A novel micro fused-casting(MFC)process is developed for semisolid aluminum alloy slurry.The microstructure evolution and properties of semisolid ZL101 aluminum alloy slurry with difierent pouring temperature by MFC a...A novel micro fused-casting(MFC)process is developed for semisolid aluminum alloy slurry.The microstructure evolution and properties of semisolid ZL101 aluminum alloy slurry with difierent pouring temperature by MFC are investigated in this paper.During the cooling process,the effects of the pouring temperature on microstructure and properties is primarily analyzed.The microstructure of the semisolid ZL101 aluminum alloy is more homogeneous and the grain is smaller under proper pouring temperature.Temperature of liquids and solids of ZL101 aluminum alloy is measured by difierential scanning calorimetry(DSC).Distribution and characteristics of the microstructure of samples are examined by optical microscope(OM),scanning electron microscopy(SEM)equipped with energy dispersive spectrometer(EDS).The results show that the ZL101 semisolid slurry fabricated by MFC presents uniform shape and good grain size under the pouring temperature of 594°C and the stirring velocity of 600 r/min,and the fine grains of the primary a-Al phase with average grain size of 55μm and shape factor up to 0.67 were obtained.Besides,the ultimate tensile strength and the average Vickers hardness for semisolid ZL101 aluminum slurry are 178.19±1.37 MPa and 86.15±1.16 HV,respectively.展开更多
An advanced rheomoulder,which is a device in the integration of melting metal,storage,slurry preparation,transportation and injection forming,was introduced and used to manufacture rheomoulding AZ91 D alloy.Effects of...An advanced rheomoulder,which is a device in the integration of melting metal,storage,slurry preparation,transportation and injection forming,was introduced and used to manufacture rheomoulding AZ91 D alloy.Effects of pouring temperature and cylinder temperature on microstructures and mechanical properties of rheomoulding AZ91 D alloy were investigated.The results show that the process can obtain such rheomoulding AZ91 D in which primary α-Mg particles are fine,spherical and uniformly distributed in the matrix.With the decrease of pouring temperature,the morphology of primary α-Mg particles changes from coarse rosette-like to fine spherical shape gradually.As the cylinder temperature decreases,the average size of primary α-Mg particles decreases firstly and then substantially maintains stable while the sphericity and solid fraction increase continuously.Also,decreasing pouring temperature or cylinder temperature properly contributes to improving mechanical properties of rheomoulding AZ91 D for the refinement of α-Mg particles and the decrease of porosity fraction.Furthermore,rheomoulding AZ91 D performs much better than thixomoulding,rheo-diecasting and high pressure die-casting（HPDC） in terms of mechanical properties.Compared with HPDC,the tensile strength,yield strength and elongation are increased by 27.8%,15.7% and 121%,respectively.展开更多
The semi-solid slurry of ZL101 alloy is prepared by a combination technology of low superheat pouring and slightly electromagnetic stirring. The effects of pouring temperature on the slurry prepared by the technology ...The semi-solid slurry of ZL101 alloy is prepared by a combination technology of low superheat pouring and slightly electromagnetic stirring. The effects of pouring temperature on the slurry prepared by the technology are investigated. The results indicate that it is feasible to prepare the slurry with globular primary phases by low superheat pouring and slightly electromagnetic stirring, and that the pouring temperature has an important effect on the morphology and the size of primary α-AI in ZL101 alloy. By applying suitable slightly electromagnetic stirring combining with relatively increased pouring temperature, i.e., in a practical way to apply low superheat pouring technology, is capable of obtaining appropriate semi-solid slurry of ZL101 alloy with globular shape of primary phase. Compared with the samples made by low superheat pouring only without stirring, the samples prepared by applying both slightly electromagnetic stirring and low superheat pouring can enable to achieve the same grain size and morphology of the primary phase with that of pouring at 15-35℃ higher.展开更多
The preparation of semisolid slurry of A356 aluminum alloy using an oblique plate was investigated. A356 alloy melt undergoes partial solidification when it flows down on an oblique plate cooled from underneath by cou...The preparation of semisolid slurry of A356 aluminum alloy using an oblique plate was investigated. A356 alloy melt undergoes partial solidification when it flows down on an oblique plate cooled from underneath by counter flowing water. It results in continuous formation of columnar dendrites on plate wall. Due to forced convection, these dendrites are sheared off into equiaxed/fragmented grains and then washed away continuously to produce semisolid slurry at plate exit. Melt pouring temperature provides required condition of solidification whereas plate inclination enables necessary shear for producing semisolid slurry of desired quality. Slurry obtained was solidified in metal mould to produce semisolid-cast billets of desired microstructure. Furthermore, semisolid-cast billets were heat treated to improve surface quality. Microstructures of both semisolid-cast and heat-treated billets were analyzed. Effects of melt pouring temperature and plate inclination on solidification and microstructure of billets produced using oblique plate were described. The investigations involved four different melt pouring temperatures (620, 625, 630 and 635 °C) associated with four different plate inclinations (30°, 45°, 60° and 75°). Melt pouring temperature of 625 °C with plate inclination of 60° shows fine and globular microstructures and it is the optimum.展开更多
The effect of pouring temperature on thixotropic microstructure of AZ91 was investigated.The results show that the pouring temperature has a pronounced effect both on microstructural morphology and grain size.By decre...The effect of pouring temperature on thixotropic microstructure of AZ91 was investigated.The results show that the pouring temperature has a pronounced effect both on microstructural morphology and grain size.By decreasing the pouring temperature,the morphology of grains changes from coarse dendritic to fine dendritic structure.The fine dendritic structure that was obtained at low pouring temperature developed into a globular structure with a grain size of 60 μm,if the AZ91 was partially remelted and held isothermally at the semisolid state(575 ℃).On the other hand,if the alloy was poured at a high superheat,the particles were irregular and interconnected with a grain size of 180 μm even after 20 min of isothermal holding.展开更多
Pouring temperature and time are the most important influencing factors on interfacial reaction during the centrifugal casting. When cast at high temperatures, the crucible becomes brittle and prone to cracking, and s...Pouring temperature and time are the most important influencing factors on interfacial reaction during the centrifugal casting. When cast at high temperatures, the crucible becomes brittle and prone to cracking, and shows a low stability. In this paper, we studied the centrifugal casting of Ti-47.5-Al-2.5V-1Cr alloy, and explored the effects of pouring temperature on the interfacial reaction. Castings at 1 600, 1 650, and 1 700 ℃ were obtained by controlling the other parameters constant in the experiments. The microstructure, elemental distribution, thickness of the reaction layer and phase composition of the castings at the interface were studied. The results show that the thickness at the interfacial reaction layer is increased by raising the pouring temperature. The elements in the mold and the matrix were double-diffused and reacted at the interface during the casting process, and formed solid solutions with the precipitation of many new phases such as AlOand TiO. The roughness of interface structure and layer thickness of reaction increase with the rise of temperature, and the interfacial reaction is more intense. There is a minimum layer thickness of the reaction layer that is 80 μm when the temperature is 1 600 ℃.展开更多
Pouring and mold temperatures are two important parameters during casting magnesium components. The present study examined their influence on hot tearing susceptibility （HTS） of commercial AZ91D and newly developed ...Pouring and mold temperatures are two important parameters during casting magnesium components. The present study examined their influence on hot tearing susceptibility （HTS） of commercial AZ91D and newly developed Mg-3Nd-0.2Zn-Zr （mass fraction, %; NZ30K） magnesium alloys in gravity permanent mold casting condition. The results indicate that mold temperature shows much more significant influence on the HTS of both alloys than pouring temperature whose influence only can be distinguished at low mold temperature （341 K for AZ91D alloy and 423 K for NZ30K alloy）. Hot tearing susceptibility prediction model concerning feeding parameters, grain size and solidification range, is more suitable to estimate the HTS of different magnesium alloys than the model only concerning feeding parameters. In order to achieve better hot tearing resistance, the ranges of pouring and mold temperatures are suggested to be 961-991 K and≥641 K for AZ91D alloy, 1003-1033 K and≥623 K for NZ30K alloy, respectively.展开更多
This paper investigated the influences of pouring temperature and cooling rate on the microstructure development and mechanical properties for casting A1-Si-Cu aluminum alloy. The microstructure of the as-cast samples...This paper investigated the influences of pouring temperature and cooling rate on the microstructure development and mechanical properties for casting A1-Si-Cu aluminum alloy. The microstructure of the as-cast samples was characterized by an optical microscope. The results showed that the dendrite arm spacing （DAS,）,） is well refined by pouring at a higher temperature. The A decreases with increasing pouring temperature due to the multiplication of the nucleation sites in the superheating liquid melt, and the mechanical properties, such as microhardness and ultimate tensile strength increase correspondingly, while the elongation decreases. The relationships between microhardness and 3, for the samples cooled in metal mould and sand mould, are given as HV：l18.9 - 1.246A and HV=l15.2- 1.029A, respectively. The effects of the cooling rate controlled by using permanent mould casting and sand mould casing processes （the cooling medium is air and sand, respectively） on the dendrite arm spacing and mechanical properties are similar to the effect of the pouring temperature.展开更多
Based on the background of navigation lock structure engineering in Changsha Integrated Hub, this study used Parametric Design Language （APDL） compilation command on the t＇mite element program ANSAYS platforms to s...Based on the background of navigation lock structure engineering in Changsha Integrated Hub, this study used Parametric Design Language （APDL） compilation command on the t＇mite element program ANSAYS platforms to simulate the temperature field of the layered pouring process about the lower lock head. The temperature contour map and the change laws of temperature field with time in each different levels of the floor were obtained. And compared with the actual instrument measurement data, the feasibility of the simulation analysis was concluded. Then, this study optimized the pouring process, obtained the suitable methods of layered pouring and put forward the measures to reduce the concrete temperature crack.展开更多
The effects of pouring temperature, short electromagnetic stirring with low strength and then soaking treatment on the microstructure of AISi7Mg alloy were investigated. The results show that if AlSi7Mg alloy is poure...The effects of pouring temperature, short electromagnetic stirring with low strength and then soaking treatment on the microstructure of AISi7Mg alloy were investigated. The results show that if AlSi7Mg alloy is poured at 630 or 650℃ and meanwhile stirred by an electromagnetic field at a low power for a short time, the pouring process can be easily controlled and most solidified primary α-Al grains become spherical and only a few of them are rosette-like. Weak electromagnetic stirring makes the temperature field more homogeneous and makes the primary α-Al grains disperse in a larger region, which leads to the spherical microstructures of primary α-Al grains. When the AISi7Mg alloy is soaked or reheated at the semisolid state, the primary α-Al grains ripen further and they become more spherical, which is favorable to the semi-solid forming of AlSi7Mg alloy.展开更多
Some investigations have been carried out on hot tears in the A713 cast alloy, which is one of the long freezing range alloys, with objective to minimize/prevent hot tears. Experiments were conducted by varying pourin...Some investigations have been carried out on hot tears in the A713 cast alloy, which is one of the long freezing range alloys, with objective to minimize/prevent hot tears. Experiments were conducted by varying pouring temperatures at 700, 750, and 780 ℃ on the alloy with the addition of grain refiners like Al-2.5Ti-0.5C and Al-3.5Ti-1.5C. It was found that hot tearing was minimized by the addition of Al-3.5Ti-1.5C grain refiner, but grain refinement alone could not prevent hot tearing in A713 cast alloy. This has contradicted the findings of some earlier researchers. Experiments conducted on hot tearing with the addition of iron were found to be interesting. It was found that grain refinement along with iron addition to the A713 alloy has reduced the inter-dendritic separation so that interlocking could take place along the grain boundaries. Thus, iron, which comes as an impurity in commercial aluminum, can prevent hot tearing of A713 alloy.展开更多
In this article, semi-solid AlSiTMg alloy slurry was prepared by low superheat pouring and weak electromagnetic stirring. The effects of pouring temperature and stirring power on the microstructure of the AISiTMg allo...In this article, semi-solid AlSiTMg alloy slurry was prepared by low superheat pouring and weak electromagnetic stirring. The effects of pouring temperature and stirring power on the microstructure of the AISiTMg alloy slurry were studied. The results showed that the semi-solid AISiTMg alloy slurry, 127 mm in diameter, could be prepared by using the low superheat pouring and weak electromagnetic stirring technology and this new technology could save energy and make the pouring process convenient. When the liquid AISiTMg alloy was poured at 650℃ or 630℃, the solidified micrastructure of the AISiTMg alloy slurry, prepared by weak electromagnetic stirring, was remarkably improved when compared with that of the slurry prepared without stirring. The primary α-Al grains appeared rosette-like or spherical. When the pouring temperature was decreased, the shape of the primary α-Al grains gradually changed from dendritic-like grains to spherical grains. When the pouring temperature was appropriately increased, that is, raised to a certain superheat, the pouring process became easier and an ideal spherical microstructure of the AISiTMg alloy slurry, prepared by weak electromagnetic stirring, could also be obtained. In this experiment, when the stirring power was 0.36 kW, the optimized pouring temperature parameter was 630 ℃. When the AISiTMg alloy slurry was prepared by low superheat pouring and weak electromagnetic stirring, the pouring temperature was 630℃. Increasing the stirring power appropriately could gain better spherical primary α-Al grains, but if the stirring power was increased to a certain value, the shape of the primary α-Al grains did not improve further. In this experiment, the optimized stirring power parameter was 0.36 kW.展开更多
The effects of pouring temperature and short electromagnetic stirring with low strength on the microstructures of AlSi7Mg alloy were investigated. The results show that if liquid AlSi7Mg alloy is poured at 630 or 650...The effects of pouring temperature and short electromagnetic stirring with low strength on the microstructures of AlSi7Mg alloy were investigated. The results show that if liquid AlSi7Mg alloy is poured at 630 or 650℃, many primary α-Al grains in the solidified melt are rosette-like, and only a small number of them are spherical. However, if liquid AlSi7Mg alloy is poured at a lower superheat and meanwhile is stirred by an electromagnetic field at a low power for a short time, then most primary α-Al grains in the solidified melt become spherical, and only a few are rosette-like. The theoretical analysis indicates that the strengthened melt flow motion induced by the short electromagnetic stirring makes the temperature field more homogeneous in the melt, which is poured at a lower superheat, and makes the primary α-Al grains deposit in a larger region at the same time, so this new solidification kinetic condition leads to the microstructure of spherical primary α-Al grains. The experiments also demonstrate that pouring at an appropriate superheat and stirring by an electromagnetic field at a low power for a short time is a good new method for preparing the semi-solid slurry or billet of AlSi7Mg alloy.展开更多
Al-based Al−V master alloys were prepared by both the stepwise heating melting experiment and stepwise melting cooling experiment with rapid solidification to investigate the transformation of V-containing phases whic...Al-based Al−V master alloys were prepared by both the stepwise heating melting experiment and stepwise melting cooling experiment with rapid solidification to investigate the transformation of V-containing phases which gave different effects on microstructures and properties of commercial Al alloys and Ti alloys,as both melting and solidification processes affect the evolution of V-containing phases largely.The results showed that the raw Al−50wt.%V alloy consisted of needle-like Al_(3)V phase and Al8V5 phase(matrix),while petal-like Al_(3)V,needle-like Al_(7)V and plate-like Al_(10)V phase were present in the Al−V master alloys.The metastable Al_(7)V phase was evolved from Al_(3)V phase and then evolved into Al_(10)V phase during melting process.The number of Al_(10)V phase increased with the decrease of temperature in the range of 800−1000℃.Petal-like Al_(3)V phases could be transformed from Al_(8)V_(5) phase,pre-precipitated from Al−V molten liquid during melting process and precipitated directly during rapid solidification,respectively.展开更多
The semi-solid slurry of an A356 Al alloy, which was grain-fined by yttrium, was manufactured by low temperature pouring, The effects of grain-refining on the morphology and the grain size of the primary α phase in t...The semi-solid slurry of an A356 Al alloy, which was grain-fined by yttrium, was manufactured by low temperature pouring, The effects of grain-refining on the morphology and the grain size of the primary α phase in the semi-solid A356 Al alloy were researched. The results indicate that the semi-solid A356 AI alloy with particle-like and rosette-like primary α-Al can be prepared by low temperature pouring from a liquid grain-refined A356 alloy. The grain size and particle morphology of primary α-Al in the A356 Al alloy are markedly improved by the addition of 0.5 wt,% Y. The fining mechanism of Y on the morphology and grain size of the primary α-Al in the semi-solid A356 Al alloy was delved.展开更多
In this paper,two ways of micro structural characterization,optical microscopy(OM) and polarized light microscopy(PLM),were both employed to describe the micro structure of semisolid slurry prepared by swirling enthal...In this paper,two ways of micro structural characterization,optical microscopy(OM) and polarized light microscopy(PLM),were both employed to describe the micro structure of semisolid slurry prepared by swirling enthalpy equilibration device(SEED).The results show that PLM is more reliable and accurate than OM to describe the special morphology feature of semisolid slurry made by SEED process.Meanwhile,the effects of pouring temperature and mass of molten liquid on the primary α-Al particle size and morphology were also investigated using PLM.The quantitative metallographic results measured from PLM demonstrate that the grain size and morphology and their distribution are significantly affected by both pouring temperature and the mass of molten liquid.The grain size poured with 2.7 kg liquid decreases from 659 to186 μm,and grain morphology transforms from dendrite to globular structure with pouring temperature reducing from690 to 630℃.The decreasing pouring temperature also promotes the distribution of spherical structure on the cross section.Meanwhile,the mass of molten liquid decreasing from 2.7 to 2.3 kg can decrease the grain size by maximum of 44% at high pouring temperature.展开更多
The influence of rare earth lanthanum and pouring temperature on the fluidity of ADC 12 aluminum alloy was studied through spiral fluidity specimens by means of optical microscopy(OM) and differential thermal analyzer...The influence of rare earth lanthanum and pouring temperature on the fluidity of ADC 12 aluminum alloy was studied through spiral fluidity specimens by means of optical microscopy(OM) and differential thermal analyzer(DTA).The least squares regression method was used to give the best fitting between the function and the experimental data.The experimental results indicate that the rare earth lanthanum can significantly increase the fluidity of ADC 12 alloy.The fluidity increases with the addition of lanthanum.The DTA results indicate that with the addition of lanthanum,the range of crystallization temperature decreases,which increases the fluidity length.Especially,the range of crystallization temperature decreases by 32.66 % and the fluidity length is 1,321 mm(increased by 38.91%) when the addition of lanthanum is 0.6 wt%.Furthermore,with the increase of pouring temperatures,the fluidity length increases linearly between 670 and 760℃.展开更多
基金Funded by the National Natural Science Foundation of China(No.51341009)。
文摘A novel micro fused-casting(MFC)process is developed for semisolid aluminum alloy slurry.The microstructure evolution and properties of semisolid ZL101 aluminum alloy slurry with difierent pouring temperature by MFC are investigated in this paper.During the cooling process,the effects of the pouring temperature on microstructure and properties is primarily analyzed.The microstructure of the semisolid ZL101 aluminum alloy is more homogeneous and the grain is smaller under proper pouring temperature.Temperature of liquids and solids of ZL101 aluminum alloy is measured by difierential scanning calorimetry(DSC).Distribution and characteristics of the microstructure of samples are examined by optical microscope(OM),scanning electron microscopy(SEM)equipped with energy dispersive spectrometer(EDS).The results show that the ZL101 semisolid slurry fabricated by MFC presents uniform shape and good grain size under the pouring temperature of 594°C and the stirring velocity of 600 r/min,and the fine grains of the primary a-Al phase with average grain size of 55μm and shape factor up to 0.67 were obtained.Besides,the ultimate tensile strength and the average Vickers hardness for semisolid ZL101 aluminum slurry are 178.19±1.37 MPa and 86.15±1.16 HV,respectively.
基金Project(2011CB606302-1)supported by the National Basic Research Program of ChinaProject(2013AA031001)supported by High-tech Research and Development Program of China
文摘An advanced rheomoulder,which is a device in the integration of melting metal,storage,slurry preparation,transportation and injection forming,was introduced and used to manufacture rheomoulding AZ91 D alloy.Effects of pouring temperature and cylinder temperature on microstructures and mechanical properties of rheomoulding AZ91 D alloy were investigated.The results show that the process can obtain such rheomoulding AZ91 D in which primary α-Mg particles are fine,spherical and uniformly distributed in the matrix.With the decrease of pouring temperature,the morphology of primary α-Mg particles changes from coarse rosette-like to fine spherical shape gradually.As the cylinder temperature decreases,the average size of primary α-Mg particles decreases firstly and then substantially maintains stable while the sphericity and solid fraction increase continuously.Also,decreasing pouring temperature or cylinder temperature properly contributes to improving mechanical properties of rheomoulding AZ91 D for the refinement of α-Mg particles and the decrease of porosity fraction.Furthermore,rheomoulding AZ91 D performs much better than thixomoulding,rheo-diecasting and high pressure die-casting（HPDC） in terms of mechanical properties.Compared with HPDC,the tensile strength,yield strength and elongation are increased by 27.8%,15.7% and 121%,respectively.
基金supported by the Hi-tech Research and Development Program of China(Authorized No.G2002AA336080)the National Natural Science Foundation of China(Authorized No.50374012)the Natural Science Foundation of Jiangxi Province(Authorized No.0650047).
文摘The semi-solid slurry of ZL101 alloy is prepared by a combination technology of low superheat pouring and slightly electromagnetic stirring. The effects of pouring temperature on the slurry prepared by the technology are investigated. The results indicate that it is feasible to prepare the slurry with globular primary phases by low superheat pouring and slightly electromagnetic stirring, and that the pouring temperature has an important effect on the morphology and the size of primary α-AI in ZL101 alloy. By applying suitable slightly electromagnetic stirring combining with relatively increased pouring temperature, i.e., in a practical way to apply low superheat pouring technology, is capable of obtaining appropriate semi-solid slurry of ZL101 alloy with globular shape of primary phase. Compared with the samples made by low superheat pouring only without stirring, the samples prepared by applying both slightly electromagnetic stirring and low superheat pouring can enable to achieve the same grain size and morphology of the primary phase with that of pouring at 15-35℃ higher.
基金financial support received from Ministry of Mines, TIFAC, and Department of Science and Technology
文摘The preparation of semisolid slurry of A356 aluminum alloy using an oblique plate was investigated. A356 alloy melt undergoes partial solidification when it flows down on an oblique plate cooled from underneath by counter flowing water. It results in continuous formation of columnar dendrites on plate wall. Due to forced convection, these dendrites are sheared off into equiaxed/fragmented grains and then washed away continuously to produce semisolid slurry at plate exit. Melt pouring temperature provides required condition of solidification whereas plate inclination enables necessary shear for producing semisolid slurry of desired quality. Slurry obtained was solidified in metal mould to produce semisolid-cast billets of desired microstructure. Furthermore, semisolid-cast billets were heat treated to improve surface quality. Microstructures of both semisolid-cast and heat-treated billets were analyzed. Effects of melt pouring temperature and plate inclination on solidification and microstructure of billets produced using oblique plate were described. The investigations involved four different melt pouring temperatures (620, 625, 630 and 635 °C) associated with four different plate inclinations (30°, 45°, 60° and 75°). Melt pouring temperature of 625 °C with plate inclination of 60° shows fine and globular microstructures and it is the optimum.
基金This work is financially supported by Program on National Key Laboratory Foundation(No9140C500101060C50)
文摘The effect of pouring temperature on thixotropic microstructure of AZ91 was investigated.The results show that the pouring temperature has a pronounced effect both on microstructural morphology and grain size.By decreasing the pouring temperature,the morphology of grains changes from coarse dendritic to fine dendritic structure.The fine dendritic structure that was obtained at low pouring temperature developed into a globular structure with a grain size of 60 μm,if the AZ91 was partially remelted and held isothermally at the semisolid state(575 ℃).On the other hand,if the alloy was poured at a high superheat,the particles were irregular and interconnected with a grain size of 180 μm even after 20 min of isothermal holding.
基金Funded by the National Natural Science Foundation of China(No.51304198)Natural Science Foundation of Jiangsu Province(Nos.2013106,20141134 and 2014028-08)
文摘Pouring temperature and time are the most important influencing factors on interfacial reaction during the centrifugal casting. When cast at high temperatures, the crucible becomes brittle and prone to cracking, and shows a low stability. In this paper, we studied the centrifugal casting of Ti-47.5-Al-2.5V-1Cr alloy, and explored the effects of pouring temperature on the interfacial reaction. Castings at 1 600, 1 650, and 1 700 ℃ were obtained by controlling the other parameters constant in the experiments. The microstructure, elemental distribution, thickness of the reaction layer and phase composition of the castings at the interface were studied. The results show that the thickness at the interfacial reaction layer is increased by raising the pouring temperature. The elements in the mold and the matrix were double-diffused and reacted at the interface during the casting process, and formed solid solutions with the precipitation of many new phases such as AlOand TiO. The roughness of interface structure and layer thickness of reaction increase with the rise of temperature, and the interfacial reaction is more intense. There is a minimum layer thickness of the reaction layer that is 80 μm when the temperature is 1 600 ℃.
基金Project (2009AA033501) supported by the High-tech Research and Development Program of China
文摘Pouring and mold temperatures are two important parameters during casting magnesium components. The present study examined their influence on hot tearing susceptibility （HTS） of commercial AZ91D and newly developed Mg-3Nd-0.2Zn-Zr （mass fraction, %; NZ30K） magnesium alloys in gravity permanent mold casting condition. The results indicate that mold temperature shows much more significant influence on the HTS of both alloys than pouring temperature whose influence only can be distinguished at low mold temperature （341 K for AZ91D alloy and 423 K for NZ30K alloy）. Hot tearing susceptibility prediction model concerning feeding parameters, grain size and solidification range, is more suitable to estimate the HTS of different magnesium alloys than the model only concerning feeding parameters. In order to achieve better hot tearing resistance, the ranges of pouring and mold temperatures are suggested to be 961-991 K and≥641 K for AZ91D alloy, 1003-1033 K and≥623 K for NZ30K alloy, respectively.
基金financially supported by China Postdoctoral Science Foundation(No. 20110491492)the Natural Science Foundation of Jiangxi Province (No.20114BAB216017)Science Foundation of the Educational Department of Jiangxi Province (No. GJJ12035)
文摘This paper investigated the influences of pouring temperature and cooling rate on the microstructure development and mechanical properties for casting A1-Si-Cu aluminum alloy. The microstructure of the as-cast samples was characterized by an optical microscope. The results showed that the dendrite arm spacing （DAS,）,） is well refined by pouring at a higher temperature. The A decreases with increasing pouring temperature due to the multiplication of the nucleation sites in the superheating liquid melt, and the mechanical properties, such as microhardness and ultimate tensile strength increase correspondingly, while the elongation decreases. The relationships between microhardness and 3, for the samples cooled in metal mould and sand mould, are given as HV：l18.9 - 1.246A and HV=l15.2- 1.029A, respectively. The effects of the cooling rate controlled by using permanent mould casting and sand mould casing processes （the cooling medium is air and sand, respectively） on the dendrite arm spacing and mechanical properties are similar to the effect of the pouring temperature.
文摘Based on the background of navigation lock structure engineering in Changsha Integrated Hub, this study used Parametric Design Language （APDL） compilation command on the t＇mite element program ANSAYS platforms to simulate the temperature field of the layered pouring process about the lower lock head. The temperature contour map and the change laws of temperature field with time in each different levels of the floor were obtained. And compared with the actual instrument measurement data, the feasibility of the simulation analysis was concluded. Then, this study optimized the pouring process, obtained the suitable methods of layered pouring and put forward the measures to reduce the concrete temperature crack.
基金The work was supported by the National Hitech Research Foundation of China under grant No. G2002AA336080 by the National Natural Science Foundation of China under grant No. 50374012.
文摘The effects of pouring temperature, short electromagnetic stirring with low strength and then soaking treatment on the microstructure of AISi7Mg alloy were investigated. The results show that if AlSi7Mg alloy is poured at 630 or 650℃ and meanwhile stirred by an electromagnetic field at a low power for a short time, the pouring process can be easily controlled and most solidified primary α-Al grains become spherical and only a few of them are rosette-like. Weak electromagnetic stirring makes the temperature field more homogeneous and makes the primary α-Al grains disperse in a larger region, which leads to the spherical microstructures of primary α-Al grains. When the AISi7Mg alloy is soaked or reheated at the semisolid state, the primary α-Al grains ripen further and they become more spherical, which is favorable to the semi-solid forming of AlSi7Mg alloy.
文摘Some investigations have been carried out on hot tears in the A713 cast alloy, which is one of the long freezing range alloys, with objective to minimize/prevent hot tears. Experiments were conducted by varying pouring temperatures at 700, 750, and 780 ℃ on the alloy with the addition of grain refiners like Al-2.5Ti-0.5C and Al-3.5Ti-1.5C. It was found that hot tearing was minimized by the addition of Al-3.5Ti-1.5C grain refiner, but grain refinement alone could not prevent hot tearing in A713 cast alloy. This has contradicted the findings of some earlier researchers. Experiments conducted on hot tearing with the addition of iron were found to be interesting. It was found that grain refinement along with iron addition to the A713 alloy has reduced the inter-dendritic separation so that interlocking could take place along the grain boundaries. Thus, iron, which comes as an impurity in commercial aluminum, can prevent hot tearing of A713 alloy.
文摘In this article, semi-solid AlSiTMg alloy slurry was prepared by low superheat pouring and weak electromagnetic stirring. The effects of pouring temperature and stirring power on the microstructure of the AISiTMg alloy slurry were studied. The results showed that the semi-solid AISiTMg alloy slurry, 127 mm in diameter, could be prepared by using the low superheat pouring and weak electromagnetic stirring technology and this new technology could save energy and make the pouring process convenient. When the liquid AISiTMg alloy was poured at 650℃ or 630℃, the solidified micrastructure of the AISiTMg alloy slurry, prepared by weak electromagnetic stirring, was remarkably improved when compared with that of the slurry prepared without stirring. The primary α-Al grains appeared rosette-like or spherical. When the pouring temperature was decreased, the shape of the primary α-Al grains gradually changed from dendritic-like grains to spherical grains. When the pouring temperature was appropriately increased, that is, raised to a certain superheat, the pouring process became easier and an ideal spherical microstructure of the AISiTMg alloy slurry, prepared by weak electromagnetic stirring, could also be obtained. In this experiment, when the stirring power was 0.36 kW, the optimized pouring temperature parameter was 630 ℃. When the AISiTMg alloy slurry was prepared by low superheat pouring and weak electromagnetic stirring, the pouring temperature was 630℃. Increasing the stirring power appropriately could gain better spherical primary α-Al grains, but if the stirring power was increased to a certain value, the shape of the primary α-Al grains did not improve further. In this experiment, the optimized stirring power parameter was 0.36 kW.
基金This work was financially supported by the National Nature Science Foundation of China (No. 50374012), the National High-Tech Research and Development Program of China (863 Program) (No. 2006AA03Z115), and the National key Basic Research Foundation of China (No.2006CB605203).
文摘The effects of pouring temperature and short electromagnetic stirring with low strength on the microstructures of AlSi7Mg alloy were investigated. The results show that if liquid AlSi7Mg alloy is poured at 630 or 650℃, many primary α-Al grains in the solidified melt are rosette-like, and only a small number of them are spherical. However, if liquid AlSi7Mg alloy is poured at a lower superheat and meanwhile is stirred by an electromagnetic field at a low power for a short time, then most primary α-Al grains in the solidified melt become spherical, and only a few are rosette-like. The theoretical analysis indicates that the strengthened melt flow motion induced by the short electromagnetic stirring makes the temperature field more homogeneous in the melt, which is poured at a lower superheat, and makes the primary α-Al grains deposit in a larger region at the same time, so this new solidification kinetic condition leads to the microstructure of spherical primary α-Al grains. The experiments also demonstrate that pouring at an appropriate superheat and stirring by an electromagnetic field at a low power for a short time is a good new method for preparing the semi-solid slurry or billet of AlSi7Mg alloy.
基金financially supported by the National Natural Science Foundation of China (No.51804010)the 2020 Yuyou Talent Training Plan Project of North China University of Technology,China (No.214051360020XN212/014)the R&D Program of Beijing Municipal Education Commission,China (No.KM201910009007)。
文摘Al-based Al−V master alloys were prepared by both the stepwise heating melting experiment and stepwise melting cooling experiment with rapid solidification to investigate the transformation of V-containing phases which gave different effects on microstructures and properties of commercial Al alloys and Ti alloys,as both melting and solidification processes affect the evolution of V-containing phases largely.The results showed that the raw Al−50wt.%V alloy consisted of needle-like Al_(3)V phase and Al8V5 phase(matrix),while petal-like Al_(3)V,needle-like Al_(7)V and plate-like Al_(10)V phase were present in the Al−V master alloys.The metastable Al_(7)V phase was evolved from Al_(3)V phase and then evolved into Al_(10)V phase during melting process.The number of Al_(10)V phase increased with the decrease of temperature in the range of 800−1000℃.Petal-like Al_(3)V phases could be transformed from Al_(8)V_(5) phase,pre-precipitated from Al−V molten liquid during melting process and precipitated directly during rapid solidification,respectively.
基金the Natural Science Foundation of Jiangxi Province, China (No. 0650047)
文摘The semi-solid slurry of an A356 Al alloy, which was grain-fined by yttrium, was manufactured by low temperature pouring, The effects of grain-refining on the morphology and the grain size of the primary α phase in the semi-solid A356 Al alloy were researched. The results indicate that the semi-solid A356 AI alloy with particle-like and rosette-like primary α-Al can be prepared by low temperature pouring from a liquid grain-refined A356 alloy. The grain size and particle morphology of primary α-Al in the A356 Al alloy are markedly improved by the addition of 0.5 wt,% Y. The fining mechanism of Y on the morphology and grain size of the primary α-Al in the semi-solid A356 Al alloy was delved.
基金financially supported by the National Key Research and Development Program of China (No. 2016YFB0301003)the Shenzhen Free Exploring Basic Research Project (No. JCYJ20170307110223452)。
文摘In this paper,two ways of micro structural characterization,optical microscopy(OM) and polarized light microscopy(PLM),were both employed to describe the micro structure of semisolid slurry prepared by swirling enthalpy equilibration device(SEED).The results show that PLM is more reliable and accurate than OM to describe the special morphology feature of semisolid slurry made by SEED process.Meanwhile,the effects of pouring temperature and mass of molten liquid on the primary α-Al particle size and morphology were also investigated using PLM.The quantitative metallographic results measured from PLM demonstrate that the grain size and morphology and their distribution are significantly affected by both pouring temperature and the mass of molten liquid.The grain size poured with 2.7 kg liquid decreases from 659 to186 μm,and grain morphology transforms from dendrite to globular structure with pouring temperature reducing from690 to 630℃.The decreasing pouring temperature also promotes the distribution of spherical structure on the cross section.Meanwhile,the mass of molten liquid decreasing from 2.7 to 2.3 kg can decrease the grain size by maximum of 44% at high pouring temperature.
基金financially supported by the National Natural Science Foundation of China (Nos.51364035 and 51165032)the Special Research Fund for the Doctoral Program for Higher School (No.20133601110001)+1 种基金the Innovative Group of Science and Technology of College of Jiangxi Province (No. 00008713)the Production and Teaching and Research Cooperation Plan of Nanchang Non-Party Experts and Doctor (No.2012-CYH-DW-XCL-002)。
文摘The influence of rare earth lanthanum and pouring temperature on the fluidity of ADC 12 aluminum alloy was studied through spiral fluidity specimens by means of optical microscopy(OM) and differential thermal analyzer(DTA).The least squares regression method was used to give the best fitting between the function and the experimental data.The experimental results indicate that the rare earth lanthanum can significantly increase the fluidity of ADC 12 alloy.The fluidity increases with the addition of lanthanum.The DTA results indicate that with the addition of lanthanum,the range of crystallization temperature decreases,which increases the fluidity length.Especially,the range of crystallization temperature decreases by 32.66 % and the fluidity length is 1,321 mm(increased by 38.91%) when the addition of lanthanum is 0.6 wt%.Furthermore,with the increase of pouring temperatures,the fluidity length increases linearly between 670 and 760℃.
