Simultaneous extraction of the coal and gas is an effective method of eliminating coal mine gas disasters while safely exploiting the coal and achieving efficient gas drainage in China, which is widely accepted by the...Simultaneous extraction of the coal and gas is an effective method of eliminating coal mine gas disasters while safely exploiting the coal and achieving efficient gas drainage in China, which is widely accepted by the main coal-producing countries around the world. However, the concrete definition of simultaneous extraction is vague and there is little accurate theoretical support for the simultaneous extraction of coal and gas, which makes it difficult to determine an efficient gas drainage method appropriate to the features of coal seams. Based on theoretical analysis, laboratory tests and field observations, a specific definition of simultaneous extraction of coal and gas is proposed after analyzing the characteristics of coal seam occurrences in China, and we developed the mechanism of mining-enhanced permeability and established the corresponding theoretical model. This comprises a process of fracture network formation, in which the original fractures are opened and new fractures are produced by unloading damage. According to the theoretical model, the engineering approaches and their quantitative parameters of ＇unloading by borehole drilling＇ for single coal seams and ＇unloading by protective seam mining＇ for groups of coal seams are proposed, and the construction principles for coal exploitation and gas-drainage systems for different conditions are given. These methods were applied successfully in the Tunlan Coal Mine in Shanxi Province and the Panyi Coal Mine in Anhui Province and could assure safe and efficient simultaneous extraction of coal and gas in these outburst coal mines.展开更多
Coalbed methane is of great value to extract and utilize in China, but the result of such research is not satisfied yet today.The paper analyzed the storage characteristics of coalbed methane, and then studied the beh...Coalbed methane is of great value to extract and utilize in China, but the result of such research is not satisfied yet today.The paper analyzed the storage characteristics of coalbed methane, and then studied the behavior of coalbed methane using the key stratum theory of strata control.According to the features related to coalbed methane accumulations and delivery, the technique for safely simultaneous extraction of coal and coalbed methane is proposed, and benefit analysis is made too.展开更多
The extraction of nucleic acid is recognized as one of the most essential steps in molecular biology for initiating other downstream applications such as sequencing, amplification, hybridization, and cloning. Many com...The extraction of nucleic acid is recognized as one of the most essential steps in molecular biology for initiating other downstream applications such as sequencing, amplification, hybridization, and cloning. Many commercial kits and methods are currently available that allow the extraction of only one type of nucleic acids-DNA or RNA. However, in parallel clinical detection of several diseases, a method for simultaneous extraction of both DNA and RNA from the same source is needed in such cases. In this study, a method for simultaneous extraction of DNA and RNA from bacteria based on magnetic nanoparticles(MNPs) was described. Lysis buffers were prepared to help the nucleic acid released and adsorbed to MNPs. Then, two washing buffers were used to remove the contamination of proteins and carbohydrates. The nucleic acids were finally eluted by Deoxyribonuclease(DNase) and Ribonucleases(RNase) free water. Different factors which might affect the purification of the nucleic acid were investigated, and the quantity and quality parameters of the nucleic acid were also recorded. The DNA and RNA extracted from bacteria were then respectively subjected to polymerase chain reaction(PCR) and reverse transcription PCR(RT-PCR) to further confirm its quality. The results indicated that our method can be successfully used to simultaneously extract DNA and RNA from bacteria.展开更多
The volatile and semi-volatile components in tobacco flavor additives were extracted by both simultaneous distillation extraction and solid-phase micro-extraction. Extraction conditions for solid-phase micro-extractio...The volatile and semi-volatile components in tobacco flavor additives were extracted by both simultaneous distillation extraction and solid-phase micro-extraction. Extraction conditions for solid-phase micro-extraction were optimized with information theory. Then, detection were accomplished by gas chromatography-mass spectrometry. Characteristic of each method was compared. Qualitative analysis and quantitative analysis of 6# tobacco flavor sample were accomplished through both simultaneous distillation extraction and solid-phase micro-extraction. The experimental results show that solid-phase micro-extraction method is the first choice for qualitative analysis and simultaneous distillation extraction is another good selection for quantitative analysis. By means of simultaneous distillation extraction, 20 components are identified, accounting for 92.77% of the total peak areas. Through solid-phase micro-extraction, there are 17 components identified accounting for 91.49% of the total peak areas. The main aromatic components in 6# tobacco flavor sample are propanoic acid, 2-hydroxy-, ethyl ester, menthol and menthyl acetate. The presented method has been successfully used for quality control of tobacco flavor.展开更多
Supercritical carbon dioxide fluid extraction (SFE) was studied as a rapid method for extraction of volatile and semivolatile compounds of Chinese commercial cigarettes. The method was compared with simultaneous disti...Supercritical carbon dioxide fluid extraction (SFE) was studied as a rapid method for extraction of volatile and semivolatile compounds of Chinese commercial cigarettes. The method was compared with simultaneous distillation and extraction (SDE). Temperature and pressure for the SFE were optimized. The extracts obtained by the two methods showed different characters in composition and represented differently the flavor characteristics of tobacco; compared to SDE, SFE can extract compounds within a shorter time and avoid the thermal degradation and solvent contamination of samples. The extracts by the two extraction methods are complementary for investigating the flavor characteristic of tobacco products.展开更多
To establish an analytical method for determination of four bisphenols （BPA, BPB, BPF, and BPS） and two alkylphenols （4-n-OP, 4-n-NP） in water by ultra performance liquid chromatography- tandem mass spectrometry ...To establish an analytical method for determination of four bisphenols （BPA, BPB, BPF, and BPS） and two alkylphenols （4-n-OP, 4-n-NP） in water by ultra performance liquid chromatography- tandem mass spectrometry （UPLC/MS/MS）. The water samples were extracted and condensed with solid-phase extraction （SPE） using C18 cartridges and eluted by acetonitrile. Separation was carried out with Acquity BEH C8 column and detection were performed by UPLC/MS/MS. Quantification was calculated by using the internal standard BPA-d16 and 4-n-NP-d8. The linear correlation coefficients of these compounds in the range of 1.0-100.0μg/L were all over 0.999. The minimum detectable concentrations were 0.75-1.0 ng/L, and the recoveries ranged from 87.0% to 106.9%.展开更多
The importance of simultaneous coal and methane extraction and its significance on green exploitation is stated, and current research situation of simultaneous coal and methane and faced new problems are introduced. T...The importance of simultaneous coal and methane extraction and its significance on green exploitation is stated, and current research situation of simultaneous coal and methane and faced new problems are introduced. The research progress on movement of overlying strata and stresses change in them, cracks development during mining in overlying strata and meth- ane emission under disturbance of mining as well as the changing rules of permeability and methane flow under the disturbance of mining is analyzed. The progress on practice of simultaneous coal and methane extraction is analyzed. The deficiencies of current research and further researching fields on simultaneous coal and methane extraction are pointed out.展开更多
The bioavailability of five divalent cationic heavy metals （Pb, Cd, Cu, Zn and Ni） in 10 superficial sediment samples from Baihua Lake was assessed based on the molar ratio of simultaneously extracted metals （SEMs...The bioavailability of five divalent cationic heavy metals （Pb, Cd, Cu, Zn and Ni） in 10 superficial sediment samples from Baihua Lake was assessed based on the molar ratio of simultaneously extracted metals （SEMs） to acid volatile sulfide （AVS）. Atomic absorption spectrometry （AAS） and X-ray powder diffraction （XRD） were used to determine the heavy metal concentrations and examine the mineralogy of the crystalline phases, respectively. The AVS loadings in sediments from Baihua Lake ranged from 64.30 to 350.08 ~rnol/g （dry weight）. The corresponding SEM levels for the sampling sites varied from 1.770 to 14.660 vrnol/g. The molar ratio of SEMs to AVS ranged from 0.014 to 0.084 with a mean value of 0.034. The XRD analysis also confirmed the presence of some metal sulfides in sediments from Baihua Lake. The SEMs/AVS ratios for all sampling sites were significantly lower than 1.0, indicating that AVS in the sediments was sufficient to bind the five heavy metals; thus, these heavy metals are currently not significantly bioavailable to benthic organisms. Comparing the SEMs results to published guideline values for metal toxicity to benthic organisms in sediments, however, suggests that Zn and Ni pose a risk at some sampling locations in Baihua Lake.展开更多
To analyze the chemical constituents of volatile oils from the fruit of Periploca forrestii Schltr.which were collected in Guizhou province.This volatile oils were extracted by simultaneous distillation extraction (SD...To analyze the chemical constituents of volatile oils from the fruit of Periploca forrestii Schltr.which were collected in Guizhou province.This volatile oils were extracted by simultaneous distillation extraction (SDE)and microwave assistant extraction(MAE) method,and ananlyzed by gas chromatography-mass spectrometry(GC-MS)method.The main chemical compounds were methyl salicylate,β-amyrin and β-amyrin acetate etc.The compounds from the volatile oils extracted with SDE and MAE are quite different.The results provide scientific proof for the further development and utilization of Periploca forrestii Schltr.展开更多
According to the deficiency of experiment system for gas adsorption and desorption in coal mass, a large scale experiment system is developed independently by researchers. This experiment system is composed of primary...According to the deficiency of experiment system for gas adsorption and desorption in coal mass, a large scale experiment system is developed independently by researchers. This experiment system is composed of primary and auxiliary boxes, power transmission system, mining system, loading system, gas charging system, data monitoring and intelligent acquisition system. The maximum experiment coal consumption is 1200 kg, the mining system is developed to conduct experiment for gas desorption under excavating disturbance, and the plane-charging cribriform ventilation device is developed to realize uniform ventilation for experiment coal sample, which is accord with the actual gas source situation of coal bed. The desorption characteristics of gas in coal are experimentally studied under the conditions of nature and mining using the experiment system. The results show that, compare with nature condition, the permeability of coal and the velocity of gas desorption could significantly increase under the influence of coal pressure relief and destruction caused by mining, and the degree of gas desorption could somewhat increase too. Finally, pressure relief gas extraction of current seam and adjacent seams after mining in a certain coal mine of Yangquan mining area are introduced, and the gas desorption experiment results is verified by analyzing the effect of gas extraction.展开更多
To achieve safe and highly efficient mining in the gassy, deep mines of the Huainan collieries simultaneous coal and gas extraction, and the corresponding ventilation methods were developed. This includes a set of min...To achieve safe and highly efficient mining in the gassy, deep mines of the Huainan collieries simultaneous coal and gas extraction, and the corresponding ventilation methods were developed. This includes a set of mining procedures and principles which help insure safe and efficient production. Furthermore, green mining, meaning the comprehensive use of emitted gas, proper treatment of the environment and appropriate mine temperature control, is now standard. The concepts of modem mining and the principles of pressure relief are described. Coal-gas simultaneous ex- traction and multi-pressure relief techniques were developed which require a combination of surface and underground gas extraction. The application of Y-ventilation systems, of roadways retained along goafs, of stress control techniques for highly fragile mine roofs and of powerful, automatic and reliable mining equipment contributes to safe operation of modem deep mines. Operating parameters for these techniques are described and the results of their use discussed.展开更多
Aiming to effectively solve the problem of deep mining with safety and high efficiency, according to geological conditions, production and stress analysis in roadway surrounding rock, experimental studies on roadway s...Aiming to effectively solve the problem of deep mining with safety and high efficiency, according to geological conditions, production and stress analysis in roadway surrounding rock, experimental studies on roadway supporting of workface 103 under three types of roof conditions with different supporting technologies and parameters were carried out based on the theory of supporting technology of gob-side entry. The results show the supporting of gob-side entry retaining is successful, and the deep surrounding rock is effectively controlled by field monitoring and drilling-hole photos. After stress in surrounding rock of roadways restores stable, the final roadway deformation of surrounding rock of haulage roadway and air-roadway are both about 300 mm; width of gob-side entry is 3.8-4.0 m and average height is 2.0-2.2 m; roadway section is above 8.0 m^2, which solves the problems of gob-side entry retaining support strength and safe mining; necessary conditions of mining safety in workface 103 are met.展开更多
The origins and main control methods of gas in coal seams were introduced cursorily, and the processes that need to be done in controlling gas, which includes prediction of gas emissions, drainage systems, the means o...The origins and main control methods of gas in coal seams were introduced cursorily, and the processes that need to be done in controlling gas, which includes prediction of gas emissions, drainage systems, the means of prevention of gas outbursts, and some suggestions were put forward. The characteristic of different gas emissions and the corresponding counter measures were presented, and ＆ case study of simultaneous extraction of coal and gas in Xieyi Coal Mine was carried out by coal mining and gas extraction without coal-pillar. The field application shows that gas drainage ratio in panel 5121（0） averages about 90% and reaches as high as 95~/0, which will give beneficial references to gas control in coal mines.展开更多
Nine elements （As, Cd, Cr, Cu, Fe, Mn, Ni, Pb, Zn） in sediment samples at 7 sites （Site 1-7） from Suzhou Creek in Shanghai were analyzed with the Community Bareau of Reference （BCR） （sequential extraction （SE...Nine elements （As, Cd, Cr, Cu, Fe, Mn, Ni, Pb, Zn） in sediment samples at 7 sites （Site 1-7） from Suzhou Creek in Shanghai were analyzed with the Community Bareau of Reference （BCR） （sequential extraction （SE）） protocol and simultaneously extracted metals （SEM）/acid volatile sulfide （AVS） procedure to assess the metal bioavailability and toxicology in this area. The results showed that the BCR extraction can be utilized as an additional tool with the AVS method for assessing the potential bioavailability and toxicity of metals in sediments. Pollution from S5 （Site 5） was more severe than from other sites, especially Pb, Cu and Zn. Among all the sites, more than 80% of the total concentration of Fe existed in the residual fraction, As, Cr, Mn also dominated in the residual fraction （more than 50%）. While Cd, Ni and Zn （more than 35%） were mainly in the non-stable phase. Cu had a strong affinity with oxidizable phase and Pb varied from site to site. The SEM/AVS ratio was less than one in these sediments and results implied that the majority of Zn and Ni （〉 40%） were bound to AVS. In contrast, Pb, Cu and Cd were little bound to AVS due to their low ration of SEM-Pb, Cu, Cd to corresponding total concentration and relatively high Dorewater concentration.展开更多
Aroma of Chinese steamed bread（CSB） is one of the important parameters that determines the overall quality attributes and consumer acceptance. However, the aroma profile of CSB still remains poorly understood, mainl...Aroma of Chinese steamed bread（CSB） is one of the important parameters that determines the overall quality attributes and consumer acceptance. However, the aroma profile of CSB still remains poorly understood, mainly because of relying on only a single method for aroma extraction in previous studies. Therefore, the objective of this study was to determine the volatile aroma compounds of five different samples of CSB using three different aroma extraction methods, namely solid-phase microextraction（SPME）, simultaneous distillation–extraction（SDE）, and purge and trap（PT）. All samples showed a unique aroma profile, which could be attributed to their unique microbial consortia.（E）-2-Nonenal and（E,E）-2,4-decadienal were the most prevalent aromatic compounds revealed by SDE, which have not been reported previously, while ethanol and acetic acid proved to be the most dominant compounds by both SPME and PT. Our approach of combining three different aroma extraction methods provided better insights into the aroma profile of CSB, which had remained largely unknown in previous studies.展开更多
基金Acknowledgments This research was supported by the National Program on Key Basic Research Project of China （973 Program） （2011CB201204）, the Visitor Foundation of the State Key Laboratory of Coal Mine Disaster Dynamics and Control （Chongqing University） （2011DA105287-FW201405）, the National Natural Science Foundation of China （51374204 and 51304204）, and a project funded by the Priority Academic Program Development of Jiangsu Higher Education Institutions.
文摘Simultaneous extraction of the coal and gas is an effective method of eliminating coal mine gas disasters while safely exploiting the coal and achieving efficient gas drainage in China, which is widely accepted by the main coal-producing countries around the world. However, the concrete definition of simultaneous extraction is vague and there is little accurate theoretical support for the simultaneous extraction of coal and gas, which makes it difficult to determine an efficient gas drainage method appropriate to the features of coal seams. Based on theoretical analysis, laboratory tests and field observations, a specific definition of simultaneous extraction of coal and gas is proposed after analyzing the characteristics of coal seam occurrences in China, and we developed the mechanism of mining-enhanced permeability and established the corresponding theoretical model. This comprises a process of fracture network formation, in which the original fractures are opened and new fractures are produced by unloading damage. According to the theoretical model, the engineering approaches and their quantitative parameters of ＇unloading by borehole drilling＇ for single coal seams and ＇unloading by protective seam mining＇ for groups of coal seams are proposed, and the construction principles for coal exploitation and gas-drainage systems for different conditions are given. These methods were applied successfully in the Tunlan Coal Mine in Shanxi Province and the Panyi Coal Mine in Anhui Province and could assure safe and efficient simultaneous extraction of coal and gas in these outburst coal mines.
文摘Coalbed methane is of great value to extract and utilize in China, but the result of such research is not satisfied yet today.The paper analyzed the storage characteristics of coalbed methane, and then studied the behavior of coalbed methane using the key stratum theory of strata control.According to the features related to coalbed methane accumulations and delivery, the technique for safely simultaneous extraction of coal and coalbed methane is proposed, and benefit analysis is made too.
基金supported by the National Basic Research Program of China(2014CB744501)the National High Technology Research and Development Program of China(2012AA022703)+8 种基金the National Key Special Science Program(2013ZX10004103-002)the National Natural Science Foundation of China(61201033,21205013,61271056,61527806)Projects of Development of Science and Medical Technology(201208038)Projects of Health Ministry of Nanjing(ZKX12038)the Clinical Science and Technology Special Projects in Jiangsu Province(BL2012067,BL2014094)the Talents Planning of Six Summit Fields of Jiangsu Province(2013-WSN-056)China Postdoctoral Science Foundation Funded Project(2014M551491,2015T80487)Jiangsu Planned Projects for Postdoctoral Research Funds(1302007A)the Economical Forest Cultivation and Utilization of 2011 Collaborative Innovation Center in Hunan Province
文摘The extraction of nucleic acid is recognized as one of the most essential steps in molecular biology for initiating other downstream applications such as sequencing, amplification, hybridization, and cloning. Many commercial kits and methods are currently available that allow the extraction of only one type of nucleic acids-DNA or RNA. However, in parallel clinical detection of several diseases, a method for simultaneous extraction of both DNA and RNA from the same source is needed in such cases. In this study, a method for simultaneous extraction of DNA and RNA from bacteria based on magnetic nanoparticles(MNPs) was described. Lysis buffers were prepared to help the nucleic acid released and adsorbed to MNPs. Then, two washing buffers were used to remove the contamination of proteins and carbohydrates. The nucleic acids were finally eluted by Deoxyribonuclease(DNase) and Ribonucleases(RNase) free water. Different factors which might affect the purification of the nucleic acid were investigated, and the quantity and quality parameters of the nucleic acid were also recorded. The DNA and RNA extracted from bacteria were then respectively subjected to polymerase chain reaction(PCR) and reverse transcription PCR(RT-PCR) to further confirm its quality. The results indicated that our method can be successfully used to simultaneously extract DNA and RNA from bacteria.
文摘The volatile and semi-volatile components in tobacco flavor additives were extracted by both simultaneous distillation extraction and solid-phase micro-extraction. Extraction conditions for solid-phase micro-extraction were optimized with information theory. Then, detection were accomplished by gas chromatography-mass spectrometry. Characteristic of each method was compared. Qualitative analysis and quantitative analysis of 6# tobacco flavor sample were accomplished through both simultaneous distillation extraction and solid-phase micro-extraction. The experimental results show that solid-phase micro-extraction method is the first choice for qualitative analysis and simultaneous distillation extraction is another good selection for quantitative analysis. By means of simultaneous distillation extraction, 20 components are identified, accounting for 92.77% of the total peak areas. Through solid-phase micro-extraction, there are 17 components identified accounting for 91.49% of the total peak areas. The main aromatic components in 6# tobacco flavor sample are propanoic acid, 2-hydroxy-, ethyl ester, menthol and menthyl acetate. The presented method has been successfully used for quality control of tobacco flavor.
文摘Supercritical carbon dioxide fluid extraction (SFE) was studied as a rapid method for extraction of volatile and semivolatile compounds of Chinese commercial cigarettes. The method was compared with simultaneous distillation and extraction (SDE). Temperature and pressure for the SFE were optimized. The extracts obtained by the two methods showed different characters in composition and represented differently the flavor characteristics of tobacco; compared to SDE, SFE can extract compounds within a shorter time and avoid the thermal degradation and solvent contamination of samples. The extracts by the two extraction methods are complementary for investigating the flavor characteristic of tobacco products.
基金supported by the Preventive medicine and public health research project of Anhui,China(No.2011Y0103)the Natural Science Foundation of Anhui,China(No.11040606M216)
文摘To establish an analytical method for determination of four bisphenols （BPA, BPB, BPF, and BPS） and two alkylphenols （4-n-OP, 4-n-NP） in water by ultra performance liquid chromatography- tandem mass spectrometry （UPLC/MS/MS）. The water samples were extracted and condensed with solid-phase extraction （SPE） using C18 cartridges and eluted by acetonitrile. Separation was carried out with Acquity BEH C8 column and detection were performed by UPLC/MS/MS. Quantification was calculated by using the internal standard BPA-d16 and 4-n-NP-d8. The linear correlation coefficients of these compounds in the range of 1.0-100.0μg/L were all over 0.999. The minimum detectable concentrations were 0.75-1.0 ng/L, and the recoveries ranged from 87.0% to 106.9%.
基金Supported by the National Science Foundation of China （51304006） the Key Project of Anhui Provincial Department of Education （KJ2011A075） the Youth Backbone Training Funds of Anhui University of Science ＆Technology （20120012）
文摘The importance of simultaneous coal and methane extraction and its significance on green exploitation is stated, and current research situation of simultaneous coal and methane and faced new problems are introduced. The research progress on movement of overlying strata and stresses change in them, cracks development during mining in overlying strata and meth- ane emission under disturbance of mining as well as the changing rules of permeability and methane flow under the disturbance of mining is analyzed. The progress on practice of simultaneous coal and methane extraction is analyzed. The deficiencies of current research and further researching fields on simultaneous coal and methane extraction are pointed out.
基金Supported by the National Natural Science Foundation of China(No.20967003)the Project of the Government of Guiyang City(No.[2010]5-2)
文摘The bioavailability of five divalent cationic heavy metals （Pb, Cd, Cu, Zn and Ni） in 10 superficial sediment samples from Baihua Lake was assessed based on the molar ratio of simultaneously extracted metals （SEMs） to acid volatile sulfide （AVS）. Atomic absorption spectrometry （AAS） and X-ray powder diffraction （XRD） were used to determine the heavy metal concentrations and examine the mineralogy of the crystalline phases, respectively. The AVS loadings in sediments from Baihua Lake ranged from 64.30 to 350.08 ~rnol/g （dry weight）. The corresponding SEM levels for the sampling sites varied from 1.770 to 14.660 vrnol/g. The molar ratio of SEMs to AVS ranged from 0.014 to 0.084 with a mean value of 0.034. The XRD analysis also confirmed the presence of some metal sulfides in sediments from Baihua Lake. The SEMs/AVS ratios for all sampling sites were significantly lower than 1.0, indicating that AVS in the sediments was sufficient to bind the five heavy metals; thus, these heavy metals are currently not significantly bioavailable to benthic organisms. Comparing the SEMs results to published guideline values for metal toxicity to benthic organisms in sediments, however, suggests that Zn and Ni pose a risk at some sampling locations in Baihua Lake.
文摘To analyze the chemical constituents of volatile oils from the fruit of Periploca forrestii Schltr.which were collected in Guizhou province.This volatile oils were extracted by simultaneous distillation extraction (SDE)and microwave assistant extraction(MAE) method,and ananlyzed by gas chromatography-mass spectrometry(GC-MS)method.The main chemical compounds were methyl salicylate,β-amyrin and β-amyrin acetate etc.The compounds from the volatile oils extracted with SDE and MAE are quite different.The results provide scientific proof for the further development and utilization of Periploca forrestii Schltr.
基金Acknowledgments This work is supported by the National Key Basic Research Program of China （2013CB227903） and the National Natural Science Foundation of China （U1361209）.
文摘According to the deficiency of experiment system for gas adsorption and desorption in coal mass, a large scale experiment system is developed independently by researchers. This experiment system is composed of primary and auxiliary boxes, power transmission system, mining system, loading system, gas charging system, data monitoring and intelligent acquisition system. The maximum experiment coal consumption is 1200 kg, the mining system is developed to conduct experiment for gas desorption under excavating disturbance, and the plane-charging cribriform ventilation device is developed to realize uniform ventilation for experiment coal sample, which is accord with the actual gas source situation of coal bed. The desorption characteristics of gas in coal are experimentally studied under the conditions of nature and mining using the experiment system. The results show that, compare with nature condition, the permeability of coal and the velocity of gas desorption could significantly increase under the influence of coal pressure relief and destruction caused by mining, and the degree of gas desorption could somewhat increase too. Finally, pressure relief gas extraction of current seam and adjacent seams after mining in a certain coal mine of Yangquan mining area are introduced, and the gas desorption experiment results is verified by analyzing the effect of gas extraction.
基金Projects 2001BA803B04 and 2004BA803B01 supported by the National Key Projects for Tackling Scientific and Technological Problems during the 10thFive-Year Plan
文摘To achieve safe and highly efficient mining in the gassy, deep mines of the Huainan collieries simultaneous coal and gas extraction, and the corresponding ventilation methods were developed. This includes a set of mining procedures and principles which help insure safe and efficient production. Furthermore, green mining, meaning the comprehensive use of emitted gas, proper treatment of the environment and appropriate mine temperature control, is now standard. The concepts of modem mining and the principles of pressure relief are described. Coal-gas simultaneous ex- traction and multi-pressure relief techniques were developed which require a combination of surface and underground gas extraction. The application of Y-ventilation systems, of roadways retained along goafs, of stress control techniques for highly fragile mine roofs and of powerful, automatic and reliable mining equipment contributes to safe operation of modem deep mines. Operating parameters for these techniques are described and the results of their use discussed.
文摘Aiming to effectively solve the problem of deep mining with safety and high efficiency, according to geological conditions, production and stress analysis in roadway surrounding rock, experimental studies on roadway supporting of workface 103 under three types of roof conditions with different supporting technologies and parameters were carried out based on the theory of supporting technology of gob-side entry. The results show the supporting of gob-side entry retaining is successful, and the deep surrounding rock is effectively controlled by field monitoring and drilling-hole photos. After stress in surrounding rock of roadways restores stable, the final roadway deformation of surrounding rock of haulage roadway and air-roadway are both about 300 mm; width of gob-side entry is 3.8-4.0 m and average height is 2.0-2.2 m; roadway section is above 8.0 m^2, which solves the problems of gob-side entry retaining support strength and safe mining; necessary conditions of mining safety in workface 103 are met.
文摘The origins and main control methods of gas in coal seams were introduced cursorily, and the processes that need to be done in controlling gas, which includes prediction of gas emissions, drainage systems, the means of prevention of gas outbursts, and some suggestions were put forward. The characteristic of different gas emissions and the corresponding counter measures were presented, and ＆ case study of simultaneous extraction of coal and gas in Xieyi Coal Mine was carried out by coal mining and gas extraction without coal-pillar. The field application shows that gas drainage ratio in panel 5121（0） averages about 90% and reaches as high as 95~/0, which will give beneficial references to gas control in coal mines.
基金supported by the Science Foundation of Shanghai Municipal Commission of Science and Technology （Grant No.04DZ12030-3）, the National High-Technology Research and Development Program of China （Grant No.2005AA60101005）, and the Shanghai Leading Academic Discipline PProject （Grant No.T0105）Project （Grant No.T0105）.
文摘Nine elements （As, Cd, Cr, Cu, Fe, Mn, Ni, Pb, Zn） in sediment samples at 7 sites （Site 1-7） from Suzhou Creek in Shanghai were analyzed with the Community Bareau of Reference （BCR） （sequential extraction （SE）） protocol and simultaneously extracted metals （SEM）/acid volatile sulfide （AVS） procedure to assess the metal bioavailability and toxicology in this area. The results showed that the BCR extraction can be utilized as an additional tool with the AVS method for assessing the potential bioavailability and toxicity of metals in sediments. Pollution from S5 （Site 5） was more severe than from other sites, especially Pb, Cu and Zn. Among all the sites, more than 80% of the total concentration of Fe existed in the residual fraction, As, Cr, Mn also dominated in the residual fraction （more than 50%）. While Cd, Ni and Zn （more than 35%） were mainly in the non-stable phase. Cu had a strong affinity with oxidizable phase and Pb varied from site to site. The SEM/AVS ratio was less than one in these sediments and results implied that the majority of Zn and Ni （〉 40%） were bound to AVS. In contrast, Pb, Cu and Cd were little bound to AVS due to their low ration of SEM-Pb, Cu, Cd to corresponding total concentration and relatively high Dorewater concentration.
基金supported by the National Natural Science Foundation of China(No.31371826)the China Postdoctoral Science Foundation(No.2016M592002)
文摘Aroma of Chinese steamed bread（CSB） is one of the important parameters that determines the overall quality attributes and consumer acceptance. However, the aroma profile of CSB still remains poorly understood, mainly because of relying on only a single method for aroma extraction in previous studies. Therefore, the objective of this study was to determine the volatile aroma compounds of five different samples of CSB using three different aroma extraction methods, namely solid-phase microextraction（SPME）, simultaneous distillation–extraction（SDE）, and purge and trap（PT）. All samples showed a unique aroma profile, which could be attributed to their unique microbial consortia.（E）-2-Nonenal and（E,E）-2,4-decadienal were the most prevalent aromatic compounds revealed by SDE, which have not been reported previously, while ethanol and acetic acid proved to be the most dominant compounds by both SPME and PT. Our approach of combining three different aroma extraction methods provided better insights into the aroma profile of CSB, which had remained largely unknown in previous studies.
