Field evidence indicates that proppant distribution and threshold pressure gradient have great impacts on well productivity.Aiming at the development of unconventional oil reservoirs in Triassic Chang-7 Unit,Ordos Bas...Field evidence indicates that proppant distribution and threshold pressure gradient have great impacts on well productivity.Aiming at the development of unconventional oil reservoirs in Triassic Chang-7 Unit,Ordos Basin of China,we presented an integrated workflow to investigate how(1)proppant placement in induced fracture and(2)non-linear flow in reservoir matrix would affect well productivity and fluid flow in the reservoir.Compared with our research before(Yue et al.,2020),here we extended this study into the development of multi-stage fractured horizontal wells(MFHWs)with large-scale complicated fracture geometry.The integrated workflow is based on the finite element method and consists of simulation models for proppant-laden fluid flow,fracture flow,and non-linear seepage flow,respectively.Simulation results indicate that the distribution of proppant inside the induced cracks significantly affects the productivity of the MFHW.When we assign an idealized proppant distribution instead of the real distribution,there will be an overestimation of 44.98%in daily oil rate and 30.63%in cumulative oil production after continuous development of 1000 days.Besides,threshold pressure gradient(TPG)also significantly affects the well performance in tight oil reservoirs.If we simply apply linear Darcy’s law to the reservoir matrix,the overall cumulative oil production can be overrated by 77%after 1000 days of development.In general,this research provides new insights into the development of tight oil reservoirs with TPG and meanwhile reveals the significance of proppant distribution and non-linear fluid flow in the production scenario design.展开更多
Slickwater fracturing fluids have gained widespread application in the development of tight oil reservoirs. After the fracturing process, the active components present in slickwater can directly induce spontaneous imb...Slickwater fracturing fluids have gained widespread application in the development of tight oil reservoirs. After the fracturing process, the active components present in slickwater can directly induce spontaneous imbibition within the reservoir. Several variables influence the eventual recovery rate within this procedure, including slickwater composition, formation temperature, degree of reservoir fracture development, and the reservoir characteristics. Nonetheless, the underlying mechanisms governing these influences remain relatively understudied. In this investigation, using the Chang-7 block of the Changqing Oilfield as the study site, we employ EM-30 slickwater fracturing fluid to explore the effects of the drag-reducing agent concentration, imbibition temperature, core permeability, and core fracture development on spontaneous imbibition. An elevated drag-reducing agent concentration is observed to diminish the degree of medium and small pore utilization. Furthermore, higher temperatures and an augmented permeability enhance the fluid flow properties, thereby contributing to an increased utilization rate across all pore sizes. Reduced fracture development results in a lower fluid utilization across diverse pore types. This study deepens our understanding of the pivotal factors affecting spontaneous imbibition in tight reservoirs following fracturing. The findings act as theoretical, technical, and scientific foundations for optimizing fracturing strategies in tight oil reservoir transformations.展开更多
The Daqing exploration area in the northern Songliao Basin has great potential for unconventional oil and gas resources,among which the total resources of tight oil alone exceed 109 t and is regarded as an important r...The Daqing exploration area in the northern Songliao Basin has great potential for unconventional oil and gas resources,among which the total resources of tight oil alone exceed 109 t and is regarded as an important resource base of Daqing oilfield.After years of exploration in the Qijia area,Songliao Basin,NE China,tight oil has been found in the Upper Cretaceous Qingshankou Formation.To work out tight oil’s geological characteristics,taking tight oil in Gaotaizi oil layers of the Upper Cretaceous Qingshankou Formation in northern Songliao Basin as an example,this paper systematically analyzed the geological characteristics of unconventional tight oil in Gao3 and Gao4 layers of the Qijia area,based on the data of the geological survey,well drilling journey,well logging,and test.It is that three sets of hydrocarbon source rocks(K2qn1,K2qn2+3,and K2n1)develop in the examined area,and exhibit excellent type I and II kerogens,high organic matter abundance,and moderate maturity.The reservoir is generally composed of thin-bedded mudstone,siltstone,and sandstone,and presents poor porosity(average 8.5 vol.%)and air permeability(average 4 mD).The main reservoir space primarily includes intergranular pores,secondary soluble pores,and intergranular soluble pores.Three types of orifice throats were identified,namely fine throat,extra-fine throat,and micro-fine throat.The siltstone is generally oil-bearing,the reservoirs with slime and calcium become worse oil-bearing,and the mudstone has no obvious oil-bearing characteristics.The brittleness indices of the sandstone in the tight oil reservoir range from 40%to 60%,and those of the mudstone range from 40%to 45%,indicating a better brittleness of the tight oil reservoir.Based on the study of typical core hole data,this paper gives a comprehensive evaluation of the properties of the tight oil and establishes a tight oil single well composite bar chart as well as the initial evaluation system with the core of properties in the tight oil reservoir.This study has theoretical guiding significance and practical application value for tight oil exploration and evaluation in the Qijia area.展开更多
Based on the typical dissection of various onshore tight oil fields in China,the tight oil migration and accumulation mechanism and enrichment-controlling factors in continental lake basins are analyzed through nuclea...Based on the typical dissection of various onshore tight oil fields in China,the tight oil migration and accumulation mechanism and enrichment-controlling factors in continental lake basins are analyzed through nuclear magnetic resonance(NMR)displacement physical simulation and Lattice Boltzmann numerical simulation by using the samples of source rock,reservoir rock and crude oil.In continental lake basins,the dynamic forces driving hydrocarbon generation and expulsion of high-quality source rocks are the foundational power that determines the charging efficiency and accumulation effect of tight oil,the oil migration resistance is a key element that influences the charging efficiency and accumulation effect of tight oil,and the coupling of charging force with pore-throat resistance in tight reservoir controls the tight oil accumulation and sweet spot enrichment.The degree of tight oil enrichment in continental lake basins is controlled by four factors:source rock,reservoir pore-throat size,anisotropy of reservoir structure,and fractures.The high-quality source rocks control the near-source distribution of tight oil,reservoir physical properties and pore-throat size are positively correlated with the degree of tight oil enrichment,the anisotropy of reservoir structure reveals that the parallel migration rate is the highest,and intralayer fractures can improve the migration and accumulation efficiency and the oil saturation.展开更多
The traditional multi-process to enhance tight oil recovery based on fracturing and huff-n-puff has obvious deficiencies,such as low recovery efficiency,rapid production decline,high cost,and complexity,etc.Therefore,...The traditional multi-process to enhance tight oil recovery based on fracturing and huff-n-puff has obvious deficiencies,such as low recovery efficiency,rapid production decline,high cost,and complexity,etc.Therefore,a new technology,the so-called fracturing-oil expulsion integration,which does not need flowback after fracturing while making full use of the fracturing energy and gel breaking fluids,are needed to enable efficient exploitation of tight oil.A novel triple-responsive smart fluid based on“pseudo-Gemini”zwitterionic viscoelastic surfactant(VES)consisting of N-erucylamidopropyl-N,N-dimethyl-3-ammonio-2-hydroxy-1-propane-sulfonate(EHSB),N,N,N′,N′-tetramethyl-1,3-propanediamine(TMEDA)and sodium p-toluenesulfonate(NaPts),is developed.Then,the rheology of smart fluid is systematically studied at varying conditions(CO_(2),temperature and pressure).Moreover,the mechanism of triple-response is discussed in detail.Finally,a series of fracturing and spontaneous imbibition performances are systematically investigated.The smart fluid shows excellent CO_(2)-,thermal-,and pressure-triple responsive behavior.It can meet the technical requirement of tight oil fracturing construction at 140°C in the presence of 3.5 MPa CO_(2).The gel breaking fluid shows excellent spontaneous imbibition oil expulsion(∼40%),salt resistance(1.2×104 mg/L Na+),temperature resistance(140°C)and aging stability(30 days).展开更多
Countercurrent imbibition is an important mechanism for tight oil recovery,that is,water imbibes spontaneously from the fracture into the porous matrix while oil flows reversely into the fracture.Its significance over...Countercurrent imbibition is an important mechanism for tight oil recovery,that is,water imbibes spontaneously from the fracture into the porous matrix while oil flows reversely into the fracture.Its significance over cocurrent imbibition and forced imbibition is highlighted when permeability reduces.We used the computed tomography(CT)scanning to measure the one-dimensional evolution of water saturation profile and countercurrent imbibition distance(CID)at different fluid pressures,initial water saturations,and permeability.Surprisingly,experiments show that CID evolution for tight reservoir cores dramatically deviates from the classical diffusive rule(i.e.,evolutes proportional to square root of time,t^(0.5)).At early stage,CID extends faster than t^(0.5)(super-diffusive);while at late stage,CID extends much slower than t^(0.5)(sub-diffusive).After tens of hours,the CID change becomes too slow to be practically efficient for tight oil recovery.This research demonstrates that this deviation from classic theory is a result of(1)a much longer characteristic capillary length than effective invasion depth,which eliminates full development of a classical displacement front;and(2)non-zero flow at low water saturation,which was always neglected for conventional reservoir and is amplified in sub-mili-Darcy rocks.To well depict the details of the imbibition front in this situation,we introduce non-zero wetting phase fluidity at low saturation into classical countercurrent imbibition model and conduct numerical simulations,which successfully rationalizes the non-diffusive behavior and fits experimental data.Our data and theory imply an optimum soaking time in tight oil recovery by countercurrent imbibition,beyond which increasing exposed fracture surface area becomes a more efficient enhanced oil recovery(EOR)strategy than soaking for longer time.展开更多
Based on imbibition replacement of shut-in well in tight oil reservoirs, this paper expounds the principle of saturation rebalancing during the shut-in process after fracturing, establishes an optimization method for ...Based on imbibition replacement of shut-in well in tight oil reservoirs, this paper expounds the principle of saturation rebalancing during the shut-in process after fracturing, establishes an optimization method for shut-in time after horizontal well volume fracturing with the goal of shortening oil breakthrough time and achieving rapid oil breakthrough, and analyzes the influences of permeability, porosity, fracture half-length and fracturing fluid volume on the shut-in time. The oil and water imbibition displacement in the matrix and fractures occurs during the shut-in process of wells after fracturing. If the shut-in time is too short, the oil-water displacement is not sufficient, and the oil breakthrough time is long after the well is put into production. If the shut-in time is too long, the oil and water displacement is sufficient, but the energy dissipation in the formation near the bottom of the well is severe, and the flowing period is short and the production is low after the well is put into production. A rational shut-in time can help shorten the oil breakthrough time, extend the flowing period and increase the production of the well. The rational shut-in time is influenced by factors such as permeability, porosity, fracture half-length and fracturing fluid volume. The shortest and longest shut-in times are negatively correlated with porosity, permeability, and fracture half-length, and positively correlated with fracturing fluid volume. The pilot test in tight oil horizontal wells in the Songliao Basin, NE China, has confirmed that the proposed optimization method can effectively improve the development effect of horizontal well volume fracturing.展开更多
Horizontal well drilling and multistage hydraulic fracturing have been demonstrated as effective approaches for stimulating oil production in the Bakken tight oil reservoir.However,after multiple years of production,p...Horizontal well drilling and multistage hydraulic fracturing have been demonstrated as effective approaches for stimulating oil production in the Bakken tight oil reservoir.However,after multiple years of production,primary oil recovery in the Bakken is generally less than 10%of the estimated original oil in place.Gas huff‘n’puff(HnP)has been tested in the Bakken Formation as an enhanced oil recovery(EOR)method;however,most field pilot test results showed no significant incremental oil production.One of the factors affecting HnP EOR performance is premature gas breakthrough,which is one of the most critical issues observed in the field because of the presence of interwell fractures.Consequently,injected gas rapidly reaches adjacent production wells without contacting reservoir rock and increasing oil recovery.Proper conformance control is therefore needed to avoid early gas breakthrough and improve EOR performance.In this study,a rich gas EOR pilot in the Bakken was carefully analyzed to collect the essential reservoir and operational data.A simulation model with 16 wells was then developed to reproduce the production history and predict the EOR performance with and without conformance control.EOR operational strategies,including single-and multiple-well HnP,with different gas injection constraints were investigated.The simulation results of single-well HnP without conformance control showed that a rich gas injection rate of at least 10 MMscfd was needed to yield meaningful incremental oil production.The strategy of conformance control via water injection could significantly improve oil production in the HnP well,but injecting an excessive amount of water also leads to water breakthrough and loss of oil production in the offset wells.By analyzing the production performance of the wells individually,the arrangement of wells was optimized for multiple-well HnP EOR.The multiwell results showed that rich gas EOR could improve oil production up to 7.4%by employing conformance control strategies.Furthermore,replacing rich gas with propane as the injection gas could result in 14%of incremental oil production.展开更多
Hydraulic fracturing facilitates the development and exploitation of unconventional reservoirs.In this study,the injected hydraulic fracturing fluid(HFF)and flowback and produced water(FPW)in tight oil reservoirs of t...Hydraulic fracturing facilitates the development and exploitation of unconventional reservoirs.In this study,the injected hydraulic fracturing fluid(HFF)and flowback and produced water(FPW)in tight oil reservoirs of the Lucaogou Formation in the Junggar Basin are temporally sampled from day 1 to day 64.Freshwater is used for fracturing,and HFF is obtained.The chemical and isotopic parameters(including the water type,total salinity,total dissolved solids(TDS),pH,concentrations of Na^(+),Cl^(-),Ba^(+),K^(+),Fe^(2+)+Fe^(3+),and CO_(3)^(2-),dD,and δ^(18)O)are experimentally obtained,and their variations with time are systematically analyzed based on the flowback water.The results show that the water type,Na/Cl ratio,total salinity,and TDS of the FPW change periodically primarily due to the HFF mixing with formation water,thus causing δD and δ^(18)O to deviate from the meteoric water line of Xinjiang.Because of watererock interaction(WRI),the concentrations of Fe^(2+)+Fe^(3+)and CO_(3)^(2-)of the FPW increase over time,with the solution pH becoming more alkaline.Furthermore,based on the significant changes observed in the geochemistry of the FPW,three separate time intervals of flowback time are identified:Stage Ⅰ(<10 days),where the FPW is dominated by the HFF and the changes in ions and isotopes are mainly caused by the WRI;Stage Ⅱ(10-37 days),where the FPW is dominated by the addition of formation water to the HFF and the WRI is weakened;and finally,Stage Ⅲ(>37 days),where the FPW is dominated by the chemistry of the formation water.The methodology implemented in this study can provide critical support for the source identification of formation water.展开更多
Tight oil reservoirs are contributing a major role to fulfill the overall crude oil needs,especially in the US.However,the dilemma is their ultra-tight permeability and an uneconomically short-lived primary recovery f...Tight oil reservoirs are contributing a major role to fulfill the overall crude oil needs,especially in the US.However,the dilemma is their ultra-tight permeability and an uneconomically short-lived primary recovery factor.Therefore,the application of EOR in the early reservoir development phase is considered effective for fast-paced and economical tight oil recovery.To achieve these objectives,it is imperative to determine the optimum EOR potential and the best-suited EOR application for every individual tight oil reservoir to maximize its ultimate recovery factor.Since most of the tight oil reservoirs are found in wide spatial source rock with complex and compacted pores and poor geophysical properties yet they hold high saturation of good quality oil and therefore,every single percent increase in oil recovery from such huge reservoirs potentially provide an additional million barrels of oil.Hence,the EOR application in such reservoirs is quite essential.However,the physical understanding of EOR applications in different circumstances from laboratory to field scale is the key to success and similarly,the fundamental physical concepts of fluid flow-dynamics under confinement conditions play an important role.This paper presents a detailed discussion on laboratory-based experimental achievements at micro-scale including fundamental concepts under confinement environment,physics-based numerical studies,and recent actual field piloting experiences based on the U.S.unconventional plays.The objective of this paper is to discuss all the critical reservoir rock and fluid properties and their contribution to reservoir development through massive multi-staged hydraulic fracture networks and the EOR applications.Especially the CO_(2)and produced hydrocarbon gas injection through single well-based huff-n-puff operational constraints are discussed in detail both at micro and macro scale.展开更多
Xin’anbian Oilfield of the Ordos Basin is the large tight oilfield to be first exploration discovery in china.The production of tight oil increased significantly in recent years.It shows great exploration potential o...Xin’anbian Oilfield of the Ordos Basin is the large tight oilfield to be first exploration discovery in china.The production of tight oil increased significantly in recent years.It shows great exploration potential of Chang 7 tight oil.But the physical property and hydrocarbon enrichment characteristics of Chang 7 tight oil reservoirs were rarely studied,The forming conditions of tight oil reservoirs are systematically summarized and analyzed through the study of hydrocarbon generation,sedimentary reservoirs and hydrocarbon migration and accumulation based on production and core experimental data.The result shows that,The porosity of the Chang 7_(2)reservoir mainly distributed in 5.0-11.0%,average at 7.9%,The permeability mainly distributed in 0.04-0.18×10^(-3)μm^(2),average at 0.12×10^(-3)μm^(2),The pore diameters of the tight oil reservoir distributed in 2-8μm.The high-quality Chang 7_(3)source rocks and the micropsammite of Chang 7_(2)subaqueous distributary channel were widely distributed in the study area.The lenticular or banded sand bodies are distributed among mudstone or hydrocarbon source rocks and have the advantage of migration distance for hydrocarbon accumulation.The reservoir space is composed of micro-nanometer pores and throat,that is formed in the process of increasing pressure during hydrocarbon generation and hydrocarbon accumulation.The Chang 7 tight oil was generated in the early Cretaceous and injected into the sand of the subaqueous distributary channel driven by continuous hydrocarbon generation supercharging.The formation and accumulation of tight oil reservoirs are mainly controlled by source rocks,sedimentary microfacies and reservoirs of good quality.展开更多
This study aimed to investigate the complete distribution of reservoir space in tight oil sandstone combining casting slices, field emission scanning electron microscopy(FE-SEM), the pore-throat theory model, high-res...This study aimed to investigate the complete distribution of reservoir space in tight oil sandstone combining casting slices, field emission scanning electron microscopy(FE-SEM), the pore-throat theory model, high-resolution image processing, mathematical statistics, and other technical means. Results of reservoir samples from the Xin’anbian area of Ordos Basin showed that the total pore radius curve of the tight oil sandstone reservoir exhibited a multi-peak distribution, and the peaks appeared to be more focused on the ends of the range. This proved that pores with a radius of 1–50,000 nm provided the most significant storage space for tight oil, indicating that special attention should be paid to this range of the pore size distribution. Meanwhile, the complete throat radius curve of the tight oil sandstone reservoir exhibited a multipeak distribution. However, the peak values were distributed throughout the scales. This confirmed that the throat radius in the tight oil sandstone reservoir was not only in the range of hundreds of nanometers but was also widely distributed in the scale approximately equal to the pore size. The new rapid determination method could provide a precise theoretical basis for the comprehensive evaluation, exploration, and development of a tight oil sandstone reservoir.展开更多
Nitrogen huff-n-puff(N_(2)HnP) appears to be an economical and high-efficiency enhanced oil recovery(EOR) technique for tight oil reservoirs.There is however a lack of understanding of the pore-level EOR performance o...Nitrogen huff-n-puff(N_(2)HnP) appears to be an economical and high-efficiency enhanced oil recovery(EOR) technique for tight oil reservoirs.There is however a lack of understanding of the pore-level EOR performance of N2HnP under tight reservoir conditions.In this work,a non-magnetic reactor was created and combined with a nuclear magnetic resonance(NMR) device for real-time monitoring of oil distribution in the HnP experiment.N_(2)HnP experiments were then performed in a tight sandstone core sample at a temperature of 353 K and an injection pressure≥ 24 MPa.The pore-level oil distribution under reservoir conditions was monitored and the EOR performance of N2HnP in specific pores was analyzed.The pore throat structures of the core sample and the phase behavior of the N_(2)-Oil system were analyzed to elucidate the EOR mechanism of N_(2)HnP.An oil recovery factor of 37.52% can be achieved after four cycles,which proves the EOR potential of N_(2)HnP for tight reservoirs.The highest recoveries after N_(2)HnP are obtained in the large pores,followed by the medium pores,the small pores,and finally the micro pores.Increases in soaking time and injection pressure resulted in slight and pronounced increases in oil recovery,respectively,both of which are mainly reflected in the first cycle.Specifically,increasing the soaking time only slightly improves the cumulative oil recovery in the small pores while increasing the injection pressure significantly improves the cumulative oil recovery in the small,medium,and large pores simultaneously.However,variations in both injection pressure and soaking time have a negligible effect on the cumulative oil recovery of the micro pores.展开更多
CO_(2)huff and puff experiments of different injection parameters,production parameters and soaking time were carried out on large-scale cubic and long columnar outcrop samples to analyze dynamic characteristics and i...CO_(2)huff and puff experiments of different injection parameters,production parameters and soaking time were carried out on large-scale cubic and long columnar outcrop samples to analyze dynamic characteristics and influencing factors of CO_(2)huff and puff and the contribution of sweeping mode to recovery.The experimental results show that the development process of CO_(2)huff and puff can be divided into four stages,namely,CO_(2)backflow,production of gas with some oil,high-speed oil production,and oil production rate decline stages.The production of gas with some oil stage is dominated by free gas displacement,and the high-speed oil production stage is dominated by dissolved gas displacement.CO_(2)injection volume and development speed are the major factors affecting the oil recovery.The larger the injected CO_(2)volume and the lower the development speed,the higher the oil recovery will be.The reasonable CO_(2)injection volume and development speed should be worked out according to oilfield demand and economic evaluation.There is a reasonable soaking time in CO_(2)huff and puff.Longer soaking time than the optimum time makes little contribution to oil recovery.In field applications,the stability of bottom hole pressure is important to judge whether the soaking time is sufficient during the huff period.The oil recovery of CO_(2)huff and puff mainly comes from the contribution of flow sweep and diffusion sweep,and diffusion sweep contributes more to the oil recovery when the soaking time is sufficient.展开更多
Tight oil reservoir development is faced with the key technical problem that"water cannot be injected and oil cannot be produced"yet.With the diphenyl ethers water-soluble(gemini)surfactants as water phase s...Tight oil reservoir development is faced with the key technical problem that"water cannot be injected and oil cannot be produced"yet.With the diphenyl ethers water-soluble(gemini)surfactants as water phase shell and C10–C14 straight-chain hydrocarbon compounds as oil phase kernel,a nanofluids permeation flooding system was prepared by microemulsion technology,and its characteristics and EOR mechanisms were evaluated through experiments.The system has the following five characteristics:(1)"Small-size liquid":the average particle size of the system is less than 30 nm,which can greatly reduce the starting pressure gradient of water injection,and effectively enter and expand the sweep volume of micro-nano matrix;(2)"Small-size oil":the system can break the crude oil into"small-size oil"under the flow condition,which can greatly improve the percolation ability and displacement efficiency of the crude oil in the micro-nano matrix;(3)Dual-phase wetting:the system has contact angles with the water-wet and oil-wet interfaces of(46±1)°and(68±1)°respectively,and makes it possible for capillarity to work fully under complex wetting conditions of the reservoir;(4)High surface activity:the interfacial tension between the system and crude oil from a tight oil reservoir in Xinjiang is 10-3–10-2 mN/m,indicating the system can effectively improve the displacement efficiency of oil in fine pore throats;(5)Demulsification and viscosity reduction:the system has a demulsification and viscosity reduction rate of more than 80%to inversely emulsified crude oil from a tight oil reservoir in Xinjiang,so it can improve the mobility of crude oil in the reservoir and wellbore.The system can be used to increase oil production by fracturing in tight reservoirs,replenish formation energy by reducing injection pressure and increasing injection rate,and enhance oil recovery by displacement and cyclic injection,providing key technical support for effective production and efficient development and recovery enhancement of tight reservoirs.展开更多
Nanofluids have been effective chemical additives for enhanced oil recovery(EOR)in tight oil reservoirs due to their special properties.However,oil imbibition recoveries vary for different nanofluids.The oil/water dis...Nanofluids have been effective chemical additives for enhanced oil recovery(EOR)in tight oil reservoirs due to their special properties.However,oil imbibition recoveries vary for different nanofluids.The oil/water distribution in rocks during imbibition using various nanofluids was less discussed in previous studies.In this study,we systematically examined the imbibition efficiencies of various nanofluids at60℃.Furthermore,the migration of nanofluids and oil distribution in the rock pores were monitored using nuclear magnetic resonance(NMR).The nanofluids were prepared by dispersing silica nanoparticles and five different types of surfactants i.e.,anionic-nonionic,anionic,nonionic,amphoteric and cationic surfactants in deionized(DI)water.Subsequently,interfacial tension(IFT)and contact angle measurements were conducted to reveal the underlying EOR mechanisms of various nanofluids.The experimental results showed that the EOR potential of the different types of nanofluids was in the order anionic-nonionic>anionic>nonionic>amphoteric>cationic>brine.Anionic-nonionic(sodium lauryl ether sulfate(SLES))and anionic(sodium dodecyl sulfonate(SDS))nanofluids exhibited excellent capability of wettability alteration,and increased oil recovery by 27.96%and 23.08%,respectively,compared to brine.The NMR results also showed that mesopores(0.1-1μm)were the dominant developed pores in the rocks,and contributed the most to imbibition efficiency.In addition,the imbibition of nanofluids initially took place in mesopores and micropores before moving into macropores.This study provides fundamental information on the selection of nanofluids for EOR in tight oil reservoirs.The study also improved the understanding of oil/water distribution during the imbibition of the proposed nanofluids.展开更多
A mathematical model, fully coupling multiple porous media deformation and fluid flow, was established based on the elastic theory of porous media and fluid-solid coupling mechanism in tight oil reservoirs. The finite...A mathematical model, fully coupling multiple porous media deformation and fluid flow, was established based on the elastic theory of porous media and fluid-solid coupling mechanism in tight oil reservoirs. The finite element method was used to determine the numerical solution and the accuracy of the model was verified. On this basis, the model was used to simulate productivity of multistage fractured horizontal wells in tight oil reservoirs. The results show that during the production of tight oil wells, the reservoir region close to artificial fractures deteriorated in physical properties significantly, e.g. the aperture and conductivity of artificial fractures dropped by 52.12% and 89.02% respectively. The simulations of 3000-day production of a horizontal well in tight oil reservoir showed that the predicted productivity by the uncoupled model had an error of 38.30% from that by the fully-coupled model. Apparently, ignoring the influence of fluid-solid interaction effect led to serious deviations of the productivity prediction results. The productivity of horizontal well in tight oil reservoir was most sensitive to the start-up pressure gradient, and second most sensitive to the opening of artificial fractures. Enhancing the initial conductivity of artificial fractures was helpful to improve the productivity of tight oil wells. The influence of conductivity, spacing, number and length of artificial fractures should be considered comprehensively in fracturing design. Increasing the number of artificial fractures unilaterally could not achieve the expected increase in production.展开更多
Based on the microscopic pore-throat characterization of typical continental tight reservoirs in China,such as sandstone of Cretaceous Qingshankou and Quantou formations in Songliao Basin,NE China sandy conglomerate o...Based on the microscopic pore-throat characterization of typical continental tight reservoirs in China,such as sandstone of Cretaceous Qingshankou and Quantou formations in Songliao Basin,NE China sandy conglomerate of Baikouquan Formation in Mahu area and hybrid rock of Lucaogou Formation in Jimusaer sag of Junggar Basin,NE China the theoretical lower limit,oil accumulation lower limit,effective flow lower limit and the upper limit of tight oil reservoirs were defined by water film thickness method,oil bearing occurrence method,oil testing productivity method and mechanical balance method,respectively.Cluster analysis method was used to compare the differences in pore-throat structure of different tight reservoirs,determine the grading criterion of tight reservoirs,and analyze its correlation with the limit of reservoir formation.The results show that the boundary between tight reservoir and conventional reservoir corresponds to the upper limit of physical properties,the boundary of classⅡand classⅢtight reservoirs corresponds to the lower limit of effective flow,the boundary of classⅢand classⅣtight reservoirs corresponds to the lower limit of reservoir forming,and the theoretical lower limit of tight reservoir corresponds to the boundary between tight reservoir and non-reservoir.Finally,the application results of the grading evaluation criterion show that the tight oil productivity is highly controlled by the type of tight reservoir,and classⅠand classⅡtight reservoirs are the favorable sections for high production of tight oil.展开更多
Taking the tight oil of the Zhongnan sag in the Ordos Basin,Jimusar sag in the Junggar Basin and Qingxi sag in the Jiuquan Basin as study objects,based on field survey,dissection of tight oil reservoirs,sample test,mo...Taking the tight oil of the Zhongnan sag in the Ordos Basin,Jimusar sag in the Junggar Basin and Qingxi sag in the Jiuquan Basin as study objects,based on field survey,dissection of tight oil reservoirs,sample test,modeling experiment and comprehensive analysis,this study reveals that the tight oil accumulates at start-up pressure,advances under differential pressure,diffuses at alternating fast and low speeds,charges in stepped large area and migrates rapidly through fractures,and enriches in dominant fractures and pores.The root cause of ladder-like charge is the multiple scales of pores.The widespread source rock with high hydrocarbon generation intensity is the material basis for tight oil enrichment;the dominant source reservoir assemblage is the basic unit for tight oil enrichment;fractures and beddings are conducive to local rapid migration of tight oil;fractures and pores work together to control the enrichment of tight oil.Two typical accumulation models of tight oil are established,namely"source reservoir in coexistence,four optimal factors controlling enrichment around central area,and large-scale continuous distribution"for a large freshwater lake clastic rock basin and"source reservoir integration,four optimal factors controlling enrichment,central area distribution,small in size but high in enrichment degree"for a small saline lake diamictite depression.展开更多
To deal with the stress interference caused by simultaneous propagation of multiple fractures and the wettability reversal and physical property changes of the reservoir caused by fracturing fluid getting in during la...To deal with the stress interference caused by simultaneous propagation of multiple fractures and the wettability reversal and physical property changes of the reservoir caused by fracturing fluid getting in during large-volume fracturing of tight oil reservoirs through a horizontal well, a non-planar 3D fracture growth model was built, wettability reversal characterizing parameters and change of relative permeability curve were introduced to correct the production prediction model of fractured horizontal well, a fracturing design optimization software(Fr Smart) by integrating geological and engineering data was developed, and a fracturing design optimization approach for tight oil reservoirs based on fracture control was worked out. The adaptability of the method was analyzed and the fracture parameters of horizontal wells in tight oil reservoirs were optimized. The simulation results show that fracturing technology based on fracture control is suitable for tight oil reservoirs, and by optimizing fracture parameters, this technology makes it possible to produce the maximum amount of reserves in the well-controlled unit of unconventional reservoirs. The key points of fracturing design optimization based on fracture control include increasing lateral length of and reducing the row spacing between horizontal wells, increasing perforation clusters in one stage to decrease the spacing of neighboring fractures, and also avoiding interference of old and new fracturing wells. Field tests show that this technology can increase single well production and ultimate recovery. Using this technology in developing unconventional resources such as tight oil reservoirs in China will enhance the economics significantly.展开更多
基金The authors gratefully acknowledge the financial supports from the National Science Foundation of China under Grant 52274027 as well as the High-end Foreign Experts Recruitment Plan of the Ministry of Science and Technology China under Grant G2022105027L.
文摘Field evidence indicates that proppant distribution and threshold pressure gradient have great impacts on well productivity.Aiming at the development of unconventional oil reservoirs in Triassic Chang-7 Unit,Ordos Basin of China,we presented an integrated workflow to investigate how(1)proppant placement in induced fracture and(2)non-linear flow in reservoir matrix would affect well productivity and fluid flow in the reservoir.Compared with our research before(Yue et al.,2020),here we extended this study into the development of multi-stage fractured horizontal wells(MFHWs)with large-scale complicated fracture geometry.The integrated workflow is based on the finite element method and consists of simulation models for proppant-laden fluid flow,fracture flow,and non-linear seepage flow,respectively.Simulation results indicate that the distribution of proppant inside the induced cracks significantly affects the productivity of the MFHW.When we assign an idealized proppant distribution instead of the real distribution,there will be an overestimation of 44.98%in daily oil rate and 30.63%in cumulative oil production after continuous development of 1000 days.Besides,threshold pressure gradient(TPG)also significantly affects the well performance in tight oil reservoirs.If we simply apply linear Darcy’s law to the reservoir matrix,the overall cumulative oil production can be overrated by 77%after 1000 days of development.In general,this research provides new insights into the development of tight oil reservoirs with TPG and meanwhile reveals the significance of proppant distribution and non-linear fluid flow in the production scenario design.
基金The authors sincerely appreciate the financial support from the National Natural Science Foundation of China(No.52074279,51874261).
文摘Slickwater fracturing fluids have gained widespread application in the development of tight oil reservoirs. After the fracturing process, the active components present in slickwater can directly induce spontaneous imbibition within the reservoir. Several variables influence the eventual recovery rate within this procedure, including slickwater composition, formation temperature, degree of reservoir fracture development, and the reservoir characteristics. Nonetheless, the underlying mechanisms governing these influences remain relatively understudied. In this investigation, using the Chang-7 block of the Changqing Oilfield as the study site, we employ EM-30 slickwater fracturing fluid to explore the effects of the drag-reducing agent concentration, imbibition temperature, core permeability, and core fracture development on spontaneous imbibition. An elevated drag-reducing agent concentration is observed to diminish the degree of medium and small pore utilization. Furthermore, higher temperatures and an augmented permeability enhance the fluid flow properties, thereby contributing to an increased utilization rate across all pore sizes. Reduced fracture development results in a lower fluid utilization across diverse pore types. This study deepens our understanding of the pivotal factors affecting spontaneous imbibition in tight reservoirs following fracturing. The findings act as theoretical, technical, and scientific foundations for optimizing fracturing strategies in tight oil reservoir transformations.
基金funded by the shale oil and gas geological survey project in Quemoco sag,Qiangtang Basin of China Geological Survey(DD20221855,DD20230315).
文摘The Daqing exploration area in the northern Songliao Basin has great potential for unconventional oil and gas resources,among which the total resources of tight oil alone exceed 109 t and is regarded as an important resource base of Daqing oilfield.After years of exploration in the Qijia area,Songliao Basin,NE China,tight oil has been found in the Upper Cretaceous Qingshankou Formation.To work out tight oil’s geological characteristics,taking tight oil in Gaotaizi oil layers of the Upper Cretaceous Qingshankou Formation in northern Songliao Basin as an example,this paper systematically analyzed the geological characteristics of unconventional tight oil in Gao3 and Gao4 layers of the Qijia area,based on the data of the geological survey,well drilling journey,well logging,and test.It is that three sets of hydrocarbon source rocks(K2qn1,K2qn2+3,and K2n1)develop in the examined area,and exhibit excellent type I and II kerogens,high organic matter abundance,and moderate maturity.The reservoir is generally composed of thin-bedded mudstone,siltstone,and sandstone,and presents poor porosity(average 8.5 vol.%)and air permeability(average 4 mD).The main reservoir space primarily includes intergranular pores,secondary soluble pores,and intergranular soluble pores.Three types of orifice throats were identified,namely fine throat,extra-fine throat,and micro-fine throat.The siltstone is generally oil-bearing,the reservoirs with slime and calcium become worse oil-bearing,and the mudstone has no obvious oil-bearing characteristics.The brittleness indices of the sandstone in the tight oil reservoir range from 40%to 60%,and those of the mudstone range from 40%to 45%,indicating a better brittleness of the tight oil reservoir.Based on the study of typical core hole data,this paper gives a comprehensive evaluation of the properties of the tight oil and establishes a tight oil single well composite bar chart as well as the initial evaluation system with the core of properties in the tight oil reservoir.This study has theoretical guiding significance and practical application value for tight oil exploration and evaluation in the Qijia area.
基金Supported by the National Science and Technology Major Project of China(2016ZX05046-001).
文摘Based on the typical dissection of various onshore tight oil fields in China,the tight oil migration and accumulation mechanism and enrichment-controlling factors in continental lake basins are analyzed through nuclear magnetic resonance(NMR)displacement physical simulation and Lattice Boltzmann numerical simulation by using the samples of source rock,reservoir rock and crude oil.In continental lake basins,the dynamic forces driving hydrocarbon generation and expulsion of high-quality source rocks are the foundational power that determines the charging efficiency and accumulation effect of tight oil,the oil migration resistance is a key element that influences the charging efficiency and accumulation effect of tight oil,and the coupling of charging force with pore-throat resistance in tight reservoir controls the tight oil accumulation and sweet spot enrichment.The degree of tight oil enrichment in continental lake basins is controlled by four factors:source rock,reservoir pore-throat size,anisotropy of reservoir structure,and fractures.The high-quality source rocks control the near-source distribution of tight oil,reservoir physical properties and pore-throat size are positively correlated with the degree of tight oil enrichment,the anisotropy of reservoir structure reveals that the parallel migration rate is the highest,and intralayer fractures can improve the migration and accumulation efficiency and the oil saturation.
基金sincerely appreciate the financial support from the National Key Research and Development Project(2019YFA0708700)the National Natural Science Foundation of China(51834010,51874261,51874337)+1 种基金the Key Research and Development Program of Shaanxi(2021GY-112)a Discovery Grant from Natural Sciences and Engineering Research Council of Canada(NSERC RGPIN-2017-05080).
文摘The traditional multi-process to enhance tight oil recovery based on fracturing and huff-n-puff has obvious deficiencies,such as low recovery efficiency,rapid production decline,high cost,and complexity,etc.Therefore,a new technology,the so-called fracturing-oil expulsion integration,which does not need flowback after fracturing while making full use of the fracturing energy and gel breaking fluids,are needed to enable efficient exploitation of tight oil.A novel triple-responsive smart fluid based on“pseudo-Gemini”zwitterionic viscoelastic surfactant(VES)consisting of N-erucylamidopropyl-N,N-dimethyl-3-ammonio-2-hydroxy-1-propane-sulfonate(EHSB),N,N,N′,N′-tetramethyl-1,3-propanediamine(TMEDA)and sodium p-toluenesulfonate(NaPts),is developed.Then,the rheology of smart fluid is systematically studied at varying conditions(CO_(2),temperature and pressure).Moreover,the mechanism of triple-response is discussed in detail.Finally,a series of fracturing and spontaneous imbibition performances are systematically investigated.The smart fluid shows excellent CO_(2)-,thermal-,and pressure-triple responsive behavior.It can meet the technical requirement of tight oil fracturing construction at 140°C in the presence of 3.5 MPa CO_(2).The gel breaking fluid shows excellent spontaneous imbibition oil expulsion(∼40%),salt resistance(1.2×104 mg/L Na+),temperature resistance(140°C)and aging stability(30 days).
文摘Countercurrent imbibition is an important mechanism for tight oil recovery,that is,water imbibes spontaneously from the fracture into the porous matrix while oil flows reversely into the fracture.Its significance over cocurrent imbibition and forced imbibition is highlighted when permeability reduces.We used the computed tomography(CT)scanning to measure the one-dimensional evolution of water saturation profile and countercurrent imbibition distance(CID)at different fluid pressures,initial water saturations,and permeability.Surprisingly,experiments show that CID evolution for tight reservoir cores dramatically deviates from the classical diffusive rule(i.e.,evolutes proportional to square root of time,t^(0.5)).At early stage,CID extends faster than t^(0.5)(super-diffusive);while at late stage,CID extends much slower than t^(0.5)(sub-diffusive).After tens of hours,the CID change becomes too slow to be practically efficient for tight oil recovery.This research demonstrates that this deviation from classic theory is a result of(1)a much longer characteristic capillary length than effective invasion depth,which eliminates full development of a classical displacement front;and(2)non-zero flow at low water saturation,which was always neglected for conventional reservoir and is amplified in sub-mili-Darcy rocks.To well depict the details of the imbibition front in this situation,we introduce non-zero wetting phase fluidity at low saturation into classical countercurrent imbibition model and conduct numerical simulations,which successfully rationalizes the non-diffusive behavior and fits experimental data.Our data and theory imply an optimum soaking time in tight oil recovery by countercurrent imbibition,beyond which increasing exposed fracture surface area becomes a more efficient enhanced oil recovery(EOR)strategy than soaking for longer time.
基金Supported by China National Major Project of Science and Technology(2016ZX05046-004)PetroChina Major Project of Science and Technology(2017B-4905)PetroChina Jilin Oilfield Company Major Project of Science and Technology(JY21A2-12).
文摘Based on imbibition replacement of shut-in well in tight oil reservoirs, this paper expounds the principle of saturation rebalancing during the shut-in process after fracturing, establishes an optimization method for shut-in time after horizontal well volume fracturing with the goal of shortening oil breakthrough time and achieving rapid oil breakthrough, and analyzes the influences of permeability, porosity, fracture half-length and fracturing fluid volume on the shut-in time. The oil and water imbibition displacement in the matrix and fractures occurs during the shut-in process of wells after fracturing. If the shut-in time is too short, the oil-water displacement is not sufficient, and the oil breakthrough time is long after the well is put into production. If the shut-in time is too long, the oil and water displacement is sufficient, but the energy dissipation in the formation near the bottom of the well is severe, and the flowing period is short and the production is low after the well is put into production. A rational shut-in time can help shorten the oil breakthrough time, extend the flowing period and increase the production of the well. The rational shut-in time is influenced by factors such as permeability, porosity, fracture half-length and fracturing fluid volume. The shortest and longest shut-in times are negatively correlated with porosity, permeability, and fracture half-length, and positively correlated with fracturing fluid volume. The pilot test in tight oil horizontal wells in the Songliao Basin, NE China, has confirmed that the proposed optimization method can effectively improve the development effect of horizontal well volume fracturing.
基金supported by the U.S.Department of Energy National Energy Technology Laboratory under Award No.DEFE0024233the North Dakota Industrial Commission under the Award Nos.G-04-080(BPOP 2.0)and G-051-98(BPOP 3.0).
文摘Horizontal well drilling and multistage hydraulic fracturing have been demonstrated as effective approaches for stimulating oil production in the Bakken tight oil reservoir.However,after multiple years of production,primary oil recovery in the Bakken is generally less than 10%of the estimated original oil in place.Gas huff‘n’puff(HnP)has been tested in the Bakken Formation as an enhanced oil recovery(EOR)method;however,most field pilot test results showed no significant incremental oil production.One of the factors affecting HnP EOR performance is premature gas breakthrough,which is one of the most critical issues observed in the field because of the presence of interwell fractures.Consequently,injected gas rapidly reaches adjacent production wells without contacting reservoir rock and increasing oil recovery.Proper conformance control is therefore needed to avoid early gas breakthrough and improve EOR performance.In this study,a rich gas EOR pilot in the Bakken was carefully analyzed to collect the essential reservoir and operational data.A simulation model with 16 wells was then developed to reproduce the production history and predict the EOR performance with and without conformance control.EOR operational strategies,including single-and multiple-well HnP,with different gas injection constraints were investigated.The simulation results of single-well HnP without conformance control showed that a rich gas injection rate of at least 10 MMscfd was needed to yield meaningful incremental oil production.The strategy of conformance control via water injection could significantly improve oil production in the HnP well,but injecting an excessive amount of water also leads to water breakthrough and loss of oil production in the offset wells.By analyzing the production performance of the wells individually,the arrangement of wells was optimized for multiple-well HnP EOR.The multiwell results showed that rich gas EOR could improve oil production up to 7.4%by employing conformance control strategies.Furthermore,replacing rich gas with propane as the injection gas could result in 14%of incremental oil production.
基金supported by the National Natural Science Foundation of China(No.U2003102).
文摘Hydraulic fracturing facilitates the development and exploitation of unconventional reservoirs.In this study,the injected hydraulic fracturing fluid(HFF)and flowback and produced water(FPW)in tight oil reservoirs of the Lucaogou Formation in the Junggar Basin are temporally sampled from day 1 to day 64.Freshwater is used for fracturing,and HFF is obtained.The chemical and isotopic parameters(including the water type,total salinity,total dissolved solids(TDS),pH,concentrations of Na^(+),Cl^(-),Ba^(+),K^(+),Fe^(2+)+Fe^(3+),and CO_(3)^(2-),dD,and δ^(18)O)are experimentally obtained,and their variations with time are systematically analyzed based on the flowback water.The results show that the water type,Na/Cl ratio,total salinity,and TDS of the FPW change periodically primarily due to the HFF mixing with formation water,thus causing δD and δ^(18)O to deviate from the meteoric water line of Xinjiang.Because of watererock interaction(WRI),the concentrations of Fe^(2+)+Fe^(3+)and CO_(3)^(2-)of the FPW increase over time,with the solution pH becoming more alkaline.Furthermore,based on the significant changes observed in the geochemistry of the FPW,three separate time intervals of flowback time are identified:Stage Ⅰ(<10 days),where the FPW is dominated by the HFF and the changes in ions and isotopes are mainly caused by the WRI;Stage Ⅱ(10-37 days),where the FPW is dominated by the addition of formation water to the HFF and the WRI is weakened;and finally,Stage Ⅲ(>37 days),where the FPW is dominated by the chemistry of the formation water.The methodology implemented in this study can provide critical support for the source identification of formation water.
文摘Tight oil reservoirs are contributing a major role to fulfill the overall crude oil needs,especially in the US.However,the dilemma is their ultra-tight permeability and an uneconomically short-lived primary recovery factor.Therefore,the application of EOR in the early reservoir development phase is considered effective for fast-paced and economical tight oil recovery.To achieve these objectives,it is imperative to determine the optimum EOR potential and the best-suited EOR application for every individual tight oil reservoir to maximize its ultimate recovery factor.Since most of the tight oil reservoirs are found in wide spatial source rock with complex and compacted pores and poor geophysical properties yet they hold high saturation of good quality oil and therefore,every single percent increase in oil recovery from such huge reservoirs potentially provide an additional million barrels of oil.Hence,the EOR application in such reservoirs is quite essential.However,the physical understanding of EOR applications in different circumstances from laboratory to field scale is the key to success and similarly,the fundamental physical concepts of fluid flow-dynamics under confinement conditions play an important role.This paper presents a detailed discussion on laboratory-based experimental achievements at micro-scale including fundamental concepts under confinement environment,physics-based numerical studies,and recent actual field piloting experiences based on the U.S.unconventional plays.The objective of this paper is to discuss all the critical reservoir rock and fluid properties and their contribution to reservoir development through massive multi-staged hydraulic fracture networks and the EOR applications.Especially the CO_(2)and produced hydrocarbon gas injection through single well-based huff-n-puff operational constraints are discussed in detail both at micro and macro scale.
基金financially supported by the Chinese National Special Plan Project"Formation conditions,enrichment regularity and resource potential of tight oil”(No.2016ZX05046-001)。
文摘Xin’anbian Oilfield of the Ordos Basin is the large tight oilfield to be first exploration discovery in china.The production of tight oil increased significantly in recent years.It shows great exploration potential of Chang 7 tight oil.But the physical property and hydrocarbon enrichment characteristics of Chang 7 tight oil reservoirs were rarely studied,The forming conditions of tight oil reservoirs are systematically summarized and analyzed through the study of hydrocarbon generation,sedimentary reservoirs and hydrocarbon migration and accumulation based on production and core experimental data.The result shows that,The porosity of the Chang 7_(2)reservoir mainly distributed in 5.0-11.0%,average at 7.9%,The permeability mainly distributed in 0.04-0.18×10^(-3)μm^(2),average at 0.12×10^(-3)μm^(2),The pore diameters of the tight oil reservoir distributed in 2-8μm.The high-quality Chang 7_(3)source rocks and the micropsammite of Chang 7_(2)subaqueous distributary channel were widely distributed in the study area.The lenticular or banded sand bodies are distributed among mudstone or hydrocarbon source rocks and have the advantage of migration distance for hydrocarbon accumulation.The reservoir space is composed of micro-nanometer pores and throat,that is formed in the process of increasing pressure during hydrocarbon generation and hydrocarbon accumulation.The Chang 7 tight oil was generated in the early Cretaceous and injected into the sand of the subaqueous distributary channel driven by continuous hydrocarbon generation supercharging.The formation and accumulation of tight oil reservoirs are mainly controlled by source rocks,sedimentary microfacies and reservoirs of good quality.
基金This work was jointly supported by National Natural Science Foundation of China(Grant No.41902132,11872363,51861145314)PetroChina Innovation Foundation(Grant No.2019D-5007-0214)+2 种基金Chinese Academy of Sciences(CAS)through the CAS Key Research Program of Frontier Sciences(Grant No.QYZDJ-SSW-JSC019)the CAS Strategic Priority Research Program(Grant No.XDB22040401)National Science and Technology Mega Project of China(Grant No.2017ZX05013005-009).
文摘This study aimed to investigate the complete distribution of reservoir space in tight oil sandstone combining casting slices, field emission scanning electron microscopy(FE-SEM), the pore-throat theory model, high-resolution image processing, mathematical statistics, and other technical means. Results of reservoir samples from the Xin’anbian area of Ordos Basin showed that the total pore radius curve of the tight oil sandstone reservoir exhibited a multi-peak distribution, and the peaks appeared to be more focused on the ends of the range. This proved that pores with a radius of 1–50,000 nm provided the most significant storage space for tight oil, indicating that special attention should be paid to this range of the pore size distribution. Meanwhile, the complete throat radius curve of the tight oil sandstone reservoir exhibited a multipeak distribution. However, the peak values were distributed throughout the scales. This confirmed that the throat radius in the tight oil sandstone reservoir was not only in the range of hundreds of nanometers but was also widely distributed in the scale approximately equal to the pore size. The new rapid determination method could provide a precise theoretical basis for the comprehensive evaluation, exploration, and development of a tight oil sandstone reservoir.
基金financial support from the National Natural Science Foundation of China(52074319)the Strategic Cooperation Technology Project of CNPC(ZLZX2020-01-08)the Science Foundation of China University of Petroleum-Beijing(2462021QNXZ008)
文摘Nitrogen huff-n-puff(N_(2)HnP) appears to be an economical and high-efficiency enhanced oil recovery(EOR) technique for tight oil reservoirs.There is however a lack of understanding of the pore-level EOR performance of N2HnP under tight reservoir conditions.In this work,a non-magnetic reactor was created and combined with a nuclear magnetic resonance(NMR) device for real-time monitoring of oil distribution in the HnP experiment.N_(2)HnP experiments were then performed in a tight sandstone core sample at a temperature of 353 K and an injection pressure≥ 24 MPa.The pore-level oil distribution under reservoir conditions was monitored and the EOR performance of N2HnP in specific pores was analyzed.The pore throat structures of the core sample and the phase behavior of the N_(2)-Oil system were analyzed to elucidate the EOR mechanism of N_(2)HnP.An oil recovery factor of 37.52% can be achieved after four cycles,which proves the EOR potential of N_(2)HnP for tight reservoirs.The highest recoveries after N_(2)HnP are obtained in the large pores,followed by the medium pores,the small pores,and finally the micro pores.Increases in soaking time and injection pressure resulted in slight and pronounced increases in oil recovery,respectively,both of which are mainly reflected in the first cycle.Specifically,increasing the soaking time only slightly improves the cumulative oil recovery in the small pores while increasing the injection pressure significantly improves the cumulative oil recovery in the small,medium,and large pores simultaneously.However,variations in both injection pressure and soaking time have a negligible effect on the cumulative oil recovery of the micro pores.
文摘CO_(2)huff and puff experiments of different injection parameters,production parameters and soaking time were carried out on large-scale cubic and long columnar outcrop samples to analyze dynamic characteristics and influencing factors of CO_(2)huff and puff and the contribution of sweeping mode to recovery.The experimental results show that the development process of CO_(2)huff and puff can be divided into four stages,namely,CO_(2)backflow,production of gas with some oil,high-speed oil production,and oil production rate decline stages.The production of gas with some oil stage is dominated by free gas displacement,and the high-speed oil production stage is dominated by dissolved gas displacement.CO_(2)injection volume and development speed are the major factors affecting the oil recovery.The larger the injected CO_(2)volume and the lower the development speed,the higher the oil recovery will be.The reasonable CO_(2)injection volume and development speed should be worked out according to oilfield demand and economic evaluation.There is a reasonable soaking time in CO_(2)huff and puff.Longer soaking time than the optimum time makes little contribution to oil recovery.In field applications,the stability of bottom hole pressure is important to judge whether the soaking time is sufficient during the huff period.The oil recovery of CO_(2)huff and puff mainly comes from the contribution of flow sweep and diffusion sweep,and diffusion sweep contributes more to the oil recovery when the soaking time is sufficient.
基金Supported by the CNPC Science and Technology Major Project(2019E-2607)RIPED Discipline Construction Project(yjxk2019-12)
文摘Tight oil reservoir development is faced with the key technical problem that"water cannot be injected and oil cannot be produced"yet.With the diphenyl ethers water-soluble(gemini)surfactants as water phase shell and C10–C14 straight-chain hydrocarbon compounds as oil phase kernel,a nanofluids permeation flooding system was prepared by microemulsion technology,and its characteristics and EOR mechanisms were evaluated through experiments.The system has the following five characteristics:(1)"Small-size liquid":the average particle size of the system is less than 30 nm,which can greatly reduce the starting pressure gradient of water injection,and effectively enter and expand the sweep volume of micro-nano matrix;(2)"Small-size oil":the system can break the crude oil into"small-size oil"under the flow condition,which can greatly improve the percolation ability and displacement efficiency of the crude oil in the micro-nano matrix;(3)Dual-phase wetting:the system has contact angles with the water-wet and oil-wet interfaces of(46±1)°and(68±1)°respectively,and makes it possible for capillarity to work fully under complex wetting conditions of the reservoir;(4)High surface activity:the interfacial tension between the system and crude oil from a tight oil reservoir in Xinjiang is 10-3–10-2 mN/m,indicating the system can effectively improve the displacement efficiency of oil in fine pore throats;(5)Demulsification and viscosity reduction:the system has a demulsification and viscosity reduction rate of more than 80%to inversely emulsified crude oil from a tight oil reservoir in Xinjiang,so it can improve the mobility of crude oil in the reservoir and wellbore.The system can be used to increase oil production by fracturing in tight reservoirs,replenish formation energy by reducing injection pressure and increasing injection rate,and enhance oil recovery by displacement and cyclic injection,providing key technical support for effective production and efficient development and recovery enhancement of tight reservoirs.
基金financial support from the National Natural Science Foundation of China(No.51974282,52074249,51874261)Fundamental Research Funds for the Central Universities(2-9-2019-103)Key Research and Development Program of Shaanxi(No.2021GY-112)。
文摘Nanofluids have been effective chemical additives for enhanced oil recovery(EOR)in tight oil reservoirs due to their special properties.However,oil imbibition recoveries vary for different nanofluids.The oil/water distribution in rocks during imbibition using various nanofluids was less discussed in previous studies.In this study,we systematically examined the imbibition efficiencies of various nanofluids at60℃.Furthermore,the migration of nanofluids and oil distribution in the rock pores were monitored using nuclear magnetic resonance(NMR).The nanofluids were prepared by dispersing silica nanoparticles and five different types of surfactants i.e.,anionic-nonionic,anionic,nonionic,amphoteric and cationic surfactants in deionized(DI)water.Subsequently,interfacial tension(IFT)and contact angle measurements were conducted to reveal the underlying EOR mechanisms of various nanofluids.The experimental results showed that the EOR potential of the different types of nanofluids was in the order anionic-nonionic>anionic>nonionic>amphoteric>cationic>brine.Anionic-nonionic(sodium lauryl ether sulfate(SLES))and anionic(sodium dodecyl sulfonate(SDS))nanofluids exhibited excellent capability of wettability alteration,and increased oil recovery by 27.96%and 23.08%,respectively,compared to brine.The NMR results also showed that mesopores(0.1-1μm)were the dominant developed pores in the rocks,and contributed the most to imbibition efficiency.In addition,the imbibition of nanofluids initially took place in mesopores and micropores before moving into macropores.This study provides fundamental information on the selection of nanofluids for EOR in tight oil reservoirs.The study also improved the understanding of oil/water distribution during the imbibition of the proposed nanofluids.
基金Supported by the National Science and Technology Major Project (2017ZX05013-005)。
文摘A mathematical model, fully coupling multiple porous media deformation and fluid flow, was established based on the elastic theory of porous media and fluid-solid coupling mechanism in tight oil reservoirs. The finite element method was used to determine the numerical solution and the accuracy of the model was verified. On this basis, the model was used to simulate productivity of multistage fractured horizontal wells in tight oil reservoirs. The results show that during the production of tight oil wells, the reservoir region close to artificial fractures deteriorated in physical properties significantly, e.g. the aperture and conductivity of artificial fractures dropped by 52.12% and 89.02% respectively. The simulations of 3000-day production of a horizontal well in tight oil reservoir showed that the predicted productivity by the uncoupled model had an error of 38.30% from that by the fully-coupled model. Apparently, ignoring the influence of fluid-solid interaction effect led to serious deviations of the productivity prediction results. The productivity of horizontal well in tight oil reservoir was most sensitive to the start-up pressure gradient, and second most sensitive to the opening of artificial fractures. Enhancing the initial conductivity of artificial fractures was helpful to improve the productivity of tight oil wells. The influence of conductivity, spacing, number and length of artificial fractures should be considered comprehensively in fracturing design. Increasing the number of artificial fractures unilaterally could not achieve the expected increase in production.
基金Supported by the National Science and Technology Major Project(2016ZX05046-001-005)National Natural Science Foundation of China(41922015)。
文摘Based on the microscopic pore-throat characterization of typical continental tight reservoirs in China,such as sandstone of Cretaceous Qingshankou and Quantou formations in Songliao Basin,NE China sandy conglomerate of Baikouquan Formation in Mahu area and hybrid rock of Lucaogou Formation in Jimusaer sag of Junggar Basin,NE China the theoretical lower limit,oil accumulation lower limit,effective flow lower limit and the upper limit of tight oil reservoirs were defined by water film thickness method,oil bearing occurrence method,oil testing productivity method and mechanical balance method,respectively.Cluster analysis method was used to compare the differences in pore-throat structure of different tight reservoirs,determine the grading criterion of tight reservoirs,and analyze its correlation with the limit of reservoir formation.The results show that the boundary between tight reservoir and conventional reservoir corresponds to the upper limit of physical properties,the boundary of classⅡand classⅢtight reservoirs corresponds to the lower limit of effective flow,the boundary of classⅢand classⅣtight reservoirs corresponds to the lower limit of reservoir forming,and the theoretical lower limit of tight reservoir corresponds to the boundary between tight reservoir and non-reservoir.Finally,the application results of the grading evaluation criterion show that the tight oil productivity is highly controlled by the type of tight reservoir,and classⅠand classⅡtight reservoirs are the favorable sections for high production of tight oil.
基金Supported by the National Natural Science Foundation of China(41672118)Strategic Cooperation Science and Technology Project Between China University of Petroleum and Petro China(ZLZX2020-01-06)。
文摘Taking the tight oil of the Zhongnan sag in the Ordos Basin,Jimusar sag in the Junggar Basin and Qingxi sag in the Jiuquan Basin as study objects,based on field survey,dissection of tight oil reservoirs,sample test,modeling experiment and comprehensive analysis,this study reveals that the tight oil accumulates at start-up pressure,advances under differential pressure,diffuses at alternating fast and low speeds,charges in stepped large area and migrates rapidly through fractures,and enriches in dominant fractures and pores.The root cause of ladder-like charge is the multiple scales of pores.The widespread source rock with high hydrocarbon generation intensity is the material basis for tight oil enrichment;the dominant source reservoir assemblage is the basic unit for tight oil enrichment;fractures and beddings are conducive to local rapid migration of tight oil;fractures and pores work together to control the enrichment of tight oil.Two typical accumulation models of tight oil are established,namely"source reservoir in coexistence,four optimal factors controlling enrichment around central area,and large-scale continuous distribution"for a large freshwater lake clastic rock basin and"source reservoir integration,four optimal factors controlling enrichment,central area distribution,small in size but high in enrichment degree"for a small saline lake diamictite depression.
基金Supported by China National Science and Technology Major Project(2016ZX05023,2017ZX05013-005)
文摘To deal with the stress interference caused by simultaneous propagation of multiple fractures and the wettability reversal and physical property changes of the reservoir caused by fracturing fluid getting in during large-volume fracturing of tight oil reservoirs through a horizontal well, a non-planar 3D fracture growth model was built, wettability reversal characterizing parameters and change of relative permeability curve were introduced to correct the production prediction model of fractured horizontal well, a fracturing design optimization software(Fr Smart) by integrating geological and engineering data was developed, and a fracturing design optimization approach for tight oil reservoirs based on fracture control was worked out. The adaptability of the method was analyzed and the fracture parameters of horizontal wells in tight oil reservoirs were optimized. The simulation results show that fracturing technology based on fracture control is suitable for tight oil reservoirs, and by optimizing fracture parameters, this technology makes it possible to produce the maximum amount of reserves in the well-controlled unit of unconventional reservoirs. The key points of fracturing design optimization based on fracture control include increasing lateral length of and reducing the row spacing between horizontal wells, increasing perforation clusters in one stage to decrease the spacing of neighboring fractures, and also avoiding interference of old and new fracturing wells. Field tests show that this technology can increase single well production and ultimate recovery. Using this technology in developing unconventional resources such as tight oil reservoirs in China will enhance the economics significantly.
