[Objectives] Response surface analysis methodology was used to optimize the extraction technology of total flavonoids from Mallotus apelta leaves. [Methods] The total flavonoids were extracted using ultrasonic assiste...[Objectives] Response surface analysis methodology was used to optimize the extraction technology of total flavonoids from Mallotus apelta leaves. [Methods] The total flavonoids were extracted using ultrasonic assisted ethanol extraction,and extraction rate of total flavonoids was taken as evaluation index. On the basis of single-factor experiment,Box-Behnken response surface methodology was employed for selecting the optimum extraction process. [Results]The optimum extraction conditions of total flavonoids were as follows: 75% of ethanol concentration,1∶ 25 of ratio of material to liquid,31 min of ultrasonic time. Under these conditions,the extraction rate of total flavonoids was 1. 115%.[Conclusions] The extraction process obtained by response surface methodology was stable,reasonable,accurate and reliable. It was a feasible method to extract the total flavonoids from M. apelta leaves.展开更多
Levulinic acid(LA) has been identified as a promising green,biomass derived platform chemical.Response surface analysis(RSA) with a four-factor-five-level central composite design(CCD) was applied to optimize the hydr...Levulinic acid(LA) has been identified as a promising green,biomass derived platform chemical.Response surface analysis(RSA) with a four-factor-five-level central composite design(CCD) was applied to optimize the hydrolysis conditions for the conversion of bamboo(Phyllostachys Praecox f.preveynalis) shoot shell(BSS) to LA catalyzed with ionic liquid [C4mim]HSO4.The effects of four main reaction parameters including temperature,time,C[C4mim]HSO4(initial [C4mim]HSO4 concentration) and XBSS(initial BSS intake) on the hydrolysis reaction for yield of LA were analyzed.A quadratic equation model for yield of LA was established and fitted to the data with an R2 of 0.9868,and effects of main factors and their corresponding relationships were obtained with RSA.Model validation and results of CCD showed good correspondence between actual and predicted values.The analysis of variance(ANOVA) of the results indicated that the yield of LA in the range studied was significantly(P<0.05) affected by the four factors.The optimized reaction conditions were as follows:temperature of 145 ℃,time of 103.8 min,C[C4mim]HSO4 of 0.9 mol.L-1 and XBSS of 2.04%(by mass),respectively.A high yield [(71±0.41)%(by mol),triplicate experiment] was obtained at the optimum conditions of temperature of 145 ℃,time of 104 min,C[C4mim]HSO4 of 0.9 mol.L-1 and XBSS of 2%(by mass),which obtained from the real experiments,concurred with the model prediction [73.8%(by mol) based on available C6 sugars in BSS or 17.9%(by mass) based on the mass of BSS],indicating that the model was adequate for the hydrolysis process.展开更多
In semiconductor manufacturing process, probe station that is testing equipment is important. Inspection step is for detecting defects on semiconductor before the packaging. Probe card is a part of probe station and c...In semiconductor manufacturing process, probe station that is testing equipment is important. Inspection step is for detecting defects on semiconductor before the packaging. Probe card is a part of probe station and contains probe tip that contacts to semiconductor. Through probe tip, it can inspect defects of semiconductor. In this paper, optimization method is used with response surface analysis to design MEMS type probe tip. And fabricating probe tip uses maskless lithography, electro-plating and lapping process.展开更多
In order to enhance hydrolysis rate of bagasse, ultrasonic-assisted pretreatment is made in the experiment. The influence of addition of sulfuric acid, ultrasonic temperature, power and time to the hydrolysis of bagas...In order to enhance hydrolysis rate of bagasse, ultrasonic-assisted pretreatment is made in the experiment. The influence of addition of sulfuric acid, ultrasonic temperature, power and time to the hydrolysis of bagasse will be discussed in this paper. Optimal process and quadratic regression equation is obtained by using the response surface method. The yield of reducing sugar increases 6.5 percent after ultrasonic-assisted pretreatment. It demonstrates that the ultrasonic-assisted pretreatment can improve the hydrolysis rate of the bagasse.展开更多
A rotating packed bed is a typical chemical process enhancement equipment that can strengthen micromixing and mass transfer.During the operation of the rotating packed bed,the nonreactants and products irregularly adh...A rotating packed bed is a typical chemical process enhancement equipment that can strengthen micromixing and mass transfer.During the operation of the rotating packed bed,the nonreactants and products irregularly adhere to the wire mesh packing in the rotor,thus resulting in an imbalance in the vibration of the rotor,which may cause serious damage to the bearing and material leakage.This study proposes a model prediction for estimating the bearing residual life of a rotating packed bed based on rotor imbalance response analysis.This method is used to determine the influence of the mass on the imbalance in the vibration of the rotor on bearing damage.The major influence on rotor vibration was found to be exerted by the imbalanced mass and its distribution radius,as revealed by the results of orthogonal experiments.Through implementing finite element analysis,the imbalance response curve for the rotating packed bed rotor was obtained,and a correlation among rotor imbalance mass,distribution radius of imbalance mass,and bearing residue life was established via data fitting.The predicted value of the bearing life can be used as the reference basis for an early safety warning of a rotating packed bed to effectively avoid accidents.展开更多
Silver nanoparticles(AgNPs)synthesized using tartaric acid as a capping agent have a great impact on the reaction kinetics and contribute significantly to the stability of AgNPs.The protective layer formed by tartaric...Silver nanoparticles(AgNPs)synthesized using tartaric acid as a capping agent have a great impact on the reaction kinetics and contribute significantly to the stability of AgNPs.The protective layer formed by tartaric acid is an important factor that protects the silver surface and reduces potential cytotoxicity problems.These attributes are critical for assessing the compatibility of AgNPs with biological systems and making them suitable for drug delivery applications.The aim of this research is to conduct a comprehensive study of the effect of tartaric acid concentration,sonication time and temperature on the formation of silver nanoparticles.Using Response Surface Methodology(RSM)with Face-Centered Central Composite Design(FCCD),the optimization process identifies the most favorable synthesis conditions.UV-Vis spectrum regression analysis shows that AgNPs stabilized with tartaric acid are more stable than AgNPs without tartaric acid.This highlights the increased stability that tartaric acid provides in AgNP ssssynthesis.Particle size distribution analysis showed a multimodal distribution for AgNPs with tartaric acid and showed the smallest size peak with an average size of 20.53 nm.The second peak with increasing intensity shows a dominant average size of 108.8 nm accompanied by one standard deviation of 4.225 nm and a zeta potential of−11.08 mV.In contrast,AgNPs synthesized with polyvinylpyrrolidone(PVP)showed a unimodal particle distribution with an average particle size of 81.62 nm and a zeta potential of−2.96 mV.The more negative zeta potential of AgNP-tartaric acid indicates its increased stability.Evaluation of antibacterial activity showed that AgNPs stabilized with tartaric acid showed better performance against E.coli and B.subtilis bacteria compared with AgNPs-PVP.In summary,this study highlights the potential of tartaric acid in AgNP synthesis and suggests an avenue for the development of stable AgNPs with versatile applications.展开更多
In this study, coconut husk cellulose was employed as a cost-effective and environmentally friendly adsorbent to eliminate methylene blue (MB) dye from aqueous solutions. The successful development of response surface...In this study, coconut husk cellulose was employed as a cost-effective and environmentally friendly adsorbent to eliminate methylene blue (MB) dye from aqueous solutions. The successful development of response surface methodology paired with a central composite design (RSM-CCD) enabled the optimization and modelling of the adsorption process. The study investigated the individual and combined effects of three variables (pH, contact time, and initial MB dye concentration) on the adsorption of MB dye onto coconut husk cellulose. The developed RSM-CCD model exhibited a remarkable degree of precision in predicting the removal efficiency of MB dye within the specified experimental parameters. This was demonstrated by the strong regression parameters, with an R<sup>2</sup> value of 99.79% and an adjusted R<sup>2</sup> value of 99.6%. The study depicted that the optimal parameters for attaining a 98.8827% removal of MB dye using coconut husk cellulose were as follows: an initial MB dye concentration of 30 mg∙L<sup>−1</sup>, contact time of 120 minutes, and pH 7 at a fixed adsorbent dose of 0.5 g. The Freundlich isotherm model provided the most satisfactory description of the equilibrium adsorption isotherms, suggesting that MB dye adsorption onto coconut husk cellulose occurs on a heterogeneous surface. The experimental results demonstrated a strong agreement with the pseudo-second-order kinetics model, indicating that the number of active sites present on the cellulose adsorbent predominantly influences the adsorption process of MB dye. Additionally, the adsorbent made from coconut husk cellulose exhibited the potential to be reused, as it retained its efficiency for a maximum of three cycles of adsorption of MB dye. The results of this study show that coconut husk cellulose has the potential to be an effective and sustainable adsorbent for removing MB dye from aqueous solutions.展开更多
This study focuses on the extraction of cellulose nanocrystals (CNC), from microcrystalline cellulose (MCC), derived from Ayous sawdust. The process involves multiple steps and a large amount of chemical products. The...This study focuses on the extraction of cellulose nanocrystals (CNC), from microcrystalline cellulose (MCC), derived from Ayous sawdust. The process involves multiple steps and a large amount of chemical products. The objective of this research was to determine the effects of factors that impact the isolation process and to identify the optimal conditions for CNC isolation by using the response surface methodology. The factors that varied during the process were the quantity of MCC, the concentration of sulfuric acid, the hydrolysis time and temperature, and the ultrasonic treatment time. The response measured was the yield. The study found that with 5.80 g of microcrystalline cellulose, a sulfuric acid concentration of 63.50% (w/w), a hydrolysis time of 53 minutes, a hydrolysis temperature of 69˚C, and a sonication time of 19 minutes are the ideal conditions for isolation. The experimental yield achieved was (37.84 ± 0.99) %. The main factors influencing the process were the sulfuric acid concentration, hydrolysis time and temperature, with a significant influence (p < 0.05). Infrared characterization results showed that nanocrystals were indeed isolated. With a crystallinity of 35.23 and 79.74, respectively, for Ayous wood fiber and nanocrystalline cellulose were observed by X-ray diffraction, with the formation of type II cellulose, thermodynamically more stable than native cellulose type I.展开更多
In this paper,the effects of different influencing factors and factor interaction on the compressive strength and permeability of recycled aggregate pervious concrete(RAPC)were studied based on the response surface me...In this paper,the effects of different influencing factors and factor interaction on the compressive strength and permeability of recycled aggregate pervious concrete(RAPC)were studied based on the response surface method(RSM).By selecting the maximum aggregate size,water cement ratio and target porosity as design variables,combined with laboratory tests and numerical analysis,the influences of three factors on the compressive strength and permeability coefficient of RAPC were revealed.The regression equation of compressive strength and permeability coefficient of recycled aggregate pervious concrete were established based on RSM,and the response surface model was optimized to determine the optimal ratio of RAPC under the conditions of meeting the mechanical and permeability properties.The results show that the mismatch item of the model is not significant,the model is credible,and the accuracy and reliability of the test are high,but the degree of uncorrelation between the test data and the model is not obvious.The sensitivity of the three factors to the compressive strength is water cement ratio>maximum coarse aggregate particle size>target porosity,and the sensitivity to the permeability coefficient is target porosity>maximum coarse aggregate particle size>water cement ratio.The absolute errors of the model prediction results and the model optimization results are 1.28 MPa and 0.19 mm/s,and the relative errors are 5.06%and 4.19%,respectively.With high accuracy,RSM can match the measured results of compressive strength and permeability coefficient of RAPC.展开更多
Case history investigations have shown that pile foundations are more critically damaged in liquefiable soils than non-liquefiable soils.This study examines the differences in seismic response of pile foundations in l...Case history investigations have shown that pile foundations are more critically damaged in liquefiable soils than non-liquefiable soils.This study examines the differences in seismic response of pile foundations in liquefiable and non-liquefiable soils and their sensitivity to numerical model parameters.A two-dimensional finite element(FE)model is developed to simulate the experiment of a single pile foundation centrifuge in liquefiable soil subjected to earthquake motions and is validated against real-world test results.The differences in soil-pile seismic response of liquefiable and non-liquefiable soils are explored.Specifically,the first-order second-moment method(FOSM)is used for sensitivity analysis of the seismic response.The results show significant differences in seismic response for a soil-pile system between liquefiable and non-liquefiable soil.The seismic responses are found to be significantly larger in liquefiable soil than in non-liquefiable soil.Moreover,the pile bending moment was mainly affected by the kinematic effect in liquefiable soil,while the inertial effect was more significant in non-liquefiable soil.The controlling parameters of seismic response were PGA,soil density,and friction angle in liquefiable soil,while the pile bending moment was mainly controlled by PGA,the friction angle of soil,and shear modulus of loose sand in non-liquefiable soil.展开更多
For laser cladding a large temperature gradient easily weakened the surface quality by generating cracks and irregular coating surfaces,which in turn affected the bearing capacity and corrosion resistance of coatings ...For laser cladding a large temperature gradient easily weakened the surface quality by generating cracks and irregular coating surfaces,which in turn affected the bearing capacity and corrosion resistance of coatings in the rapid heating and cooling process.The response surface methodology(RSM)was used to predict coating cracks by changing the powder ratio,energy density,and preheating temperature,which obtained the relevant mathematical model.After that,the sensitivity of the crack length to process parameters was analyzed based on the sensitivity analysis method.The effect of Ni60/WC composite powder process parameters on the surface quality was revealed in laser cladding.The crack length first decreased and then increased,and the Smooth decreased with the increased powder ratio.The crack length and Smooth increased with the increased energy density.The crack length decreased and Smooth increased with the increased preheating temperature.Sensitivity analysis showed that the crack length and Smooth were the most sensitive to the powder ratio.Therefore,the process parameters were reasonably selected to control the surface quality.The mathematical model and sensitivity analysis method in the work could improve the surface quality,which provided a theoretical basis for the prediction and control of laser cladding cracks.展开更多
Due to the size effects of rockfill materials, the settlement difference between numerical simulation and in situ monitoring of rockfill dams is a topic of general concern.The constitutive model parameters obtained fr...Due to the size effects of rockfill materials, the settlement difference between numerical simulation and in situ monitoring of rockfill dams is a topic of general concern.The constitutive model parameters obtained from laboratory triaxial tests often underestimate the deformation of high rockfill dams.Therefore, constitutive model parameters obtained by back analysis were used to calculate and predict the long-term deformation of rockfill dams.Instead of using artificial neural networks (ANNs), the response surface method (RSM) was employed to replace the finite element simulation used in the optimization iteration.Only 27 training samples were required for RSM, improving computational efficiency compared with ANN, which required 300 training samples.RSM can be used to describe the relationship between the constitutive model parameters and dam settlements.The inversion results of the Shuibuya concrete face rockfill dam (CFRD) show that the calculated settlements agree with the measured data, indicating the accuracy and efficiency of RSM.展开更多
The innovative Subsurface Tension Leg Platform(STLP), which is designed to be located below Mean Water Level(M.W.L) to minimize direct wave loading and mitigate the effect of strong surface currents, is considered as ...The innovative Subsurface Tension Leg Platform(STLP), which is designed to be located below Mean Water Level(M.W.L) to minimize direct wave loading and mitigate the effect of strong surface currents, is considered as a competitive alternative system to support shallow-water rated well completion equipment and rigid risers for large ultra-deep water oil field development. A detailed description of the design philosophy of STLP has been published in the series of papers and patents. Nonetheless, design uncertainties arise as limited understanding of various parameters effects on the structural response of STLP, pertaining to the environmental loading, structural properties and hydrodynamic characteristics. This paper focuses on providing quantitative methodology on how each parameter affects the structural response of STLP, which will facilitate establishing the unique design criteria as regards to STLP. Firstly, the entire list of dimensionless groups of input and output parameters is proposed based on VaschyBuckingham theory. Then, numerical models are built and a series of numerical tests are carried out for validating the obtained dimensionless groups. On this basis, the calculation results of a great quantity of parametric studies on the structural response of STLP are presented and discussed in detail. Further, empirical formulae for predicting STLP response are derived through nonlinear regression analysis. Finally, conclusions and discussions are made. It has been demonstrated that the study provides a methodology for better control of key parameters and lays the foundation for optimal design of STLP. The obtained conclusions also have wide ranging applicability in reference to the engineering design and design analysis aspects of deepwater buoy supporting installations, such as Grouped SLOR or TLR system.展开更多
The fatigue life of aeroengine turbine disc presents great dispersion due to the randomness of the basic variables,such as applied load,working temperature,geometrical dimensions and material properties.In order to am...The fatigue life of aeroengine turbine disc presents great dispersion due to the randomness of the basic variables,such as applied load,working temperature,geometrical dimensions and material properties.In order to ameliorate reliability analysis efficiency without loss of reliability,the distributed collaborative response surface method(DCRSM) was proposed,and its basic theories were established in this work.Considering the failure dependency among the failure modes,the distributed response surface was constructed to establish the relationship between the failure mode and the relevant random variables.Then,the failure modes were considered as the random variables of system response to obtain the distributed collaborative response surface model based on structure failure criterion.Finally,the given turbine disc structure was employed to illustrate the feasibility and validity of the presented method.Through the comparison of DCRSM,Monte Carlo method(MCM) and the traditional response surface method(RSM),the results show that the computational precision for DCRSM is more consistent with MCM than RSM,while DCRSM needs far less computing time than MCM and RSM under the same simulation conditions.Thus,DCRSM is demonstrated to be a feasible and valid approach for improving the computational efficiency of reliability analysis for aeroengine turbine disc fatigue life with multiple random variables,and has great potential value for the complicated mechanical structure with multi-component and multi-failure mode.展开更多
Caulerpa sertularioides is an invasive potential blooming green alga in China but it remains poorly studied.We studied the effects of ecological factors on its growth.Optimum conditions of ecological factors,i.e.,irra...Caulerpa sertularioides is an invasive potential blooming green alga in China but it remains poorly studied.We studied the effects of ecological factors on its growth.Optimum conditions of ecological factors,i.e.,irradiance,temperature,and salinity,for the growth of its fragments were determined in the response surface methodology(RSM).The specific growth rates(SGR)of the fragments were determined in single-factor experiment.The results show that the SGR of C.sertularioides peaked under the conditions of irradiance 37.5μmol/(m~2·s),temperature25℃,and salinity 30.Meanwhile,using the Box-Behnken design,the conditions were further optimized and verified to be:irradiance 39.03μmol/(m~2·s),temperature 25.29℃,and salinity 30.06,under which the SGR reached 4.66%.The results provide new theoretical data and solutions for the cultivation,invasion prediction,and monitoring of Caulerpa species in China and the world.The RSM method may have great potential applications in the environmental adaptation characteristics of new macroalgal cultivars,intensive orientation cultured germplasm,and environmental hazard analysis of cultivated species in the field.展开更多
In order to comprehensively utilize the remaining bamboo residue of bamboo products,this paper presents a research on recycling the bamboo fibers from bamboo residue for improving the performance of the asphalt mixtur...In order to comprehensively utilize the remaining bamboo residue of bamboo products,this paper presents a research on recycling the bamboo fibers from bamboo residue for improving the performance of the asphalt mixtures.First of all,the basic performance parameters of sinocalamus affinis fiber,phyllostachys pubescens fiber,green bamboo fiber were tested and analyzed,and the optimal content and length were put forward.Then,the mix ratio design of the bamboo fiber modified asphalt mixture was further designed through the response surface method,and was verified the rationality of the mix ratio.Finally,the mixture specimens were made according to the experimental design mix ratio,and the high temperature,low temperature performance and moisture susceptibility of the bamboo fiber modified mixtures asphalt were tested.The results showed that the high temperature performance,low temperature performance and moisture susceptibility of bamboo fiber modified asphalt mixtures were improved compared with the performance of SBS modified asphalt mixture.When the length of bamboo fiber is 7.25 mm and the content of 0.22%,the road performance of the asphalt mixture was optimal.Consequentially,the decomposition of bamboo residue into bamboo fiber and its application in asphalt pavement can improve the reuse of bamboo waste,with remarkable environmental benefits and great promotion value.展开更多
The flow field induced by internal solitary waves(ISWs)is peculiar wherein water motion occurs in the whole water depth,and the strong shear near the pycnocline can be generated due to the opposite flow direction betw...The flow field induced by internal solitary waves(ISWs)is peculiar wherein water motion occurs in the whole water depth,and the strong shear near the pycnocline can be generated due to the opposite flow direction between the upper and lower layers,which is a potential threat to marine risers.In this paper,the flow field of ISWs is obtained with the Korteweg-de Vries(Kd V)equation for a two-layer fluid system.Then,a linear analysis is performed for the dynamic response of a riser with its two ends simply supported under the action of ISWs.The explicit expressions of the deflection and the moment of the riser are deduced based on the modal superposition method.The applicable conditions of the theoretical expressions are discussed.Through comparisons with the finite element simulations for nonlinear dynamic responses,it is proved that the theoretical expressions can roughly reveal the nonlinear dynamic response of risers under ISWs when the approximation for the linear analysis is relaxed to some extent.展开更多
This study aimed to investigate optimal fermentation conditions of biological acetic acid fermentation for vinegar production. Optimization was performed on 3 acetic acid bacteria strains namely VMA1, VMA7 and VMAO us...This study aimed to investigate optimal fermentation conditions of biological acetic acid fermentation for vinegar production. Optimization was performed on 3 acetic acid bacteria strains namely VMA1, VMA7 and VMAO using Response Surface Methodology (RSM). A Box-Behnken-Design (BBD) was achieved with three different independent process parameters involving: fermentation temperature, original alcohol concentration and original acetic acid concentration and one dependent variable (acetic acid yield). The results showed that the mathematical models describe correctly the relationship between responses and factors (F values of the models (p R<sup>2</sup> (coefficient of correlation) respectively 0.96, 0.94, 0.98, and adjusted R<sup>2</sup> 0.95, 0.92, 0.98). The maximum acidity was obtained respectively at fermentation temperatures, original alcohol concentrations and original acetic acid concentrations ranging from [37.5°C - 45°C], [16% - 20% (v/v)], [1.5% - 2% (w/v)] for VMA1, [40°C - 45°C], [14.5% - 20% (v/v)], [1.7% - 2% (w/v)] for VMA7 and [42°C - 45°C], [17% - 20% (v/v)], [1.5% - 2% (w/v)] for VMAO. The use of these acetic strains in the production of vinegar may seriously lead to a decrease or even an ablation of the costs related to the cooling of bioreactors especially in warm and hot countries, in the context of global warming.展开更多
Waste Glass(WGs)and Coir Fiber(CF)are not widely utilized,even though their silica and cellulose content can be used to create construction materials.This study aimed to optimize mortar compressive strength using Resp...Waste Glass(WGs)and Coir Fiber(CF)are not widely utilized,even though their silica and cellulose content can be used to create construction materials.This study aimed to optimize mortar compressive strength using Response Surface Methodology(RSM).The Central Composite Design(CCD)was applied to determine the optimization of WGs and CF addition to the mortar compressive strength.Compressive strength and microstructure testing with Scanning Electron Microscope(SEM),Fourier-transform Infrared Spectroscopy(FT-IR),and X-Ray Diffraction(XRD)were conducted to specify the mechanical ability and bonding between the matrix,CF,and WGs.The results showed that the chemical treatment of CF produced 49.15%cellulose,with an average particle size of 1521μm.The regression of a second-order polynomial model yielded an optimum composition consisting of 12.776%WGs and 2.344%CF with a predicted compressive strength of 19.1023 MPa.C-S-H gels were identified in the mortars due to the dissolving of SiO_(2) in WGs and cement.The silica from WGs increased the C-S-H phase.CF plays a role in preventing,bridging,and branching micro-cracks before reaching maximum stress.WGs aggregates and chemically treated CF are suitable to be composited in mortar to increase compressive strength.展开更多
In this paper,the residue from bamboo factory has been used to design photo-Fenton catalyst,which has the advantages of low cost and magnetic recycling.The photo-Fenton catalytic performance of the biocarbon-based cat...In this paper,the residue from bamboo factory has been used to design photo-Fenton catalyst,which has the advantages of low cost and magnetic recycling.The photo-Fenton catalytic performance of the biocarbon-based catalyst was excellent and its optimal preparation process was also explored by response surface methodology.First,bamboo-carbon fiber was selected as the photo-Fenton catalyst carrier.Subsequently,the surface of the car-bon fiber was modified,with which dopamine,nano-Fe_(3)O_(4) and nano-TiO_(2) were successively loaded by hydro-thermal method.After the single factor tests,four factors including dopamine concentration,ferric chloride mass,P25 titanium dioxide mass and liquid-solid ratio were selected as the characteristic values.The degradation efficiency of photo-Fenton catalyst to methylene blue(MB)solution was treated as the response value.After the analysis of the response surface optimization,it was shown that the significance sequence of the selected 4 factors in terms of the MB degradation efficiency was arranged as follows:dopamine concentration>liquid-solid ratio>P25 titanium dioxide quality>ferric chloride quality.The optimal process parameters of fiber-carbon catalyst were affirmed as follows:the 1.7 mg/mL concentration of dopamine,the 1.2 g mass of ferric chloride,the 0.2 g mass of P25 titanium dioxide and the liquid-solid ratio of 170 mL/g.The experiment-measured average MB degra-dation efficiency performed by the optimized catalyst was 99.3%,which was nearly similar to the model-predicted value of 98.9%.It showed that the prediction model and response surface model were accurate and reliable.The results from response surface optimization could provide a good reference to design bamboo-based Fenton-like catalyst with excellent catalytic performance.展开更多
基金Supported by the Program of Guilin Municipal Science and Technology Bureau(20130403-4)Science and Technology Program of Traditional Chinese Medicine from Guangxi Administration of Traditional Chinese Medicine(GZLC14-31)Undergraduate Innovation and Entrepreneurship Training Plan Project of Autonomous District Level in 2017(201710601082)
文摘[Objectives] Response surface analysis methodology was used to optimize the extraction technology of total flavonoids from Mallotus apelta leaves. [Methods] The total flavonoids were extracted using ultrasonic assisted ethanol extraction,and extraction rate of total flavonoids was taken as evaluation index. On the basis of single-factor experiment,Box-Behnken response surface methodology was employed for selecting the optimum extraction process. [Results]The optimum extraction conditions of total flavonoids were as follows: 75% of ethanol concentration,1∶ 25 of ratio of material to liquid,31 min of ultrasonic time. Under these conditions,the extraction rate of total flavonoids was 1. 115%.[Conclusions] The extraction process obtained by response surface methodology was stable,reasonable,accurate and reliable. It was a feasible method to extract the total flavonoids from M. apelta leaves.
基金Supported by the National Natural Science Foundation of China（30940058,31170672）the Natural Science Foundation of Zhejiang Province of China（Y3110025）+1 种基金Key Laboratory for Physical Processing of Agricultural Products（JAPP2010-4）Key Laboratory of Exploitation and Preservation of Coastal Bio-resource（2010F30003）
文摘Levulinic acid(LA) has been identified as a promising green,biomass derived platform chemical.Response surface analysis(RSA) with a four-factor-five-level central composite design(CCD) was applied to optimize the hydrolysis conditions for the conversion of bamboo(Phyllostachys Praecox f.preveynalis) shoot shell(BSS) to LA catalyzed with ionic liquid [C4mim]HSO4.The effects of four main reaction parameters including temperature,time,C[C4mim]HSO4(initial [C4mim]HSO4 concentration) and XBSS(initial BSS intake) on the hydrolysis reaction for yield of LA were analyzed.A quadratic equation model for yield of LA was established and fitted to the data with an R2 of 0.9868,and effects of main factors and their corresponding relationships were obtained with RSA.Model validation and results of CCD showed good correspondence between actual and predicted values.The analysis of variance(ANOVA) of the results indicated that the yield of LA in the range studied was significantly(P<0.05) affected by the four factors.The optimized reaction conditions were as follows:temperature of 145 ℃,time of 103.8 min,C[C4mim]HSO4 of 0.9 mol.L-1 and XBSS of 2.04%(by mass),respectively.A high yield [(71±0.41)%(by mol),triplicate experiment] was obtained at the optimum conditions of temperature of 145 ℃,time of 104 min,C[C4mim]HSO4 of 0.9 mol.L-1 and XBSS of 2%(by mass),which obtained from the real experiments,concurred with the model prediction [73.8%(by mol) based on available C6 sugars in BSS or 17.9%(by mass) based on the mass of BSS],indicating that the model was adequate for the hydrolysis process.
文摘In semiconductor manufacturing process, probe station that is testing equipment is important. Inspection step is for detecting defects on semiconductor before the packaging. Probe card is a part of probe station and contains probe tip that contacts to semiconductor. Through probe tip, it can inspect defects of semiconductor. In this paper, optimization method is used with response surface analysis to design MEMS type probe tip. And fabricating probe tip uses maskless lithography, electro-plating and lapping process.
文摘In order to enhance hydrolysis rate of bagasse, ultrasonic-assisted pretreatment is made in the experiment. The influence of addition of sulfuric acid, ultrasonic temperature, power and time to the hydrolysis of bagasse will be discussed in this paper. Optimal process and quadratic regression equation is obtained by using the response surface method. The yield of reducing sugar increases 6.5 percent after ultrasonic-assisted pretreatment. It demonstrates that the ultrasonic-assisted pretreatment can improve the hydrolysis rate of the bagasse.
基金the High-Performance Computing Platform of Beijing University of Chemical Technology(BUCT)for supporting this papersupported by the Fundamental Research Funds for the Central Universities(JD2319)+2 种基金the CNOOC Technical Cooperation Project(ZX2022ZCTYF7612)the National Natural Science Foundation of China(51775029,52004014)the Chinese Universities Scientific Fund(XK2020-04)。
文摘A rotating packed bed is a typical chemical process enhancement equipment that can strengthen micromixing and mass transfer.During the operation of the rotating packed bed,the nonreactants and products irregularly adhere to the wire mesh packing in the rotor,thus resulting in an imbalance in the vibration of the rotor,which may cause serious damage to the bearing and material leakage.This study proposes a model prediction for estimating the bearing residual life of a rotating packed bed based on rotor imbalance response analysis.This method is used to determine the influence of the mass on the imbalance in the vibration of the rotor on bearing damage.The major influence on rotor vibration was found to be exerted by the imbalanced mass and its distribution radius,as revealed by the results of orthogonal experiments.Through implementing finite element analysis,the imbalance response curve for the rotating packed bed rotor was obtained,and a correlation among rotor imbalance mass,distribution radius of imbalance mass,and bearing residue life was established via data fitting.The predicted value of the bearing life can be used as the reference basis for an early safety warning of a rotating packed bed to effectively avoid accidents.
基金funded by the Directorate of Research and Community Service (DRPM,Direktorat Riset dan Pengabdian Kepada Masyarakat)ITS through the ITS Research Local Grant (No:1665/PKS/ITS/2023).
文摘Silver nanoparticles(AgNPs)synthesized using tartaric acid as a capping agent have a great impact on the reaction kinetics and contribute significantly to the stability of AgNPs.The protective layer formed by tartaric acid is an important factor that protects the silver surface and reduces potential cytotoxicity problems.These attributes are critical for assessing the compatibility of AgNPs with biological systems and making them suitable for drug delivery applications.The aim of this research is to conduct a comprehensive study of the effect of tartaric acid concentration,sonication time and temperature on the formation of silver nanoparticles.Using Response Surface Methodology(RSM)with Face-Centered Central Composite Design(FCCD),the optimization process identifies the most favorable synthesis conditions.UV-Vis spectrum regression analysis shows that AgNPs stabilized with tartaric acid are more stable than AgNPs without tartaric acid.This highlights the increased stability that tartaric acid provides in AgNP ssssynthesis.Particle size distribution analysis showed a multimodal distribution for AgNPs with tartaric acid and showed the smallest size peak with an average size of 20.53 nm.The second peak with increasing intensity shows a dominant average size of 108.8 nm accompanied by one standard deviation of 4.225 nm and a zeta potential of−11.08 mV.In contrast,AgNPs synthesized with polyvinylpyrrolidone(PVP)showed a unimodal particle distribution with an average particle size of 81.62 nm and a zeta potential of−2.96 mV.The more negative zeta potential of AgNP-tartaric acid indicates its increased stability.Evaluation of antibacterial activity showed that AgNPs stabilized with tartaric acid showed better performance against E.coli and B.subtilis bacteria compared with AgNPs-PVP.In summary,this study highlights the potential of tartaric acid in AgNP synthesis and suggests an avenue for the development of stable AgNPs with versatile applications.
文摘In this study, coconut husk cellulose was employed as a cost-effective and environmentally friendly adsorbent to eliminate methylene blue (MB) dye from aqueous solutions. The successful development of response surface methodology paired with a central composite design (RSM-CCD) enabled the optimization and modelling of the adsorption process. The study investigated the individual and combined effects of three variables (pH, contact time, and initial MB dye concentration) on the adsorption of MB dye onto coconut husk cellulose. The developed RSM-CCD model exhibited a remarkable degree of precision in predicting the removal efficiency of MB dye within the specified experimental parameters. This was demonstrated by the strong regression parameters, with an R<sup>2</sup> value of 99.79% and an adjusted R<sup>2</sup> value of 99.6%. The study depicted that the optimal parameters for attaining a 98.8827% removal of MB dye using coconut husk cellulose were as follows: an initial MB dye concentration of 30 mg∙L<sup>−1</sup>, contact time of 120 minutes, and pH 7 at a fixed adsorbent dose of 0.5 g. The Freundlich isotherm model provided the most satisfactory description of the equilibrium adsorption isotherms, suggesting that MB dye adsorption onto coconut husk cellulose occurs on a heterogeneous surface. The experimental results demonstrated a strong agreement with the pseudo-second-order kinetics model, indicating that the number of active sites present on the cellulose adsorbent predominantly influences the adsorption process of MB dye. Additionally, the adsorbent made from coconut husk cellulose exhibited the potential to be reused, as it retained its efficiency for a maximum of three cycles of adsorption of MB dye. The results of this study show that coconut husk cellulose has the potential to be an effective and sustainable adsorbent for removing MB dye from aqueous solutions.
文摘This study focuses on the extraction of cellulose nanocrystals (CNC), from microcrystalline cellulose (MCC), derived from Ayous sawdust. The process involves multiple steps and a large amount of chemical products. The objective of this research was to determine the effects of factors that impact the isolation process and to identify the optimal conditions for CNC isolation by using the response surface methodology. The factors that varied during the process were the quantity of MCC, the concentration of sulfuric acid, the hydrolysis time and temperature, and the ultrasonic treatment time. The response measured was the yield. The study found that with 5.80 g of microcrystalline cellulose, a sulfuric acid concentration of 63.50% (w/w), a hydrolysis time of 53 minutes, a hydrolysis temperature of 69˚C, and a sonication time of 19 minutes are the ideal conditions for isolation. The experimental yield achieved was (37.84 ± 0.99) %. The main factors influencing the process were the sulfuric acid concentration, hydrolysis time and temperature, with a significant influence (p < 0.05). Infrared characterization results showed that nanocrystals were indeed isolated. With a crystallinity of 35.23 and 79.74, respectively, for Ayous wood fiber and nanocrystalline cellulose were observed by X-ray diffraction, with the formation of type II cellulose, thermodynamically more stable than native cellulose type I.
基金supported by the Jiangsu Water Conservancy Science and Technology Project of China(2016036).
文摘In this paper,the effects of different influencing factors and factor interaction on the compressive strength and permeability of recycled aggregate pervious concrete(RAPC)were studied based on the response surface method(RSM).By selecting the maximum aggregate size,water cement ratio and target porosity as design variables,combined with laboratory tests and numerical analysis,the influences of three factors on the compressive strength and permeability coefficient of RAPC were revealed.The regression equation of compressive strength and permeability coefficient of recycled aggregate pervious concrete were established based on RSM,and the response surface model was optimized to determine the optimal ratio of RAPC under the conditions of meeting the mechanical and permeability properties.The results show that the mismatch item of the model is not significant,the model is credible,and the accuracy and reliability of the test are high,but the degree of uncorrelation between the test data and the model is not obvious.The sensitivity of the three factors to the compressive strength is water cement ratio>maximum coarse aggregate particle size>target porosity,and the sensitivity to the permeability coefficient is target porosity>maximum coarse aggregate particle size>water cement ratio.The absolute errors of the model prediction results and the model optimization results are 1.28 MPa and 0.19 mm/s,and the relative errors are 5.06%and 4.19%,respectively.With high accuracy,RSM can match the measured results of compressive strength and permeability coefficient of RAPC.
基金National Science Foundation for Excellent Young Scholars of China under Grant No.51722801National Natural Science Foundation of China under Grant Nos.51808006 and 52078016。
文摘Case history investigations have shown that pile foundations are more critically damaged in liquefiable soils than non-liquefiable soils.This study examines the differences in seismic response of pile foundations in liquefiable and non-liquefiable soils and their sensitivity to numerical model parameters.A two-dimensional finite element(FE)model is developed to simulate the experiment of a single pile foundation centrifuge in liquefiable soil subjected to earthquake motions and is validated against real-world test results.The differences in soil-pile seismic response of liquefiable and non-liquefiable soils are explored.Specifically,the first-order second-moment method(FOSM)is used for sensitivity analysis of the seismic response.The results show significant differences in seismic response for a soil-pile system between liquefiable and non-liquefiable soil.The seismic responses are found to be significantly larger in liquefiable soil than in non-liquefiable soil.Moreover,the pile bending moment was mainly affected by the kinematic effect in liquefiable soil,while the inertial effect was more significant in non-liquefiable soil.The controlling parameters of seismic response were PGA,soil density,and friction angle in liquefiable soil,while the pile bending moment was mainly controlled by PGA,the friction angle of soil,and shear modulus of loose sand in non-liquefiable soil.
基金supported by Science and Technology Major Project of Fujian Province(Grant No.2020HZ03018).
文摘For laser cladding a large temperature gradient easily weakened the surface quality by generating cracks and irregular coating surfaces,which in turn affected the bearing capacity and corrosion resistance of coatings in the rapid heating and cooling process.The response surface methodology(RSM)was used to predict coating cracks by changing the powder ratio,energy density,and preheating temperature,which obtained the relevant mathematical model.After that,the sensitivity of the crack length to process parameters was analyzed based on the sensitivity analysis method.The effect of Ni60/WC composite powder process parameters on the surface quality was revealed in laser cladding.The crack length first decreased and then increased,and the Smooth decreased with the increased powder ratio.The crack length and Smooth increased with the increased energy density.The crack length decreased and Smooth increased with the increased preheating temperature.Sensitivity analysis showed that the crack length and Smooth were the most sensitive to the powder ratio.Therefore,the process parameters were reasonably selected to control the surface quality.The mathematical model and sensitivity analysis method in the work could improve the surface quality,which provided a theoretical basis for the prediction and control of laser cladding cracks.
基金supported by the National Natural Science Foundation of China(Grant No.51579193)the Science and Technology Planning Project of Guizhou Province(Grant No.[2016]1154)
文摘Due to the size effects of rockfill materials, the settlement difference between numerical simulation and in situ monitoring of rockfill dams is a topic of general concern.The constitutive model parameters obtained from laboratory triaxial tests often underestimate the deformation of high rockfill dams.Therefore, constitutive model parameters obtained by back analysis were used to calculate and predict the long-term deformation of rockfill dams.Instead of using artificial neural networks (ANNs), the response surface method (RSM) was employed to replace the finite element simulation used in the optimization iteration.Only 27 training samples were required for RSM, improving computational efficiency compared with ANN, which required 300 training samples.RSM can be used to describe the relationship between the constitutive model parameters and dam settlements.The inversion results of the Shuibuya concrete face rockfill dam (CFRD) show that the calculated settlements agree with the measured data, indicating the accuracy and efficiency of RSM.
基金financially supported by the National Natural Science Foundation of China(Grant No.51709041)China Postdoctoral Science Foundation(Grant Nos.2017M610178 and 2018T110224)the Fundamental Research Funds for the Central Universities(Grant No.DUT18RC(4)069)
文摘The innovative Subsurface Tension Leg Platform(STLP), which is designed to be located below Mean Water Level(M.W.L) to minimize direct wave loading and mitigate the effect of strong surface currents, is considered as a competitive alternative system to support shallow-water rated well completion equipment and rigid risers for large ultra-deep water oil field development. A detailed description of the design philosophy of STLP has been published in the series of papers and patents. Nonetheless, design uncertainties arise as limited understanding of various parameters effects on the structural response of STLP, pertaining to the environmental loading, structural properties and hydrodynamic characteristics. This paper focuses on providing quantitative methodology on how each parameter affects the structural response of STLP, which will facilitate establishing the unique design criteria as regards to STLP. Firstly, the entire list of dimensionless groups of input and output parameters is proposed based on VaschyBuckingham theory. Then, numerical models are built and a series of numerical tests are carried out for validating the obtained dimensionless groups. On this basis, the calculation results of a great quantity of parametric studies on the structural response of STLP are presented and discussed in detail. Further, empirical formulae for predicting STLP response are derived through nonlinear regression analysis. Finally, conclusions and discussions are made. It has been demonstrated that the study provides a methodology for better control of key parameters and lays the foundation for optimal design of STLP. The obtained conclusions also have wide ranging applicability in reference to the engineering design and design analysis aspects of deepwater buoy supporting installations, such as Grouped SLOR or TLR system.
基金Project(51335003)supported by the National Natural Science Foundation of ChinaProject(20111102110011)supported by the Specialized Research Fund for the Doctoral Program of Higher Education of China
文摘The fatigue life of aeroengine turbine disc presents great dispersion due to the randomness of the basic variables,such as applied load,working temperature,geometrical dimensions and material properties.In order to ameliorate reliability analysis efficiency without loss of reliability,the distributed collaborative response surface method(DCRSM) was proposed,and its basic theories were established in this work.Considering the failure dependency among the failure modes,the distributed response surface was constructed to establish the relationship between the failure mode and the relevant random variables.Then,the failure modes were considered as the random variables of system response to obtain the distributed collaborative response surface model based on structure failure criterion.Finally,the given turbine disc structure was employed to illustrate the feasibility and validity of the presented method.Through the comparison of DCRSM,Monte Carlo method(MCM) and the traditional response surface method(RSM),the results show that the computational precision for DCRSM is more consistent with MCM than RSM,while DCRSM needs far less computing time than MCM and RSM under the same simulation conditions.Thus,DCRSM is demonstrated to be a feasible and valid approach for improving the computational efficiency of reliability analysis for aeroengine turbine disc fatigue life with multiple random variables,and has great potential value for the complicated mechanical structure with multi-component and multi-failure mode.
基金The National Natural Science Foundation of China under contract Nos 31970216,32270219 and 31670199。
文摘Caulerpa sertularioides is an invasive potential blooming green alga in China but it remains poorly studied.We studied the effects of ecological factors on its growth.Optimum conditions of ecological factors,i.e.,irradiance,temperature,and salinity,for the growth of its fragments were determined in the response surface methodology(RSM).The specific growth rates(SGR)of the fragments were determined in single-factor experiment.The results show that the SGR of C.sertularioides peaked under the conditions of irradiance 37.5μmol/(m~2·s),temperature25℃,and salinity 30.Meanwhile,using the Box-Behnken design,the conditions were further optimized and verified to be:irradiance 39.03μmol/(m~2·s),temperature 25.29℃,and salinity 30.06,under which the SGR reached 4.66%.The results provide new theoretical data and solutions for the cultivation,invasion prediction,and monitoring of Caulerpa species in China and the world.The RSM method may have great potential applications in the environmental adaptation characteristics of new macroalgal cultivars,intensive orientation cultured germplasm,and environmental hazard analysis of cultivated species in the field.
基金Funded by the Key Research and Development Projects in Shaanxi Province(No.2022SF-328)Science and Technology Project of Shaanxi Department of Transportation(Nos.19-10K,19-28K)Science and Technology Project of Henan Department of Transportation(No.2020J-2-3)。
文摘In order to comprehensively utilize the remaining bamboo residue of bamboo products,this paper presents a research on recycling the bamboo fibers from bamboo residue for improving the performance of the asphalt mixtures.First of all,the basic performance parameters of sinocalamus affinis fiber,phyllostachys pubescens fiber,green bamboo fiber were tested and analyzed,and the optimal content and length were put forward.Then,the mix ratio design of the bamboo fiber modified asphalt mixture was further designed through the response surface method,and was verified the rationality of the mix ratio.Finally,the mixture specimens were made according to the experimental design mix ratio,and the high temperature,low temperature performance and moisture susceptibility of the bamboo fiber modified mixtures asphalt were tested.The results showed that the high temperature performance,low temperature performance and moisture susceptibility of bamboo fiber modified asphalt mixtures were improved compared with the performance of SBS modified asphalt mixture.When the length of bamboo fiber is 7.25 mm and the content of 0.22%,the road performance of the asphalt mixture was optimal.Consequentially,the decomposition of bamboo residue into bamboo fiber and its application in asphalt pavement can improve the reuse of bamboo waste,with remarkable environmental benefits and great promotion value.
基金Project supported by the National Natural Science Foundation of China(Nos.12132018,11972352,12202455)the Strategic Priority Research Program of the Chinese Academy of Sciences of China(No.XDA22000000)。
文摘The flow field induced by internal solitary waves(ISWs)is peculiar wherein water motion occurs in the whole water depth,and the strong shear near the pycnocline can be generated due to the opposite flow direction between the upper and lower layers,which is a potential threat to marine risers.In this paper,the flow field of ISWs is obtained with the Korteweg-de Vries(Kd V)equation for a two-layer fluid system.Then,a linear analysis is performed for the dynamic response of a riser with its two ends simply supported under the action of ISWs.The explicit expressions of the deflection and the moment of the riser are deduced based on the modal superposition method.The applicable conditions of the theoretical expressions are discussed.Through comparisons with the finite element simulations for nonlinear dynamic responses,it is proved that the theoretical expressions can roughly reveal the nonlinear dynamic response of risers under ISWs when the approximation for the linear analysis is relaxed to some extent.
文摘This study aimed to investigate optimal fermentation conditions of biological acetic acid fermentation for vinegar production. Optimization was performed on 3 acetic acid bacteria strains namely VMA1, VMA7 and VMAO using Response Surface Methodology (RSM). A Box-Behnken-Design (BBD) was achieved with three different independent process parameters involving: fermentation temperature, original alcohol concentration and original acetic acid concentration and one dependent variable (acetic acid yield). The results showed that the mathematical models describe correctly the relationship between responses and factors (F values of the models (p R<sup>2</sup> (coefficient of correlation) respectively 0.96, 0.94, 0.98, and adjusted R<sup>2</sup> 0.95, 0.92, 0.98). The maximum acidity was obtained respectively at fermentation temperatures, original alcohol concentrations and original acetic acid concentrations ranging from [37.5°C - 45°C], [16% - 20% (v/v)], [1.5% - 2% (w/v)] for VMA1, [40°C - 45°C], [14.5% - 20% (v/v)], [1.7% - 2% (w/v)] for VMA7 and [42°C - 45°C], [17% - 20% (v/v)], [1.5% - 2% (w/v)] for VMAO. The use of these acetic strains in the production of vinegar may seriously lead to a decrease or even an ablation of the costs related to the cooling of bioreactors especially in warm and hot countries, in the context of global warming.
基金funded by the Ministry of Education,Culture,Research,and the Technology,Indonesia for Matching Fund (Kedaireka)Scheme in 2022 with Contract No.155/E1/KS.06.02/2022.
文摘Waste Glass(WGs)and Coir Fiber(CF)are not widely utilized,even though their silica and cellulose content can be used to create construction materials.This study aimed to optimize mortar compressive strength using Response Surface Methodology(RSM).The Central Composite Design(CCD)was applied to determine the optimization of WGs and CF addition to the mortar compressive strength.Compressive strength and microstructure testing with Scanning Electron Microscope(SEM),Fourier-transform Infrared Spectroscopy(FT-IR),and X-Ray Diffraction(XRD)were conducted to specify the mechanical ability and bonding between the matrix,CF,and WGs.The results showed that the chemical treatment of CF produced 49.15%cellulose,with an average particle size of 1521μm.The regression of a second-order polynomial model yielded an optimum composition consisting of 12.776%WGs and 2.344%CF with a predicted compressive strength of 19.1023 MPa.C-S-H gels were identified in the mortars due to the dissolving of SiO_(2) in WGs and cement.The silica from WGs increased the C-S-H phase.CF plays a role in preventing,bridging,and branching micro-cracks before reaching maximum stress.WGs aggregates and chemically treated CF are suitable to be composited in mortar to increase compressive strength.
基金funding from Hunan Provincial Key Research and Development Program(2020WK2018)Hunan Provincial Forestry Technological Innovation Funds(XLK202107-3)+2 种基金Scientific Research Project of Hunan Education Department(19A505,21B0242)National Natural Science Foundation of China(No.21908251)Hunan Provincial Natural Science Foundation of China(No.2020JJ2058).
文摘In this paper,the residue from bamboo factory has been used to design photo-Fenton catalyst,which has the advantages of low cost and magnetic recycling.The photo-Fenton catalytic performance of the biocarbon-based catalyst was excellent and its optimal preparation process was also explored by response surface methodology.First,bamboo-carbon fiber was selected as the photo-Fenton catalyst carrier.Subsequently,the surface of the car-bon fiber was modified,with which dopamine,nano-Fe_(3)O_(4) and nano-TiO_(2) were successively loaded by hydro-thermal method.After the single factor tests,four factors including dopamine concentration,ferric chloride mass,P25 titanium dioxide mass and liquid-solid ratio were selected as the characteristic values.The degradation efficiency of photo-Fenton catalyst to methylene blue(MB)solution was treated as the response value.After the analysis of the response surface optimization,it was shown that the significance sequence of the selected 4 factors in terms of the MB degradation efficiency was arranged as follows:dopamine concentration>liquid-solid ratio>P25 titanium dioxide quality>ferric chloride quality.The optimal process parameters of fiber-carbon catalyst were affirmed as follows:the 1.7 mg/mL concentration of dopamine,the 1.2 g mass of ferric chloride,the 0.2 g mass of P25 titanium dioxide and the liquid-solid ratio of 170 mL/g.The experiment-measured average MB degra-dation efficiency performed by the optimized catalyst was 99.3%,which was nearly similar to the model-predicted value of 98.9%.It showed that the prediction model and response surface model were accurate and reliable.The results from response surface optimization could provide a good reference to design bamboo-based Fenton-like catalyst with excellent catalytic performance.
