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基于SEM的土体微观结构三维分析与分维计算方法
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作者 张豫川 高旭龙 +1 位作者 刘东发 黄鸿伟 《长江科学院院报》 CSCD 北大核心 2024年第2期91-97,共7页
土体微观结构研究很早就建立了三维空间的分形模型,但分形维数计算所需参数很难由常规土工试验得到,限制了分形理论在土体研究中的应用。基于陕西定边与甘肃兰州原状土样的扫描电镜(SEM)试验,提出了三维化处理与三角形网格原理联合方法... 土体微观结构研究很早就建立了三维空间的分形模型,但分形维数计算所需参数很难由常规土工试验得到,限制了分形理论在土体研究中的应用。基于陕西定边与甘肃兰州原状土样的扫描电镜(SEM)试验,提出了三维化处理与三角形网格原理联合方法,可以得到土体颗粒(孔隙)不同测量尺度对应的表面积与体积计算值,由此实现分形维数的计算,并通过分形理论在土水特征中的应用验证了方法的有效性与可靠性。另外,三维化处理还可获取视孔隙率、比面等土体微观结构参数,可以作为土体微观结构定量分析研究的新途径。 展开更多
关键词 扫描电镜(sem) 微观结构 三维分析 分形维数
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Chalkiness Characters and Scanning Electron Microscope Observation of Rice Grain Endosperm of Japonica Varieties in Southern Henan 被引量:5
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作者 Bo PENG Yanfang SUN +8 位作者 Dongyan KONG Ruihua PANG Xiaohua SONG Huilong LI Jintao LI Qiying ZHOU Qiu HAN Shizhi SONG Hongyu YUAN 《Asian Agricultural Research》 2017年第3期80-85,共6页
Chalkiness characters affect not only the grain appearance,milling,eating and cooking qualities but also the grain nutritional quality in rice,thus it is one of the most important traits in rice. It is very important ... Chalkiness characters affect not only the grain appearance,milling,eating and cooking qualities but also the grain nutritional quality in rice,thus it is one of the most important traits in rice. It is very important for us to investigate the relation of the chalkiness formation and the development of endosperm structure and starch granule of different rice varieties. Here,we have investigated the chalkiness characters such as chalkiness rate,chalkiness degree and chalkiness area in 15 japonica rice varieties from southern Henan. Furthermore,the endosperm structure and starch granules of rice grain were also observed with scanning electron microscope. The results showed that the 15 japonica varieties have a significantly linear relationship between the chalkiness rate and chalkiness degree. Among the varieties,the biggest difference is the chalkiness rate,the second is the chalkiness area,and the last is the chalkiness degree. Moreover,there is a certain correlation between the distribution of starch granules,the arrangement of endosperm cells and the occurrence of grain chalkiness in the different rice varieties. For the same variety,the starch granules of chalky and non-chalky grains have obvious difference,while the starch granules from the transparent part of chalky rice and non-chalky rice do not have significant difference. The results would provide useful references for the improvement of grain quality in rice. 展开更多
关键词 CHALKINESS scanning electron microscope Japonica rice Starch granule ENDOSPERM
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Adverse Effects of Permanent Waving and Hair Relaxation—Assessment by Scanning Electron Microscopy (SEM)
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作者 Tokuya Omi Seiji Kawana 《Journal of Cosmetics, Dermatological Sciences and Applications》 2013年第3期45-48,共4页
Permanent waving is very popular in Japan. Polypeptide chains (main chains) form the principal components of hair, and they are lined up longitudinally. Hair relaxation is also called straight permanent waving, and th... Permanent waving is very popular in Japan. Polypeptide chains (main chains) form the principal components of hair, and they are lined up longitudinally. Hair relaxation is also called straight permanent waving, and there are methods that change curly or wavy hair into straight hair. Hair damage as a result of winding, combing, and using high-temperature hairdressing irons is also often seen. By using scanning electron micrographs (SEM) we showed broken hairs and hair damage caused by permanent wave solutions. The hair damage is obvious when comparisons are made with the condition of the hair surface, condition of the cuticle, etc. Hair swelling by permanent wave solutions, manipulations such as winding, etc., inadequate rinsing with water, procedures on injured hair at the outset, etc., are considered possible reasons for any of these types of injury. 展开更多
关键词 PERMANENT Waving HAIR RELAXATION scanning electron MICROGRAPHS (sem) HAIR Damage
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致密砂岩碳酸盐矿物SEM-CL和EPMA矿物学表征及其成岩意义——以川西坳陷须家河组为例
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作者 余瑜 林良彪 +3 位作者 李真 孟万斌 童馗 梁庆韶 《沉积学报》 CAS CSCD 北大核心 2023年第5期1468-1477,共10页
扫描电镜—阴极发光(SEM-CL)可通过同时分析矿物的微观结构和阴极发光特性来反映成岩机制及流体来源,但碳酸盐矿物在SEM-CL下的发光特性及其影响因素尚不明确。应用光学显微镜阴极发光(OM-CL)、电子探针(EPMA)和SEM-CL等技术手段,以川... 扫描电镜—阴极发光(SEM-CL)可通过同时分析矿物的微观结构和阴极发光特性来反映成岩机制及流体来源,但碳酸盐矿物在SEM-CL下的发光特性及其影响因素尚不明确。应用光学显微镜阴极发光(OM-CL)、电子探针(EPMA)和SEM-CL等技术手段,以川西坳陷须家河组致密砂岩中碳酸盐矿物为研究对象,分析碳酸盐矿物在OM-CL和SEM-CL下发光特性的差异,评估影响碳酸盐矿物SEM-CL发光特性的因素,探讨砂岩中方解石胶结物的成岩意义。结果表明,相比OM-CL,SEM-CL在区分碳酸盐岩屑和碳酸盐胶结物方面具有更高的灵敏度。当Mn/Fe值低于0.1或Mn/Fe值介于0.1~0.5且Fe含量低于0.1%时,碳酸盐矿物具有中低强度的SEM-CL发光强度;当Mn/Fe值高于0.5且Fe含量高于0.1%时,碳酸盐矿物在SEM-CL照射下几乎不发光。Mn/Fe值和Fe含量是影响SEM-CL照射下碳酸盐矿物发光强度的主要因素。阴极发光分析和EPMA元素组成面扫描分析表明,方解石胶结物的元素分布是均质的,形成于同一成岩世代,晚于长石等矿物的溶解。岩屑砂岩和岩屑石英砂岩的方解石胶结物具有相同的来源,表现为高Mn/Fe特征;钙屑砂岩的方解石胶结物具低Mn高Fe特征,成分组成与白云石岩屑相似,推测流体可能受到白云石岩屑溶解的影响。 展开更多
关键词 方解石胶结物 扫描电镜—阴极发光 成岩作用 致密砂岩 须家河组 四川盆地
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Surface characteristics analysis of fractures induced by supercritical CO_(2)and water through three-dimensional scanning and scanning electron micrography 被引量:3
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作者 Hao Chen Yi Hu +4 位作者 Jiawei Liu Feng Liu Zheng Liu Yong Kang Xiaochuan Wang 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2021年第5期1047-1058,共12页
Morphology of hydraulic fracture surface has significant effects on oil and gas flow,proppant migration and fracture closure,which plays an important role in oil and gas fracturing stimulation.In this paper,we analyze... Morphology of hydraulic fracture surface has significant effects on oil and gas flow,proppant migration and fracture closure,which plays an important role in oil and gas fracturing stimulation.In this paper,we analyzed the fracture surface characteristics induced by supercritical carbon dioxide(SC-CO_(2))and water in open-hole and perforation completion conditions under triaxial stresses.A simple calculation method was proposed to quantitatively analyze the fracture surface area and roughness in macro-level based on three-dimensional(3D)scanning data.In micro-level,scanning electron micrograph(SEM)was used to analyze the features of fracture surface.The results showed that the surface area of the induced fracture increases with perforation angle for both SC-CO_(2)and water fracturing,and the surface area of SC-CO_(2)-induced fracture is 6.49%e58.57%larger than that of water-induced fracture.The fractal dimension and surface roughness of water-induced fractures increase with the increase in perforation angle,while those of SC-CO_(2)-induced fractures decrease with the increasing perforation angle.A considerable number of microcracks and particle peeling pits can be observed on SC-CO_(2)-induced fracture surface while there are more flat particle surfaces in water-induced fracture surface through SEM images,indicating that fractures tend to propagate along the boundary of the particle for SC-CO_(2)fracturing while water-induced fractures prefer to cut through particles.These findings are of great significance for analyzing fracture mechanism and evaluating fracturing stimulation performance. 展开更多
关键词 Supercritical carbon dioxide(SC-CO_(2))fracturing Quantitative characterization of surface features Surface roughness and fractal dimension Three-dimensional(3D)scanning scanning electron micrograph(sem)
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SCANNING ELECTRON MICROSCOPIC STUDY OF FETAL CHICKEN CALVARIAL OSTEOBLAST-LIKE CELLS CULTURED IN VITRO 被引量:1
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作者 柴本甫 汤雪明 +1 位作者 徐荣辉 朱雅萍 《Medical Bulletin of Shanghai Jiaotong University》 CAS 1993年第2期54-59,共6页
Three types of osteoblast-like cells with different cnfigurations could be ob-tained through culturing fetal chicken calvaria in vitro. They were spindle-shaped cells,globular cells, and polygonal or squamous cells. W... Three types of osteoblast-like cells with different cnfigurations could be ob-tained through culturing fetal chicken calvaria in vitro. They were spindle-shaped cells,globular cells, and polygonal or squamous cells. With passage of culture time, there werechanges in configuration so that the spindle-shaped cells and the globular cells turnedgradually into squamous cells, in quantity which increased greatly to produce confluenceand multi-layer formation of cells, and in function as evidenced by emergence ofintracytoplasmic granules, reflecting collagen synthesis. 展开更多
关键词 osteoblast-like cells FETAL CHICKEN CALVARIA in VITRO scanning electron microscope
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Ultrastructural Analysis of the Ontogenetic Development of Shoot Induced from Embryonic Axes of Costa Rican Bean Varieties (<i>Phaseolus vulgaris</i>L.) under <i>in Vitro</i>Conditions by Scanning Electronic Microscopy
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作者 Marisol Jiménez Andrés Gatica +1 位作者 Ethel Sánchez Marta Valdez 《American Journal of Plant Sciences》 2012年第4期489-494,共6页
Common bean (Phaseolus vulgaris L.) is an economic important crop and one of the major grain legumes for human consumption in Latin America, Africa and Asia. A morphological study of shoot induced from embryonic axes ... Common bean (Phaseolus vulgaris L.) is an economic important crop and one of the major grain legumes for human consumption in Latin America, Africa and Asia. A morphological study of shoot induced from embryonic axes development in four Costa Rican bean varieties (Brunca, Huetar, Guaymi and Bribri) cultivated on MS media with or without 5 mg·L–1 de N6-benzylaminopurine (BAP) by scanning electron microscopy (SEM) was developed in the present work. Micrographs showed similarities and differences in the ultrastructure of the apical dome, epidermal surface, stomata and different types of trichomes in the varieties cultivated on organogenesis media. Genotypes with advantageous morphological characteristics for genetic transformation, in particular an exposed apical dome, were identified. This work will contribute to the optimization of the in vitro regeneration of four common bean varieties. 展开更多
关键词 PHASEOLUS vulgaris L BEAN In Vitro ORGANOGENESIS SHOOT scanning electron Microscopy (sem)
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Electronic Scanning of Uterine Endometrium in Postpartum Cow
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作者 TIANWen-ru HEJian-bin 《Journal of Northeast Agricultural University(English Edition)》 CAS 2000年第2期118-124,共7页
Two postpartum cows were used to study the ultrastructural changes of uterine endometrium by using scanning electron microscope.The results showed that the process of repair of uterine endometrium after calving was de... Two postpartum cows were used to study the ultrastructural changes of uterine endometrium by using scanning electron microscope.The results showed that the process of repair of uterine endometrium after calving was demonstrated by scanning electron microscope through a series of endometrium biopsy.Some part of the endometrium was damaged after calving and its adjacent endometrium cells became necrosis and exfoliated during the first 7 days post-partum;the cilium and microvillus of the epithelial cell in the undamaged area of the endometrium disappeared.By 26 days postpartum the damaged area reduced and the cilium and microvillus increased in their numbers.The damaged tissues were all repaired by day 60 postpartum. 展开更多
关键词 产后母牛 体内寄生虫 显微镜观察 子宫 放射性扫描 生理性状
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Scanning Electron Microscopic Observation on Morphologic Characteristics of Sperms in Uremic Patients
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作者 Long-gen XU Shi-fang SHI +6 位作者 Hai-zhen ZHONG Xiao-feng HUANG Xiao-ping QI Qi-zhe SONG Xin-hong WANG Li YAN Zong-fu SHAO 《Journal of Reproduction and Contraception》 CAS 2004年第4期227-232,共6页
Objective To observe the morphologic characteristics of spermatozoon ultramicro- scopic structure in uremic subjects Method Semen sample from 10 patients with uremia and 5 healthy men were observed under light microsc... Objective To observe the morphologic characteristics of spermatozoon ultramicro- scopic structure in uremic subjects Method Semen sample from 10 patients with uremia and 5 healthy men were observed under light microscope and scanning electronic microscope. Results Abnormalities were found in sperms of uremic patients either in the sperm head (acrosome, acrosomic deficit, nuclear abnormality, pointed head, headless and double head of spermatozoon), neck (rupture, separation and enlargement), or tail (mitochondrial swelling, mitochondrial deficit, tailless, double tail, short tail and curled tail); whereas none of the above-mentioned abnormalities was observed in healthy men. Conclusion Sperms of uremic patients had many morphologic and structural abnor- malities in the head, neck and tail. 展开更多
关键词 电子扫描显微镜 形态学 尿毒症 精子细胞
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COEXISTENCE OF OSTEOARTHRITIS AND OSTEOPOROSIS IN FEMORAL HEAD: A SCANNING ELECTRON MICROSCOPIC STUDY
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作者 柴本甫 汤雪明 李慧 《Medical Bulletin of Shanghai Jiaotong University》 CAS 2000年第2期71-76,共6页
Objective To ascertain the coexistence of osteoarthritis and osteoporosis in the femoral head. Methods During total hip replacement for osteoarthritis of hip joint in 12 female patients with an average age of 56 years... Objective To ascertain the coexistence of osteoarthritis and osteoporosis in the femoral head. Methods During total hip replacement for osteoarthritis of hip joint in 12 female patients with an average age of 56 years, the femoral heads were procured. After processing the femoral had, specimens were studied under scanning electron microscope. Results Different degrees of osteoarthritic lesions (characterized by degeneration of articular cartilage and hyperplasia of subchondral bone tissues) could coexust with osteoporotic lesions (characterized by icicle-like trabeculae ) in the femoral had. The hyperplas- tic bone tissues of osteoarthritis lay in the vicinity of icicle-like trabeculae. However, they did not care into contact, nor did they exert influence on each other. Coexistence of these two different lesions covered a brood territory extending from the deep surface of subchondral bone plate to the head-neck junction of femoral head. Conclusion The results suggest that osteoarthritis and osteoporosis do coexist in the femoral head. 展开更多
关键词 osteoarthritis osteoporosis coexistence scanning electron microscope
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基于带电粒子追踪与蒙特卡洛方法的低真空SEM电子探测器仿真分析
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作者 陈禹滔 阴达 +4 位作者 郑传懋 徐龙泉 卢志钢 曹峰 秦熙 《电子显微学报》 CAS CSCD 北大核心 2023年第2期208-215,共8页
低真空扫描电子显微镜对含水、含气以及不导电样品等的表征方面有着重要应用。国仪量子公司团队基于电子轨迹追踪模拟和粒子碰撞蒙特卡洛模拟,对低真空信号探测器的工作过程进行仿真和实测,分析了探测器在不同位置和气压大小对收集效率... 低真空扫描电子显微镜对含水、含气以及不导电样品等的表征方面有着重要应用。国仪量子公司团队基于电子轨迹追踪模拟和粒子碰撞蒙特卡洛模拟,对低真空信号探测器的工作过程进行仿真和实测,分析了探测器在不同位置和气压大小对收集效率的影响。根据模型所预测的探测电流的大致范围同实测探测电流较为一致。同时仿真分析的结果表明,空间中不同区域的放电强度有较大区别,局部区域的雪崩倍增剧烈程度与该区域的电场强度成正相关。这对探测器的形状和位置布局设计具有显著的指导意义。 展开更多
关键词 扫描电子显微镜 低真空探测器 带电粒子追踪 蒙特卡洛模拟
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Scanning Electron Microscopically Study of Sesame Seeds Infected with Macrophomina phaseolina
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作者 D. A. El-Wakil A. M. Mahdy R. Z. El-Menshawy 《Journal of Agricultural Science and Technology(A)》 2011年第1X期96-99,共4页
关键词 扫描电子显微镜 感染 芝麻 种子传播 质量分级 种子产量 商业价值 种子细胞
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基于FIB-SEM和TEM的催化裂化催化剂元素分布研究
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作者 安谧 徐华 +3 位作者 张若霖 张兆前 郑方 王剑 《石油炼制与化工》 CAS CSCD 北大核心 2023年第3期48-53,共6页
为了研究催化裂化(FCC)催化剂的失活机理,利用聚集离子束扫描电镜(FIB-SEM)制作透射电镜样品;采用扫描电镜、透射电镜、X射线荧光光谱、X射线能谱等手段,对FCC催化剂单个颗粒及其FIB切片的元素分布进行表征。结果发现:与新鲜剂相比,催... 为了研究催化裂化(FCC)催化剂的失活机理,利用聚集离子束扫描电镜(FIB-SEM)制作透射电镜样品;采用扫描电镜、透射电镜、X射线荧光光谱、X射线能谱等手段,对FCC催化剂单个颗粒及其FIB切片的元素分布进行表征。结果发现:与新鲜剂相比,催化裂化过程中FCC平衡剂上沉积了Fe,Ni,V,Ca,P等元素;随着杂质元素沉积量的增加,催化剂的骨架密度逐渐增大;随着骨架密度增大,催化剂Fe,Ni,Ca含量提高,而其硅铝比、P含量、比表面积降低;Fe,Ni,P元素主要分布在催化剂颗粒外表面,V元素在催化剂内部和外部分布比较均匀。 展开更多
关键词 催化裂化 催化剂 铁污染 单颗粒 失活 聚集离子束扫描电镜 透射电镜
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硼砂煅制工艺优化及质量评价
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作者 杨辛欣 洪禹昕 +5 位作者 张睿 赵晶丽 刘佳 王楚盈 许天阳 于澎 《中成药》 CAS CSCD 北大核心 2024年第2期404-410,共7页
目的 优化硼砂煅制工艺,并对其进行质量评价。方法 以铺设厚度、煅制温度、煅制时间为影响因素,失水率、蓬松度、粉碎率、四硼酸钠含量为评价指标,星点设计-效应面法优化硼砂煅制工艺。采用扫描电镜(SEM)、热重分析(TG)、拉曼光谱、X射... 目的 优化硼砂煅制工艺,并对其进行质量评价。方法 以铺设厚度、煅制温度、煅制时间为影响因素,失水率、蓬松度、粉碎率、四硼酸钠含量为评价指标,星点设计-效应面法优化硼砂煅制工艺。采用扫描电镜(SEM)、热重分析(TG)、拉曼光谱、X射线衍射(XRD),比较硼砂煅制前后质量差异。结果 最佳条件为铺设厚度2 cm,煅制温度365℃,煅制时间100 min。煅制后,硼砂微观形态、成分组成、晶型结构发生变化,失去全部结晶水而转变为非晶体状态。结论 该方法稳定可行,可用于工业大批量生产煅硼砂。 展开更多
关键词 硼砂 煅制工艺 星点设计-效应面法 扫描电镜(sem) 热重分析(TG) 拉曼光谱 X射线衍射(XRD)
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膨胀土微结构对膨胀行为的影响
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作者 刘正楠 张锐 +2 位作者 唐德力 刘昭京 周豫 《土木与环境工程学报(中英文)》 CSCD 北大核心 2024年第2期60-69,共10页
评估膨胀土的膨胀行为对于膨胀土地区的结构设计十分重要。因降雨入渗,膨胀土在垂直方向和水平方向均产生膨胀变形,当膨胀变形受抑制时将产生膨胀压力,影响其周围结构的稳定性。为揭示膨胀土在增湿膨胀过程中出现各向异性的原因,从微观... 评估膨胀土的膨胀行为对于膨胀土地区的结构设计十分重要。因降雨入渗,膨胀土在垂直方向和水平方向均产生膨胀变形,当膨胀变形受抑制时将产生膨胀压力,影响其周围结构的稳定性。为揭示膨胀土在增湿膨胀过程中出现各向异性的原因,从微观角度出发,通过电镜扫描(SEM)对百色中膨胀土和枝江弱膨胀土的微观结构进行观察,并通过图像处理技术统计分析膨胀土内黏土矿物颗粒的层状排列。通过研发的二维膨胀仪和改进的试件制备方法,从宏观角度测得了侧限条件下的两向膨胀规律。研究结果表明,膨胀土的微观结构呈片状且面-面相叠;当膨胀土处于天然松散状态时,其内部的黏土矿物颗粒随机定向排列且集聚;压实后,因受各向不均等应力作用,黏土矿物颗粒开始趋向于水平层状排列;干密度越大,土样越密实,其水平层状排列越显著。侧限条件下,两向的膨胀规律表现出显著的差异,干密度越大,膨胀性越强,这种差异就越明显。然而,对黏土矿物颗粒来说,其膨胀的方向垂直于其长轴,高度的水平定向是造成膨胀土在宏观上表现出膨胀各向异性的原因,这种两向的膨胀差异受到干密度和膨胀性的影响,难以做出预测,建议在工程实践中实测两向的膨胀规律。 展开更多
关键词 膨胀土 膨胀各向异性 微观结构 电镜扫描 膨胀试验
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原子力显微镜-扫描电子显微镜共定位表征系统的研发与应用
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作者 蔡蕊 万鹏 +2 位作者 徐强 吕天明 孙智广 《分析测试技术与仪器》 CAS 2024年第1期53-57,共5页
微纳加工过程中,常有样品需要进行聚焦离子束(FIB)溅射、切割,扫描电子显微镜(SEM)以及原子力显微镜(AFM)表征,而这三类仪器都需要将样品固定在样品台上才可测试,固定不佳会影响表征结果.但固定好的样品在不同仪器之间转移、拆卸、再固... 微纳加工过程中,常有样品需要进行聚焦离子束(FIB)溅射、切割,扫描电子显微镜(SEM)以及原子力显微镜(AFM)表征,而这三类仪器都需要将样品固定在样品台上才可测试,固定不佳会影响表征结果.但固定好的样品在不同仪器之间转移、拆卸、再固定的过程中极易受到破坏.基于以上问题,设计了AFM-SEM-FIB样品共定位系统,可实现样品在此三种仪器之间的无损转移及共定位,避免珍贵样品破坏及目标丢失,以及解决AFM扫描无法控制方向、迅速调整位点等问题.在微纳表征中有优异的表现,系统已被开发成产品并量产销售. 展开更多
关键词 共定位系统 原子力显微镜 扫描电子显微镜 聚焦离子束 微纳表征
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成型工艺对水泥稳定碎石性能的影响
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作者 郝培文 齐梓超 李天洋 《中国科技论文》 CAS 2024年第4期468-474,共7页
为研究不同成型工艺对水泥稳定碎石宏观性能的影响,基于骨架密实和悬浮密实2种级配,分别采用强制搅拌静压成型、强制搅拌振动压实、振动搅拌静压成型、振动搅拌振动压实4种工艺制备了8种水泥稳定碎石,采用7 d无侧限抗压试验、28 d单轴... 为研究不同成型工艺对水泥稳定碎石宏观性能的影响,基于骨架密实和悬浮密实2种级配,分别采用强制搅拌静压成型、强制搅拌振动压实、振动搅拌静压成型、振动搅拌振动压实4种工艺制备了8种水泥稳定碎石,采用7 d无侧限抗压试验、28 d单轴贯入试验、7 d温缩试验和7 d干缩试验对水泥稳定碎石宏观性能进行了研究,同时结合扫描电子显微镜微观手段,分析了水泥稳定碎石宏观性能变化机理。结果表明:振动搅拌振动压实工艺下骨架密实级配的水泥稳定碎石力学性能最优,其7 d无侧限抗压强度和28 d单轴压缩模量较强制搅拌静压成型分别提升了169.5%、97.2%。采用振动搅拌振动压实工艺可以促使水泥水化产物生成量增多、结构完善,整体均匀性提高,进而改善水泥稳定碎石宏观性能。 展开更多
关键词 振动搅拌 振动压实 宏观性能 扫描电子显微镜 成型工艺
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基于金字塔池化网络的质子交换膜燃料电池气体扩散层组分推理方法
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作者 王虎 尹泽泉 +6 位作者 王雯婕 黄笠舟 方宁宁 隋俊友 张加乐 张锐明 隋邦傑 《重庆大学学报》 CAS CSCD 北大核心 2024年第1期84-92,共9页
针对质子交换膜燃料电池气体扩散层(gas diffusion layer composition,GDL)形貌划分与制备工艺改进问题,提出了一种基于金字塔池化网络(pyramid scene parsing network,PSPNet)与多层感知器(multi-layer perception,MLP)的气体扩散层组... 针对质子交换膜燃料电池气体扩散层(gas diffusion layer composition,GDL)形貌划分与制备工艺改进问题,提出了一种基于金字塔池化网络(pyramid scene parsing network,PSPNet)与多层感知器(multi-layer perception,MLP)的气体扩散层组分识别与比例推理方法:首先将带标签的气体扩散层扫描电镜(scanning electron microscope,SEM)图片输入神经网络,得到特征图;得到的图像特征层进入金字塔池化模块后,获取SEM图像的深层和浅层特征;随后将深层和浅层特征图层融合输入全卷积网络(fully convolutional network,FCN)模块,得到预测图像;最后统计各个组分上的像素点比例,通过MLP完成组分比例推理。结果表明:所提方法组分识别像素准确率达81.24%;在5%偏差范围内,比例推理准确率为88.89%。该方法解决了气体扩散层多组分无法区分、比例无法获知的问题,可有效应用于气体扩散层的质检、数值重构以及制备工艺改进。 展开更多
关键词 质子交换膜燃料电池 气体扩散层制备 扫描电镜 人工智能 金字塔池化网络 多层感知器
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扫描电镜实验课程教学模式探索
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作者 张毅 欧阳静 杨阳 《科教导刊》 2024年第11期122-124,共3页
文章提出了“导学、自学、助学”模式,通过展示高校学科专业背景,建立依托大型精密仪器和科研项目的课程内容遴选机制,充分发挥扫描电镜在本科实验教学中的作用,将理论教学与实践教学融合,拓宽了学生的职业前景并培养其创造性思维和意识... 文章提出了“导学、自学、助学”模式,通过展示高校学科专业背景,建立依托大型精密仪器和科研项目的课程内容遴选机制,充分发挥扫描电镜在本科实验教学中的作用,将理论教学与实践教学融合,拓宽了学生的职业前景并培养其创造性思维和意识,深化了学生对基础知识的理解,培养了学生解决仪器科学与工程技术领域复杂问题的能力,为交叉学科的高质量发展和培养满足国家高新技术需求的拔尖人才奠定了基础。 展开更多
关键词 学生 扫描电镜 实验课程 教学模式
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基于SEM和MIP试验结构性黏土压缩过程中微观孔隙的变化规律 被引量:77
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作者 张先伟 孔令伟 +1 位作者 郭爱国 拓勇飞 《岩石力学与工程学报》 EI CAS CSCD 北大核心 2012年第2期406-412,共7页
为探求土体在变形过程中微结构形态的演化规律,对湛江结构性黏土进行室内压缩试验,通过真空冷冻升华干燥法对天然土和压缩后土制样,进行扫描电子显微镜扫描试验和压汞试验,基于灰度计算土的三维孔隙率,分析压缩过程中微观孔隙的变化规... 为探求土体在变形过程中微结构形态的演化规律,对湛江结构性黏土进行室内压缩试验,通过真空冷冻升华干燥法对天然土和压缩后土制样,进行扫描电子显微镜扫描试验和压汞试验,基于灰度计算土的三维孔隙率,分析压缩过程中微观孔隙的变化规律。结果表明,较二值化处理获得的二维孔隙率,三维孔隙率物理意义明确,求取方法简单,有较高准确性。湛江天然黏土孔径为1.0~0.1μm的小孔隙组占优,其孔隙体积占总孔隙体积的73%。压缩过程中,P>k前,各孔径组分变化甚微。P>k后,随压力的增大,小孔隙含量表现为先增加后降低。各孔隙组对外力的敏感度与孔隙体积含量正相关。由于压汞过程存在"瓶颈"效应,其结果可能会夸大小孔隙的分布密度而低估大孔隙的分布密度。结构性黏土压缩过程中微观结构形态的演化可分为结构微调、结构破损、结构固化3个阶段。该研究有助于深入了解土的变形机制,为结构性土的工程设计提供科学的依据。 展开更多
关键词 土力学 结构性黏土 扫描电子显微镜试验 压汞试验 结构屈服压力 微观孔隙 孔隙率
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