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Determination the Hydrogen Stored in Carbon Nanotubes by NO Titration Method
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作者 Shui Hua TANG Li Zhen GAO +4 位作者 Bao Chun LIU He LI Bo Lan ZHANG Liang Fu ZHANG Zuo Long YU 《Chinese Chemical Letters》 SCIE CAS CSCD 2001年第11期1015-1018,共4页
A novel method was established to determine the H2-storage capacity in carbon nanotubes. According to 2NO+2H2 (or 4H) = N2+2H2O reaction, the H2-storage capacity in carbon nanotubes could be calculated. The H2-storage... A novel method was established to determine the H2-storage capacity in carbon nanotubes. According to 2NO+2H2 (or 4H) = N2+2H2O reaction, the H2-storage capacity in carbon nanotubes could be calculated. The H2-storage capacity in carbon nanotubes is at least 2.89 wt%. 展开更多
关键词 NO titration HYDROGEN STORAGE carbon nanotubes.
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Studies on Determination of Ge in Au Alloys by Potassium Iodate Potentiometric Titration Method
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作者 ZHU Liya ZHOU Yu +8 位作者 TAN Yanshan LIU Wen LI Yong HAN Shouli TAN Wenjin HE Xiaotan WU Xilong XIE Hongchao CHEN Liangwei 《贵金属》 CAS CSCD 北大核心 2012年第A01期298-304,共7页
The paper presents a new method of determining Ge in gold alloys by potassium iodate potentiometric titration rather than by traditional distillation separation. The influences of conditions such as the reduction acid... The paper presents a new method of determining Ge in gold alloys by potassium iodate potentiometric titration rather than by traditional distillation separation. The influences of conditions such as the reduction acidity, dosage of sodium hypophosphite and reduction time on the determination of Ge were studied. Comparison was made between the influences of end-point indication for potential method and starch method on accruracy and precision of the analysed results, stability and sensitivity of end-point, selectivity of method and so on. The possibility of reaction in an electrochemical way was discussed. Ge in the alloys such as AuGe 12 , AuGeNi 12 2 , AuAgGe 18.8 12.5 and AuAgGeNi 43.8 6 0.2 was measured, respectively, with the relative standard deviation of 0.10%~0.31% and the recoveries of added standard Ge in sample of 99.40%~100.40% when the reduction acidity was 0.40~0.80 mol/L HCl and 3.3 mol/L H 3 PO 4, 15 g sodium hypophosphite and reduction time 40 min. The new method presented is high accuracy and precision in results, good stability and sensibility in end point, easy operation and strong selectivity of determination. When it is applied to analyse actual samples, satisfactory results are achieved. 展开更多
关键词 analytical chemistry GERMANIUM gold alloy potentiometric titration
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Determination of Formation Constants of Co^2+,Ni^2+,Cu^2+and Zn^2+ Complexes with Humic and Fulvic Acids by Potentionmetric Titration Method 被引量:1
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作者 DUJIN-ZHOU LUCHANG-QING 《Pedosphere》 SCIE CAS CSCD 1994年第4期289-296,共8页
The formation constants of Co^2+,Ni^2+,Cu^2+ and Zn^2+ complexes with humic acid(HA) and fulvic acid(FA) in red soil wrer determined by the potentiometric titration method.The constants as a function of composition of... The formation constants of Co^2+,Ni^2+,Cu^2+ and Zn^2+ complexes with humic acid(HA) and fulvic acid(FA) in red soil wrer determined by the potentiometric titration method.The constants as a function of composition of the complexation solutions were obtained by two graphical approaches respetively,The formation constants decreased with increasing concentration of metal in the solution,The results provide unambiguous evidence for the heterogeneity of the function groups of humic substances,the formation constants of FA were much smaller than those of HA,and the formation constants of Cu^2+ were much greater than those of Co^2+ ,Ni^2+ and Zn^2+,The potentiometric titration methon for determining formation constants are also discussed in the article. 展开更多
关键词 电位滴定法 红壤 钴配合物 镍配合物 铜配合物 锌配合物 腐植酸 灰黄霉酸 反应常数 测定
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QUANTITATIVE ANALYSIS OF VERY WEAK ACID AND BASE BY pH-FIXED TITRATION METHOD
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作者 Gang XU Ping WEI Yu Cheng XIE Xing Dong YU(Jiangsu Institute of Chemical Technology,Changzhou,213016) 《Chinese Chemical Letters》 SCIE CAS CSCD 1990年第1期81-84,共4页
pH-fixed titration method for the determination of weak acids andbases has been studied in this paper.It is not necessary to know theionization constant of weak acid or base and the concentration of titrant.This metho... pH-fixed titration method for the determination of weak acids andbases has been studied in this paper.It is not necessary to know theionization constant of weak acid or base and the concentration of titrant.This method had been applied to determine phenol,4-aminoantipyrine andglycine,whose ionization constants range from 10<sup>-10</sup>to 10<sup>-12</sup>.Theresults were satisfactory. 展开更多
关键词 satisfactory CONSTANTS PHENOL titration ACID bases OVERCOME PHENOL IONIZATION GLYCINE
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Titration Method Validation of Live Vaccines against Infectious Bursal Disease
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作者 Fatima Tahiri Khadija Id Sidi Yahia +1 位作者 Benaissa Attrassi Driss Belghyti 《Journal of Life Sciences》 2013年第10期1084-1102,共19页
关键词 鸡传染性法氏囊病 滴定方法 活疫苗 验证 胚胎成纤维细胞 重复性和再现性 测试测量 控制试验
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Determination of Fructose and Glucose Contents in Honey by Liquid Chromatography-refractive Index Detection Method and Direct Titration Method 被引量:1
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作者 Xiaoya PU Xusheng DU +1 位作者 Bo LIU Hua ZHANG 《Agricultural Biotechnology》 CAS 2016年第2期31-33,共3页
In this study,fructose and glucose contents in honey were determined by liquid chromatography-refractive index detection method and alkaline copper tartrate solution-direct titration method.According to the results,th... In this study,fructose and glucose contents in honey were determined by liquid chromatography-refractive index detection method and alkaline copper tartrate solution-direct titration method.According to the results,there were great differences between determination results of reducing sugar contents by liquid chromatography-refractive index detection method and alkaline copper tartrate solution-direct titration method.Specifically,average determination results of reducing sugar contents by liquid chromatography-refractive index detection method were reduced by about 9.5% compared with alkaline copper tartrate solution-direct titration method.Subsequently,determination results of reducing sugar contents by two methods were compared and analyzed.Liquid chromatography-refractive index detection method was used to determine fructose and glucose monomers in honey,but alkaline copper tartrate solution-direct titration method was used to determine reducing sugar composition in honey,which might lead to significantly different results.Due to small sample size and limited conditions,the determination results were not necessarily representative.Bee product acquisition and processing enterprises and relevant departments should pay much attention on these issues and fully consider the current situation of grass-roots units to develop scientific,rigorous,simple,universal,convenient,low-cost and practicable standards,thus ensuring the safety and reliability of food quality. 展开更多
关键词 滴定法测定 葡萄糖含量 液相色谱 检测法 蜂蜜 果糖 折射率 还原糖含量
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A Review on Sources,Extractions and Analysis Methods of a Sustainable Biomaterial:Tannins
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作者 Antonio Pizzi Marie-Pierre Laborie Zeki Candan 《Journal of Renewable Materials》 EI CAS 2024年第3期397-425,共29页
Condensed and hydrolysable tannins are non-toxic natural polyphenols that are a commercial commodity industrialized for tanning hides to obtain leather and for a growing number of other industrial applications mainly ... Condensed and hydrolysable tannins are non-toxic natural polyphenols that are a commercial commodity industrialized for tanning hides to obtain leather and for a growing number of other industrial applications mainly to substitute petroleum-based products.They are a definite class of sustainable materials of the forestry industry.They have been in operation for hundreds of years to manufacture leather and now for a growing number of applications in a variety of other industries,such as wood adhesives,metal coating,pharmaceutical/medical applications and several others.This review presents the main sources,either already or potentially commercial of this forestry by-materials,their industrial and laboratory extraction systems,their systems of analysis with their advantages and drawbacks,be these methods so simple to even appear primitive but nonetheless of proven effectiveness,or very modern and instrumental.It constitutes a basic but essential summary of what is necessary to know of these sustainable materials.In doing so,the review highlights some of the main challenges that remain to be addressed to deliver the quality and economics of tannin supply necessary to fulfill the industrial production requirements for some materials-based uses. 展开更多
关键词 TANNINS FLAVONOIDS SOURCES extraction methods analysis methods
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Review of Collocation Methods and Applications in Solving Science and Engineering Problems
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作者 Weiwu Jiang Xiaowei Gao 《Computer Modeling in Engineering & Sciences》 SCIE EI 2024年第7期41-76,共36页
The collocation method is a widely used numerical method for science and engineering problems governed by partial differential equations.This paper provides a comprehensive review of collocation methods and their appl... The collocation method is a widely used numerical method for science and engineering problems governed by partial differential equations.This paper provides a comprehensive review of collocation methods and their applications,focused on elasticity,heat conduction,electromagnetic field analysis,and fluid dynamics.The merits of the collocation method can be attributed to the need for element mesh,simple implementation,high computational efficiency,and ease in handling irregular domain problems since the collocation method is a type of node-based numerical method.Beginning with the fundamental principles of the collocation method,the discretization process in the continuous domain is elucidated,and how the collocation method approximation solutions for solving differential equations are explained.Delving into the historical development of the collocation methods,their earliest applications and key milestones are traced,thereby demonstrating their evolution within the realm of numerical computation.The mathematical foundations of collocation methods,encompassing the selection of interpolation functions,definition of weighting functions,and derivation of integration rules,are examined in detail,emphasizing their significance in comprehending the method’s effectiveness and stability.At last,the practical application of the collocation methods in engineering contexts is emphasized,including heat conduction simulations,electromagnetic coupled field analysis,and fluid dynamics simulations.These specific case studies can underscore collocation method’s broad applicability and effectiveness in addressing complex engineering challenges.In conclusion,this paper puts forward the future development trend of the collocation method through rigorous analysis and discussion,thereby facilitating further advancements in research and practical applications within these fields. 展开更多
关键词 Collocation method meshless method discrete schemes for functions numerical calculation
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Stabilization With Prescribed Instant via Lyapunov Method
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作者 Jiyuan Kuang Yabin Gao +2 位作者 Yizhuo Sun Aohua Liu Jianxing Liu 《IEEE/CAA Journal of Automatica Sinica》 SCIE EI CSCD 2024年第2期557-559,共3页
Dear Editor,This letter presents a prescribed-instant stabilization approach to high-order integrator systems by the Lyapunov method. Under the presented controller, the settling time of controlled systems is independ... Dear Editor,This letter presents a prescribed-instant stabilization approach to high-order integrator systems by the Lyapunov method. Under the presented controller, the settling time of controlled systems is independent of the initial conditions and equals the prescribed time instant. 展开更多
关键词 method. PRESCRIBED INSTANT
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Implementation of a particle-in-cell method for the energy solver in 3D spherical geodynamic modeling
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作者 Hao Dong ZeBin Cao +4 位作者 LiJun Liu YanChong Li SanZhong Li LiMing Dai XinYu Li 《Earth and Planetary Physics》 EI CAS CSCD 2024年第3期549-563,共15页
The thermal evolution of the Earth’s interior and its dynamic effects are the focus of Earth sciences.However,the commonly adopted grid-based temperature solver is usually prone to numerical oscillations,especially i... The thermal evolution of the Earth’s interior and its dynamic effects are the focus of Earth sciences.However,the commonly adopted grid-based temperature solver is usually prone to numerical oscillations,especially in the presence of sharp thermal gradients,such as when modeling subducting slabs and rising plumes.This phenomenon prohibits the correct representation of thermal evolution and may cause incorrect implications of geodynamic processes.After examining several approaches for removing these numerical oscillations,we show that the Lagrangian method provides an ideal way to solve this problem.In this study,we propose a particle-in-cell method as a strategy for improving the solution to the energy equation and demonstrate its effectiveness in both one-dimensional and three-dimensional thermal problems,as well as in a global spherical simulation with data assimilation.We have implemented this method in the open-source finite-element code CitcomS,which features a spherical coordinate system,distributed memory parallel computing,and data assimilation algorithms. 展开更多
关键词 numerical oscillation overshooting and undershooting particle-in-cell method three-dimensional spherical geodynamic modeling energy solver finite element method
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An Evidence-Based CoCoSo Framework with Double Hierarchy Linguistic Data for Viable Selection of Hydrogen Storage Methods
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作者 Raghunathan Krishankumar Dhruva Sundararajan +1 位作者 K.S.Ravichandran Edmundas Kazimieras Zavadskas 《Computer Modeling in Engineering & Sciences》 SCIE EI 2024年第3期2845-2872,共28页
Hydrogen is the new age alternative energy source to combat energy demand and climate change.Storage of hydrogen is vital for a nation’s growth.Works of literature provide different methods for storing the produced h... Hydrogen is the new age alternative energy source to combat energy demand and climate change.Storage of hydrogen is vital for a nation’s growth.Works of literature provide different methods for storing the produced hydrogen,and the rational selection of a viable method is crucial for promoting sustainability and green practices.Typically,hydrogen storage is associated with diverse sustainable and circular economy(SCE)criteria.As a result,the authors consider the situation a multi-criteria decision-making(MCDM)problem.Studies infer that previous models for hydrogen storage method(HSM)selection(i)do not consider preferences in the natural language form;(ii)weights of experts are not methodically determined;(iii)hesitation of experts during criteria weight assessment is not effectively explored;and(iv)three-stage solution of a suitable selection of HSM is unexplored.Driven by these gaps,in this paper,authors put forward a new integrated framework,which considers double hierarchy linguistic information for rating,criteria importance through inter-criteria correlation(CRITIC)for expert weight calculation,evidence-based Bayesian method for criteria weight estimation,and combined compromise solution(CoCoSo)for ranking HSMs.The applicability of the developed framework is testified by using a case example of HSM selection in India.Sensitivity and comparative analysis reveal the merits and limitations of the developed framework. 展开更多
关键词 Hydrogen storage methods double hierarchy hesitant fuzzy linguistic term set evidence theory CoCoSo method sustainability circular economy
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A Hierarchical Method for Locating the Interferometric Fringes of Celestial Sources in the Visibility Data
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作者 Rong Ma Ruiqing Yan +7 位作者 Hanshuai Cui Xiaochun Cheng Jixia Li Fengquan Wu Zongyao Yin Hao Wang Wenyi Zeng Xianchuan Yu 《Research in Astronomy and Astrophysics》 SCIE CAS CSCD 2024年第3期110-128,共19页
In source detection in the Tianlai project,locating the interferometric fringe in visibility data accurately will influence downstream tasks drastically,such as physical parameter estimation and weak source exploratio... In source detection in the Tianlai project,locating the interferometric fringe in visibility data accurately will influence downstream tasks drastically,such as physical parameter estimation and weak source exploration.Considering that traditional locating methods are time-consuming and supervised methods require a great quantity of expensive labeled data,in this paper,we first investigate characteristics of interferometric fringes in the simulation and real scenario separately,and integrate an almost parameter-free unsupervised clustering method and seeding filling or eraser algorithm to propose a hierarchical plug and play method to improve location accuracy.Then,we apply our method to locate single and multiple sources’interferometric fringes in simulation data.Next,we apply our method to real data taken from the Tianlai radio telescope array.Finally,we compare with unsupervised methods that are state of the art.These results show that our method has robustness in different scenarios and can improve location measurement accuracy effectively. 展开更多
关键词 methods data analysis-techniques image processing-techniques INTERFEROMETRIC
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Nonlinear Flap-Wise Vibration Characteristics ofWind Turbine Blades Based onMulti-Scale AnalysisMethod
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作者 Qifa Lang Yuqiao Zheng +2 位作者 Tiancai Cui Chenglong Shi Heyu Zhang 《Energy Engineering》 EI 2024年第2期483-498,共16页
This work presents a novel approach to achieve nonlinear vibration response based on the Hamilton principle.We chose the 5-MW reference wind turbine which was established by the National Renewable Energy Laboratory(NR... This work presents a novel approach to achieve nonlinear vibration response based on the Hamilton principle.We chose the 5-MW reference wind turbine which was established by the National Renewable Energy Laboratory(NREL),to research the effects of the nonlinear flap-wise vibration characteristics.The turbine wheel is simplified by treating the blade of a wind turbine as an Euler-Bernoulli beam,and the nonlinear flap-wise vibration characteristics of the wind turbine blades are discussed based on the simplification first.Then,the blade’s large-deflection flap-wise vibration governing equation is established by considering the nonlinear term involving the centrifugal force.Lastly,it is truncated by the Galerkin method and analyzed semi-analytically using the multi-scale analysis method,and numerical simulations are carried out to compare the simulation results of finite elements with the numerical simulation results using Campbell diagram analysis of blade vibration.The results indicated that the rotational speed of the impeller has a significant impact on blade vibration.When the wheel speed of 12.1 rpm and excitation amplitude of 1.23 the maximum displacement amplitude of the blade has increased from 0.72 to 3.16.From the amplitude-frequency curve,it can be seen that the multi-peak characteristic of blade amplitude frequency is under centrifugal nonlinearity.Closed phase trajectories in blade nonlinear vibration,exhibiting periodic motion characteristics,are found through phase diagrams and Poincare section diagrams. 展开更多
关键词 Wind turbine blades nonlinear vibration Galerkin method multi-scales method
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Efficient method to calculate the eigenvalues of the Zakharov–Shabat system
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作者 崔世坤 王振 《Chinese Physics B》 SCIE EI CAS CSCD 2024年第1期243-249,共7页
A numerical method is proposed to calculate the eigenvalues of the Zakharov–Shabat system based on Chebyshev polynomials. A mapping in the form of tanh(ax) is constructed according to the asymptotic of the potential ... A numerical method is proposed to calculate the eigenvalues of the Zakharov–Shabat system based on Chebyshev polynomials. A mapping in the form of tanh(ax) is constructed according to the asymptotic of the potential function for the Zakharov–Shabat eigenvalue problem. The mapping can distribute Chebyshev nodes very well considering the gradient for the potential function. Using Chebyshev polynomials, tanh(ax) mapping, and Chebyshev nodes, the Zakharov–Shabat eigenvalue problem is transformed into a matrix eigenvalue problem. This method has good convergence for the Satsuma–Yajima potential and the convergence rate is faster than the Fourier collocation method. This method is not only suitable for simple potential functions but also converges quickly for a complex Y-shape potential. It can also be further extended to other linear eigenvalue problems. 展开更多
关键词 Zakharov–Shabat system EIGENVALUE numerical method Chebyshev polynomials
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Research into Applicability of Wöhler Curve Method for Low-Cycle Fatigue of Metallic Materials
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作者 Xiangqiao Yan 《Journal of Harbin Institute of Technology(New Series)》 CAS 2024年第2期22-37,共16页
Recently,a description on a practicability of the Wöhler Curve Method for low-cycle fatigue of metals was given by the author.By the description and the low cycle fatigue test data of 16 MnR steel,it is important... Recently,a description on a practicability of the Wöhler Curve Method for low-cycle fatigue of metals was given by the author.By the description and the low cycle fatigue test data of 16 MnR steel,it is important to show that,for low cycle fatigue of metals,such a way that a stress-based intensity parameter calculated by the linear-elastic analysis is taken to be a stress intensity parameter,S,to establish a relationship between the stress intensity parameter,S,and the fatigue life,N,is practicable.In this paper,many metallic materials from the literature are given to show that the Wöhler Curve Method is well suitable for low-cycle fatigue analysis of metals. 展开更多
关键词 low cycle fatigue Wöhler curve method coffin-manson curve method METALS
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Recommendation Method for Contrastive Enhancement of Neighborhood Information
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作者 Hairong Wang Beijing Zhou +1 位作者 Lisi Zhang He Ma 《Computers, Materials & Continua》 SCIE EI 2024年第1期453-472,共20页
Knowledge graph can assist in improving recommendation performance and is widely applied in various person-alized recommendation domains.However,existing knowledge-aware recommendation methods face challenges such as ... Knowledge graph can assist in improving recommendation performance and is widely applied in various person-alized recommendation domains.However,existing knowledge-aware recommendation methods face challenges such as weak user-item interaction supervisory signals and noise in the knowledge graph.To tackle these issues,this paper proposes a neighbor information contrast-enhanced recommendation method by adding subtle noise to construct contrast views and employing contrastive learning to strengthen supervisory signals and reduce knowledge noise.Specifically,first,this paper adopts heterogeneous propagation and knowledge-aware attention networks to obtain multi-order neighbor embedding of users and items,mining the high-order neighbor informa-tion of users and items.Next,in the neighbor information,this paper introduces weak noise following a uniform distribution to construct neighbor contrast views,effectively reducing the time overhead of view construction.This paper then performs contrastive learning between neighbor views to promote the uniformity of view information,adjusting the neighbor structure,and achieving the goal of reducing the knowledge noise in the knowledge graph.Finally,this paper introduces multi-task learning to mitigate the problem of weak supervisory signals.To validate the effectiveness of our method,experiments are conducted on theMovieLens-1M,MovieLens-20M,Book-Crossing,and Last-FM datasets.The results showthat compared to the best baselines,our method shows significant improvements in AUC and F1. 展开更多
关键词 Contrastive learning knowledge graph recommendation method
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Dynamic Coupling Analysis of Semisubmersible Platform Float-over Method for Docking Case
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作者 DING Hongyan QIN Licheng +2 位作者 ZHANG Puyang SONG Zhengrong XIE Weiwei 《Journal of Ocean University of China》 CAS CSCD 2024年第2期345-357,共13页
In this paper,the multi-body coupled dynamic characteristics of a semisubmersible platform and an HYSY 229 barge were investigated.First,coupled hydrodynamic analysis of the HYSY 229 barge and the semisubmersible plat... In this paper,the multi-body coupled dynamic characteristics of a semisubmersible platform and an HYSY 229 barge were investigated.First,coupled hydrodynamic analysis of the HYSY 229 barge and the semisubmersible platform was performed.Relevant hydrodynamic parameters were obtained using the retardation function method of three-dimensional frequency-domain potential flow theory.The results of the hydrodynamic analysis were highly consistent with the test findings,verifying the accuracy of the multifloating hydrodynamic coupling analysis,and key hydrodynamic parameters were solved for different water depths and the coupling effect.According to the obtained results,the hydrodynamic influence was the largest in shallow waters when the coupling effect was considered.Furthermore,the coupled motion equation combined with viscous damping,fender system,and mooring system was established,and the hydrodynamics,floating body motion,and dynamic response of the fender system were analyzed.Motion analysis revealed good agreement among the surge,sway,and yaw motions of the two floating bodies.However,when the wave period reached 10 s,the motion of the two floating bodies showed severe shock,and a relative motion was also observed.Therefore,excessive constraints should be added between the two floating bodies during construction to ensure construction safety.The numerical analysis and model test results of the semisubmersible platform and HYSY 229 barge at a water depth of 42 m and sea conditions of 0°,45°,and 90° were in good agreement,and the error was less than 5%.The maximum movement of the HYSY 229 barge reached 2.61 m in the sway direction,whereas that of the semisubmersible platform was 2.11 m.During construction,excessive constraints should be added between the two floating bodies to limit their relative movement and ensure construction safety. 展开更多
关键词 float-over method semisubmersible platform coupling hydrodynamic fender system time-domain analysis
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Comparison study on measurement of rail weld joint between inertial reference method and multi-point chord reference method
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作者 Yifan Shi Yuan Wang +1 位作者 Xiaozhou Liu Ping Wang 《Railway Sciences》 2024年第1期69-83,共15页
Purpose – Straightness measurement of rail weld joint is of essential importance to railway maintenance. Dueto the lack of efficient measurement equipment, there has been limited in-depth research on rail weld joint ... Purpose – Straightness measurement of rail weld joint is of essential importance to railway maintenance. Dueto the lack of efficient measurement equipment, there has been limited in-depth research on rail weld joint with a5-m wavelength range, leaving a significant knowledge gap in this field.Design/methodology/approach – In this study, the authors used the well-established inertial referencemethod (IR-method), and the state-of-the-art multi-point chord reference method (MCR-method). Two methodshave been applied in different types of rail straightness measurement trollies, respectively. These instrumentswere tested in a high-speed rail section within a certain region of China. The test results were ultimatelyvalidated through using traditional straightedge and feeler gauge methods as reference data to evaluate the railweld joint straightness within the 5-m wavelength range.Findings – The research reveals that IR-method and MCR-method produce reasonably similar measurementresults for wavelengths below 1 m. However, MCR-method outperforms IR-method in terms of accuracy forwavelengths exceeding 3 m. Furthermore, it was observed that IR-method, while operating at a slower speed,carries the risk of derailing and is incapable of detecting rail weld joints and low joints within the track.Originality/value – The research compare two methods’ measurement effects in a longer wavelength rangeand demonstrate the superiority of MCR-method. 展开更多
关键词 Rail weld joint Inertial reference method Short-wavelength irregularities Multi-point chord reference method 5-m wavelength range
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Simplified quantitative analysis method and its application in the insitu synthesized copper-based azide chips
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作者 Jie Ren Yunfeng Li +3 位作者 Mingyu Li Xingyu Wu Jiabao Wang Qingxuan Zeng 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2024年第2期309-316,共8页
Copper-based azide(Cu(N_(3))2 or CuN_(3),CA)chips synthesized by in-situ azide reaction and utilized in miniaturized explosive systems has become a hot research topic in recent years.However,the advantages of in-situ ... Copper-based azide(Cu(N_(3))2 or CuN_(3),CA)chips synthesized by in-situ azide reaction and utilized in miniaturized explosive systems has become a hot research topic in recent years.However,the advantages of in-situ synthesis method,including small size and low dosage,bring about difficulties in quantitative analysis and differences in ignition capabilities of CA chips.The aim of present work is to develop a simplified quantitative analysis method for accurate and safe analysis of components in CA chips to evaluate and investigate the corresponding ignition ability.In this work,Cu(N_(3))2 and CuN_(3)components in CA chips were separated through dissolution and distillation by utilizing the difference in solubility and corresponding content was obtained by measuring N_(3)-concentration through spectrophotometry.The spectrophotometry method was optimized by studying influencing factors and the recovery rate of different separation methods was studied,ensuring the accuracy and reproducibility of test results.The optimized method is linear in range from 1.0-25.0 mg/L,with a correlation coefficient R^(2)=0.9998,which meets the requirements of CA chips with a milligram-level content test.Compared with the existing ICP method,component analysis results of CA chips obtained by spectrophotometry are closer to real component content in samples and have satisfactory accuracy.Moreover,as its application in miniaturized explosive systems,the ignition ability of CA chips with different component contents for direct ink writing CL-20 and the corresponding mechanism was studied.This study provided a basis and idea for the design and performance evaluation of CA chips in miniaturized explosive systems. 展开更多
关键词 Copper-based azide chips SPECTROPHOTOMETRY Separation method Quantitative analysis Ignition ability
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Numerical Simulation of the Seismic Response of a Horizontal Storage Tank Based on a SPH-FEM Coupling Method
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作者 Peilei Yan Endong Guo +1 位作者 HouliWu Liangchao Zhang 《Computer Modeling in Engineering & Sciences》 SCIE EI 2024年第5期1655-1678,共24页
A coupled numerical calculation method combining smooth particle hydrodynamics(SPH)and the finite element method(FEM)was implemented to investigate the seismic response of horizontal storage tanks.Anumericalmodel of a... A coupled numerical calculation method combining smooth particle hydrodynamics(SPH)and the finite element method(FEM)was implemented to investigate the seismic response of horizontal storage tanks.Anumericalmodel of a horizontal storage tank featuring a free liquid surface under seismic action was constructed using the SPH–FEM coupling method.The stored liquid was discretized using SPH particles,while the tank and supports were discretized using the FEM.The interaction between the stored liquid and the tank was simulated by using the meshless particle contact method.Then,the numerical simulation results were compared and analyzed against seismic simulation shaking table test data to validate the method.Subsequently,a series of numerical models,considering different liquid storage volumes and seismic effects,were constructed to obtain time history data of base shear and top center displacement,which revealed the seismic performance of horizontal storage tanks.Numerical simulation results and experimental data showed good agreement,with an error rate of less than 18.85%.And this conformity signifies the rationality of the SPH-FEM coupling method.The base shear and top center displacement values obtained by the coupled SPH-FEM method were only 53.3% to 69.1% of those calculated by the equivalent mass method employed in the current code.As the stored liquid volume increased,the seismic response of the horizontal storage tank exhibited a gradual upward trend,with the seismic response increasing from 73% to 388% for every 35% increase in stored liquid volume.The maximum von Mises stress of the tank and the supports remained below the steel yield strength during the earthquake.The coupled SPH-FEM method holds certain advantages in studying the seismic problems of tanks with complex structural forms,particularly due to the representation of the flow field distribution during earthquakes by involving reservoir fluid participation. 展开更多
关键词 SPH-FEM coupling method horizontal storage tank seismic response SLOSHING
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