孔渗、薄片分析、X衍射等测试资料表明,牛东地区砂砾岩储层具有较强的非均质性,且根据毛管压力形态可将储层分... 牛东地区砂砾岩储层具有低孔、低渗等特征,储层结构复杂,非均质性较强,常规测井对储层类型划分困难,影响了储层评价精度。岩心孔渗、薄片分析、X衍射等测试资料表明,牛东地区砂砾岩储层具有较强的非均质性,且根据毛管压力形态可将储层分为3个类别。本次研究利用电成像测井资料对储层层内非均质性进行评价:首先对电成像测井资料进行处理得到储层孔隙度谱,再对随深度变化的孔隙度谱进行研究,分别计算不同深度上孔隙度谱的均值、方差、洛伦兹系数和集中程度函数;根据综合概率模型,利用层次分析法确定评价指标的权重,得到储层非均质性综合指数,据此对储层进行划分,并建立储层非均质性的评价标准。应用该方法得到的研究结果与压汞实验结果一致,说明利用该方法能够有效地评价储层非均质性,可丰富现有的储层非均质性评价方法,为储层的精细评价提供一定的理论支撑。 展开更多
关键词 电成像测井 非均质性评价 压汞曲线 洛伦兹系数 储层分类
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致密砂岩储层孔隙结构分形与分级评价——以莺歌海盆地乐东区黄流组为例
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作者 赵静 黄志龙 +2 位作者 张景缘 邓广君 许马光 《沉积学报》 CAS CSCD 2024年第1期295-308,共14页
[目的]明确致密砂岩储层孔喉微观形态,划分储层孔隙结构级次,多角度半定量评价储层的储集特征和渗流能力,有助于明确具有高效产能潜力的储层类型。[方法]以莺歌海盆乐东区黄流组致密砂岩为例,利用铸体薄片、扫描电镜、高压压汞等实验手... [目的]明确致密砂岩储层孔喉微观形态,划分储层孔隙结构级次,多角度半定量评价储层的储集特征和渗流能力,有助于明确具有高效产能潜力的储层类型。[方法]以莺歌海盆乐东区黄流组致密砂岩为例,利用铸体薄片、扫描电镜、高压压汞等实验手段,开展储层孔隙结构分形维数计算与分级评价的研究。[结果]致密砂岩储层质量的影响因素之一是大孔喉孔隙结构;分形维数越接近3,孔隙结构越复杂,连通的大孔喉越少。依据孔喉分级特征、成岩相、孔隙结构复杂程度,建立了孔隙结构分级评价的四类模型:类型Ⅰ为小孔喉优势型储层,强胶结成岩相,大孔喉孔隙度占比小于45%,D_(max)值为2.75~2.90,致密储层;类型Ⅱ为大—小孔喉连续型储层,弱胶结—弱溶蚀成岩相,大孔喉孔隙度占比45%~70%,D_(max)值为2.70~2.85,低渗储层;类型Ⅲ为大孔喉优势型储层,强溶蚀成岩相,大孔喉孔隙度占比大于70%,D_(max)值为2.55~2.65,优质储层;类型Ⅳ为大孔喉单峰型储层,强压实成岩相,大孔喉孔隙度占比50%~60%,D_(max)值为2.65~2.75,低渗储层。通过Fisher判别方法,建立储层类型测井预测模型,对比储层类型与气测响应和储层含气饱和度,发现Ⅲ类储层的产气效能高,具有勘探价值。[结论]研究成果为致密砂岩储层评价与分类提供了新思路,明确了储层孔隙结构对气水分布存在控制作用。 展开更多
关键词 莺歌海盆地 致密砂岩储层 高压压汞 孔隙结构分形
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致密砂岩储层微观孔喉结构及其分形特征
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作者 刘硕 王飞 +3 位作者 于瑞 高建星 师昊 朱玉双 《吉林大学学报(地球科学版)》 CAS CSCD 2024年第1期96-107,共12页
孔喉微观结构定量评价一直是致密砂岩储层研究的热点和难点。以分形维数为突破口,在鄂尔多斯盆地子长地区不同井中采集了上三叠统延长组长6段12个岩心样品,通过扫描电镜、铸体薄片、高压压汞等实验方法以及分形理论对致密砂岩样品的孔... 孔喉微观结构定量评价一直是致密砂岩储层研究的热点和难点。以分形维数为突破口,在鄂尔多斯盆地子长地区不同井中采集了上三叠统延长组长6段12个岩心样品,通过扫描电镜、铸体薄片、高压压汞等实验方法以及分形理论对致密砂岩样品的孔喉结构及其分形特征进行了研究。结果表明,研究区致密砂岩储层的孔隙类型主要由剩余粒间孔、溶孔和晶间孔组成。总分形维数与孔隙度和渗透率存在良好的负相关性,表明研究区致密砂岩储层孔喉结构的复杂程度和非均质性对物性具有一定的影响。中孔的分形维数与孔喉结构参数的相关性更好,表明中孔的非均质性和表面粗糙度主要影响储集空间和渗流性质。致密砂岩储层的品质与分形维数呈明显的负相关关系,越有利于油气富集的储层,其分形维数越小。 展开更多
关键词 鄂尔多斯盆地 致密砂岩 高压压汞 孔喉结构 分形特征 分形维数
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单、双孔隙结构非饱和黏土孔隙分布变化规律试验研究
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作者 张思奇 裴华富 +1 位作者 谭道远 朱鸿鹄 《岩土力学》 EI CAS CSCD 2024年第2期353-363,374,共12页
由于孔隙分布曲线的复杂性,在非饱和过程中黏土的孔隙结构变化规律尚不明晰,这导致基于孔隙分布模型计算土-水特征曲线存在较大的误差。针对这一问题,基于干缩试验与压汞试验,对单孔与双孔结构重塑黏土在脱湿过程中孔隙分布曲线的变化... 由于孔隙分布曲线的复杂性,在非饱和过程中黏土的孔隙结构变化规律尚不明晰,这导致基于孔隙分布模型计算土-水特征曲线存在较大的误差。针对这一问题,基于干缩试验与压汞试验,对单孔与双孔结构重塑黏土在脱湿过程中孔隙分布曲线的变化规律进行了定量分析。研究表明:在脱湿过程中孔隙分布曲线存在平移、缩放等变换。构建了t分布和双t分布函数,提取了孔隙分布曲线的自由度、峰值、峰值对应的孔隙直径作为特征参数来表征孔隙分布变化规律,发现了特征参数和土样孔隙比之间存在较好的线性关系。基于试验结果,建立了含水率-孔隙比-孔隙分布曲线关系,提出了一个考虑孔隙结构变化的重塑黏土土-水特征曲线计算框架。最后,与试验测得的土-水特征曲线进行比较,验证了所提出的计算方法的准确性。 展开更多
关键词 黏土 非饱和土 孔隙分布曲线 压汞试验 土-水特征曲线 干缩试验
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基于压汞-低温液氮联孔与核磁共振分析的煤中孔径分布对比研究
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作者 李娜娜 刘会虎 桑树勋 《煤矿安全》 CAS 2024年第2期1-9,共9页
煤中孔隙结构测量常用压汞法、低温液氮法和核磁共振法,因不同方法的原理和测试范围不同,导致结果无法统一使用,且压汞法中基质压缩效应会造成较大误差;为解决该问题,以沁水盆地晋城和长治矿区的3个高阶煤样为例,利用压汞、低温液氮吸... 煤中孔隙结构测量常用压汞法、低温液氮法和核磁共振法,因不同方法的原理和测试范围不同,导致结果无法统一使用,且压汞法中基质压缩效应会造成较大误差;为解决该问题,以沁水盆地晋城和长治矿区的3个高阶煤样为例,利用压汞、低温液氮吸附及核磁共振驰豫法分别测试煤样的孔隙结构,通过对压汞数据进行压缩性校正,与低温液氮数据在衔接孔径处拼接,对煤的孔隙结构进行了联合表征,并结合核磁共振对比分析了煤的孔径分布特征。结果表明:压汞数据校正后孔体积与低温液氮的结果更接近,偏差值在22.40%~38.51%;不同煤样采用联孔法进行孔隙结构分析的联孔位置在75~89 nm之间;联孔法煤样孔容积为0.00136~0.00458 cm^(3)/g,不同孔径孔容比例表现为过渡孔>大孔>中孔>微孔;与单一测试方法相比,联孔法与核磁共振法孔径分布更为接近,但同时也存在差异,联孔法表征的微孔、过渡孔、中孔和大孔平均分布比例分别为8.68%、45.58%、20.54%和25.20%,核磁法微孔、过渡孔、中孔和大孔平均分布比例分别为10.64%、64.21%、14.23%和10.92%,结果差异原因可能主要与压汞法、低温液氮法加压改变了煤的孔隙结构有关;通过核磁共振结果对比,联合校正后的压汞与低温液氮数据可提高煤中孔径分布测试结果的准确性。 展开更多
关键词 煤孔隙结构 孔径拼接 压汞法 低温液氮吸附法 低场核磁共振驰豫法
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管道特性曲线法在注射水储存分配系统的应用
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作者 马宁 江进 马鸿志 《山西建筑》 2024年第4期116-118,130,共4页
应用管道特性曲线法对制药企业注射水储存分配系统的流量与压力关系进行了分析探讨,提出了简化计算的方法,并结合具体工程案例进行了分析比较。针对系统实际运行调试过程中出现的常见问题,提出了相应的理论依据及措施。
关键词 制药厂房 注射水 储存分配系统 回水流量 管道特性曲线
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核磁共振氢谱法测定注射用微球专用溶剂中硅油的含量
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作者 马佳慧 夏昀卿 +4 位作者 沈莉 薛英 周凤梅 刘万卉 许丽晓 《山东化工》 CAS 2024年第3期138-140,145,共4页
目的:建立测定注射用微球专用溶剂中硅油含量的定量核磁共振氢谱(qHNMR)法。方法:采用Bruker Avance NEO 600型核磁共振波谱仪测定核磁共振氢谱(^(1)H NMR),脉冲序列zg30,弛豫延迟时间15 s,采样次数16,测定温度25℃,以咖啡因为内标,不... 目的:建立测定注射用微球专用溶剂中硅油含量的定量核磁共振氢谱(qHNMR)法。方法:采用Bruker Avance NEO 600型核磁共振波谱仪测定核磁共振氢谱(^(1)H NMR),脉冲序列zg30,弛豫延迟时间15 s,采样次数16,测定温度25℃,以咖啡因为内标,不加四甲基硅烷(TMS)的氘代氯仿为溶剂,对注射用微球专用溶剂中的硅油进行定量研究,以硅油定量峰与内标定量峰面积之比对其含量(μg)绘制标准曲线,计算注射用微球专用溶剂中硅油含量。结果:硅油含量在6~100μg范围内线性关系良好,r=0.9999,低、中、高浓度的平均回收率为97.8%(n=9),重复性RSD为9.8%。结论:该方法操作简单快捷、灵敏度高、结果准确,可用于注射用微球专用溶剂中硅油含量的测定。 展开更多
关键词 定量核磁共振氢谱法 注射用微球专用溶剂 硅油 含量测定 标准曲线法
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基于注汞法的液冷花岗岩微观特性实验研究
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作者 尹土兵 苏巨振 +1 位作者 庄登登 李夕兵 《Journal of Central South University》 SCIE EI CAS CSCD 2024年第1期169-181,共13页
在开采高温储层的过程中,微观特征变化重要影响深部热储层人工裂隙网络的建立。因此,研究该过程中微观特征的变化对深部地热能的安全高效开采具有重要意义。采用液体冷却(包括酸冷却和水冷却)处理高温花岗岩,模拟向高温储层注酸情况,以... 在开采高温储层的过程中,微观特征变化重要影响深部热储层人工裂隙网络的建立。因此,研究该过程中微观特征的变化对深部地热能的安全高效开采具有重要意义。采用液体冷却(包括酸冷却和水冷却)处理高温花岗岩,模拟向高温储层注酸情况,以获取相应条件下的花岗岩试样。随后,使用扫描电子显微镜-能量散射谱(SEM-EDS)和高压注汞法对样品进行测试。SEM-EDS结果显示,水冷却几乎不会影响元素的组成,酸冷却导致氧、硅和金属元素减少。在两种情况下,都观察到了孔隙和裂缝的形成。此外,与水冷却相比,酸冷却的样品表面更加不平整、疏松和粗糙。注汞法测试结果显示,随着处理温度的升高,液冷花岗岩样品的孔隙率、孔隙体积和比表面积有增加,但分形维数呈相反的趋势。研究结果表明,与水冷却相比,酸冷却条件对花岗岩的腐蚀作用使各项参数的变化更加显著,在酸冷却过程中产生更多的孔隙,提供更好的运输空间,使孔隙结构的复杂性降低。在高温储层的地热能有效提取方面,酸冷却具有更大应用潜力。 展开更多
关键词 孔隙结构 微观结构 液体冷却 土酸溶液 注汞法 花岗岩 分形理论
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致密砂岩储层微观孔喉结构及可动流体分布特征:以鄂尔多斯盆地东部神木地区盒8段储层为例
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作者 夏玉磊 兰建平 姚伟 《地质科技通报》 CAS CSCD 2024年第2期41-51,共11页
致密砂岩复杂的孔喉结构导致多变的可动流体分布,而微观孔隙结构和可动流体分布又是研究致密砂岩储层的重点。基于核磁共振可动流体测试原理,采用离心试验、高压压汞、扫描电镜、X射线衍射及铸体薄片等方法,建立了神木地区盒8段储层孔... 致密砂岩复杂的孔喉结构导致多变的可动流体分布,而微观孔隙结构和可动流体分布又是研究致密砂岩储层的重点。基于核磁共振可动流体测试原理,采用离心试验、高压压汞、扫描电镜、X射线衍射及铸体薄片等方法,建立了神木地区盒8段储层孔隙结构分类标准,明确了3类岩石孔隙结构参数及孔隙、喉道类型,提出了适用于目标储层转换系数的新方法,并定量评价了3类岩石可动流体分布特征。研究结果表明,目标储层中Ⅰ、Ⅱ类岩石孔隙以孔径大于10μm的残余粒间孔和孔径大于1μm的溶蚀孔为主,喉道以缩小型和弯片状喉道为主,孔隙结构参数较好,大孔隙发育程度高、孔喉间连通性好、可动流体赋存量大,大部分可动流体赋存于T_(2)谱右峰对应的大孔隙中,而左峰对应的小孔隙中可动流体含量低。Ⅲ类岩石孔隙结构参数差、可动流体百分比低、孔喉以晶间孔和管束状喉道为主。目标储层平均转换系数为0.029μm/ms,但Ⅰ、Ⅱ类岩石转换系数小于Ⅲ类,转换后的Ⅰ、Ⅱ类岩石T_(2)谱的右峰与压汞孔隙半径分布的主峰相对应,而Ⅲ类岩石T_(2)谱的左峰与压汞孔隙半径分布的主峰相对应。Ⅰ、Ⅱ类岩石孔径大于1μm的孔隙中可动流体百分比高,是未来勘探开发的主要方向。研究成果为提高致密油藏采收率提供了参考和借鉴。 展开更多
关键词 致密砂岩储层 高压压汞 核磁共振 可动流体 微观孔喉结构
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食品总汞测定中三种不同前处理方法的对比研究
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作者 王慧 吴炜 《食品安全导刊》 2024年第3期112-114,118,共4页
本文使用《食品安全国家标准食品中总汞及有机汞的测定》(GB 5009.17—2021)第四法“冷原子光谱法”对胡萝卜、豆角、大米、芹菜等8种标准物质中的总汞进行测定。采用直接进样法、快速消解法与微波消解法3种不同方式对样品进行处理,使用... 本文使用《食品安全国家标准食品中总汞及有机汞的测定》(GB 5009.17—2021)第四法“冷原子光谱法”对胡萝卜、豆角、大米、芹菜等8种标准物质中的总汞进行测定。采用直接进样法、快速消解法与微波消解法3种不同方式对样品进行处理,使用DMA-80型测汞仪进行测定。结果表明,快速消解法测定结果最为准确,8种标准物质检测结果均在标示值范围内。 展开更多
关键词 总汞 直接进样法 快速消解法 微波消解法
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苏里格气田A区块储层基础物性特征分析
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作者 万慈昡 胡维首 +2 位作者 沈雅斐 刘志凯 祝瑶 《能源与节能》 2024年第2期14-19,共6页
储层基础物性分析对了解气藏、制定气田开发方案及研究气井合理生产制度都至关重要。以苏里格气田A区块实物岩心为基础,依次开展基础孔渗、矿物成分、扫描电镜和高压压汞实验分析,分析储层的微观结构特征。实验结果表明:1)目标区域属于... 储层基础物性分析对了解气藏、制定气田开发方案及研究气井合理生产制度都至关重要。以苏里格气田A区块实物岩心为基础,依次开展基础孔渗、矿物成分、扫描电镜和高压压汞实验分析,分析储层的微观结构特征。实验结果表明:1)目标区域属于低孔低渗碳酸盐岩储层,非均质性强;2)岩石以脆性矿物为主,黏土矿物质量分数极小(大部分岩石中黏土矿物质量分数小于2.0%);3)孔隙以粒间孔为主,孔隙形态多样,纳米级微裂缝少见,填充度不高,缝洞呈现几何式特征;4)最大进汞饱和度差异大,孔喉结构不均匀,分选性差,孔喉半径小且分布广。 展开更多
关键词 基础物性 高压压汞 扫描电镜 矿物成分
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标准曲线的建立对原子荧光法测定水中汞准确度的影响
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作者 卜鑫 韩友虎 《皮革制作与环保科技》 2024年第4期5-7,共3页
通过建立两条不同标准模块下的标准曲线对原子荧光法测定水中汞的准确性进行研究,得出不同的两种标准曲线截距的正负值。采用仪器自动稀释模块的标准曲线具有操作简便、标准溶液校准点少、线性回归较好的优点。在对地表水、地下水及生... 通过建立两条不同标准模块下的标准曲线对原子荧光法测定水中汞的准确性进行研究,得出不同的两种标准曲线截距的正负值。采用仪器自动稀释模块的标准曲线具有操作简便、标准溶液校准点少、线性回归较好的优点。在对地表水、地下水及生活污水进行监测时,合理地扣除实验空白值的影响,保证了测定结果的精密度及准确度。 展开更多
关键词 标准曲线 原子荧光法 准确度
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Equation of Energy Injection to a Dielectric Barrier Discharge Reactor 被引量:1
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作者 姚水良 翁珊 +3 位作者 金旗 韩竞一 江博琼 吴祖良 《Plasma Science and Technology》 SCIE EI CAS CSCD 2016年第8期804-811,共8页
The electric energy injection from a pulsed power supply to a planar type of dielectric barrier discharge(DBD) reactor at atmospheric pressure was studied. Relations of the energy injection with barrier materials, bar... The electric energy injection from a pulsed power supply to a planar type of dielectric barrier discharge(DBD) reactor at atmospheric pressure was studied. Relations of the energy injection with barrier materials, barrier thickness, peak voltage, gap distance, electrode area,and operation temperature were experimentally investigated. The energy injection is a function of relative permittivity, barrier thickness, peak voltage, gap distance, and electrode area. The influence of operation temperature on energy injection is slight in the range of 27–300℃ but becomes obvious in the range of 300–500℃. A model was established using which the energy injection can be easily predicted. 展开更多
关键词 介质阻挡放电 放电反应器 电能量 方程 相对介电常数 峰值电压 电极面积 操作温度
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Pore-throat Structure of Tight Sandstone in Yanchang Formation of Huangling Mining Area Based on Scanning Electron Microscopy and Mercury Porosimmetry
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作者 Yajing SHI Xiaofu YANG 《Meteorological and Environmental Research》 CAS 2021年第4期57-61,64,共6页
Based on scanning electron microscopy and mercury porosimmetry,a large number of experimental data of pores and pore throats of tight sandstone reservoirs are obtained,and the characteristics of pore types,capillary p... Based on scanning electron microscopy and mercury porosimmetry,a large number of experimental data of pores and pore throats of tight sandstone reservoirs are obtained,and the characteristics of pore types,capillary pressure curves and quantitative parameters of pore throats of Yanchang Formation in Huangling mining area are studied.The results show that the main reservoir space types of Yanchang Formation sandstone are primary intergranular pores and feldspar dissolution pores.The pore-throat structure is medium-small pore and thin-small throat type,and the sorting is good to medium.The mercury porosimmetry curve shows a slightly coarse-thin skew.Combining the morphological characteristics of the mercury porosimmetry capillary pressure curve and the quantitative parameter characteristics of pore throats,the Yanchang Formation s micro pore structure is divided into types I,II,III,and IV.Tight oil reservoirs with type I and II pore structure characteristics are favorable.This study has reference significance for the later evaluation of tight sandstone reservoirs in Huangling mining area. 展开更多
关键词 Huangling mining area mercury porosimmetry Pore type Pore throat structure Capillary pressure curve
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