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Calibration curve and support vector regression methods applied for quantification of cement raw meal using laser-induced breakdown spectroscopy 被引量:1
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作者 贾军伟 付洪波 +3 位作者 侯宗余 王华东 倪志波 董凤忠 《Plasma Science and Technology》 SCIE EI CAS CSCD 2019年第3期23-30,共8页
Laser-induced breakdown spectroscopy(LIBS) is a qualitative and quantitative analytical technique with great potential in the cement industrial analysis. Calibration curve(CC) and support vector regression(SVR) method... Laser-induced breakdown spectroscopy(LIBS) is a qualitative and quantitative analytical technique with great potential in the cement industrial analysis. Calibration curve(CC) and support vector regression(SVR) methods coupled with LIBS technology were applied for the quantification of three types of cement raw meal samples to compare their analytical concentration range and the ability to reduce matrix effects, respectively. To reduce the effects of fluctuations of the pulse-to-pulse, the unstable ablation and improve the reproducibility, all of the analysis line intensities were normalized on a per-detector basis. The prediction results of the elements of interest in the three types of samples, Ca, Si, Fe, Al, Mg, Na, K and Ti, were compared with the results of the wet chemical analysis. The average relative error(ARE),relative standard deviation(RSD) and root mean squared error of prediction(RMSEP) were employed to investigate and evaluate the prediction accuracy and stability of the two prediction methods. The maximum average ARE of the CC and SVR methods is 34.62% instead of 6.13%,RSD is 40.89% instead of 7.60% and RMSEP is 1.34% instead of 0.43%. The results show that SVR method can accurately analyze samples within a wider concentration range and reduce the matrix effects, and LIBS coupled with it for a rapid, stable and accurate quantification of different types of cement raw meal samples is promising. 展开更多
关键词 cement RAW MEAL calibration curveS SVR LIBS
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Fitting Nonlinear Calibration Curves: No Models Perfect
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作者 Julia Martin Alberto Romero Gracia Agustín G. Asuero 《Journal of Analytical Sciences, Methods and Instrumentation》 2017年第1期1-17,共17页
The study of the calibration of a series of compounds of environmental concern (six perfluoroalkyl compounds (perfluorooctane sulfonic acid and five perfluoroalkyl carboxylic acids), three preservatives (methyl-, ethy... The study of the calibration of a series of compounds of environmental concern (six perfluoroalkyl compounds (perfluorooctane sulfonic acid and five perfluoroalkyl carboxylic acids), three preservatives (methyl-, ethyl- and propylparabens) and the brominated flame retardant hexabromocyclododecane) by LC-MS/MS has been carries out, with a view to their simultaneous determination in samples of environmental interest. In some cases nonlinear calibration curves are obtained, but restricting the concentration range a linear model may be used to fit the data. Residual analysis has been performed in order to verify which models fit the data better, opting for a compromise decision given the apparent complexity of residuals plots. As Box states there are no perfect models (but models that work better than others). 展开更多
关键词 calibration Non Linear calibration Residual Analysis Liquid Chromatography-Tandem Mass SPECTROMETRY Emerging POLLUTANTS
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Establishment of a calibration curve for an isocentric cobalt unit using Monte Carlo simulation
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作者 Seyed Milad Vahabi Mojtaba Shamsaie-Zafarghandi 《Nuclear Science and Techniques》 SCIE CAS CSCD 2017年第9期21-24,共4页
Measurement of dose distribution in patients during radiotherapy is impossible. The Monte Carlo simulation is an alternative method for dose calculations. In routine radiotherapy, the source-to-surface distance(SSD)me... Measurement of dose distribution in patients during radiotherapy is impossible. The Monte Carlo simulation is an alternative method for dose calculations. In routine radiotherapy, the source-to-surface distance(SSD)method is not practical for an isocentric unit because it requires numerous values of tissue–air ratios and inverse square law. Therefore, this method is time consuming. In this paper, the curves of relative depth doses were obtained for three different SSDs using the MCNP4C Monte Carlo simulation and approximated with a single curve called calibration curve. This curve was compared to the curve obtained by published data, differing in approximately 5% in the worst case. It was also observed that the obtained results were more accurate for distances between-5 and 10 cm from source-to-axis distance. 展开更多
关键词 校准曲线 蒙特卡罗模拟 蒙特卡洛模拟 单位 平方反比定律 剂量分布 放射治疗 剂量计算
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A Weakly-Supervised Crowd Density Estimation Method Based on Two-Stage Linear Feature Calibration
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作者 Yong-Chao Li Rui-Sheng Jia +1 位作者 Ying-Xiang Hu Hong-Mei Sun 《IEEE/CAA Journal of Automatica Sinica》 SCIE EI CSCD 2024年第4期965-981,共17页
In a crowd density estimation dataset,the annotation of crowd locations is an extremely laborious task,and they are not taken into the evaluation metrics.In this paper,we aim to reduce the annotation cost of crowd dat... In a crowd density estimation dataset,the annotation of crowd locations is an extremely laborious task,and they are not taken into the evaluation metrics.In this paper,we aim to reduce the annotation cost of crowd datasets,and propose a crowd density estimation method based on weakly-supervised learning,in the absence of crowd position supervision information,which directly reduces the number of crowds by using the number of pedestrians in the image as the supervised information.For this purpose,we design a new training method,which exploits the correlation between global and local image features by incremental learning to train the network.Specifically,we design a parent-child network(PC-Net)focusing on the global and local image respectively,and propose a linear feature calibration structure to train the PC-Net simultaneously,and the child network learns feature transfer factors and feature bias weights,and uses the transfer factors and bias weights to linearly feature calibrate the features extracted from the Parent network,to improve the convergence of the network by using local features hidden in the crowd images.In addition,we use the pyramid vision transformer as the backbone of the PC-Net to extract crowd features at different levels,and design a global-local feature loss function(L2).We combine it with a crowd counting loss(LC)to enhance the sensitivity of the network to crowd features during the training process,which effectively improves the accuracy of crowd density estimation.The experimental results show that the PC-Net significantly reduces the gap between fullysupervised and weakly-supervised crowd density estimation,and outperforms the comparison methods on five datasets of Shanghai Tech Part A,ShanghaiTech Part B,UCF_CC_50,UCF_QNRF and JHU-CROWD++. 展开更多
关键词 Crowd density estimation linear feature calibration vision transformer weakly-supervision learning
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Method for determining the position of landslide slip-surface with a typical inclinometric curves
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作者 CHEN Hao WU Hong-gang 《Journal of Mountain Science》 SCIE CSCD 2024年第2期413-432,共20页
In the actual monitoring of deep hole displacement,the identification of slip surfaces is primarily based on abrupt changes observed in the inclinometric curve.In conventional identification methods,inclinometric curv... In the actual monitoring of deep hole displacement,the identification of slip surfaces is primarily based on abrupt changes observed in the inclinometric curve.In conventional identification methods,inclinometric curves exhibiting indications of sliding can be categorized into three types:B-type,D-type,and r-type.The position of the slip surface is typically determined by identifying the depth corresponding to the point of maximum displacement mutation.However,this method is sensitive to the interval of measurement points and the observation scale of the coordinate axes and suffers from unclear sliding surfaces and uncertain values.Based on the variation characteristics of these diagonal curves,we classified the landslide into three components:the sliding body,the sliding interval,and the immobile body.Moreover,three different generalization models were established to analyze the relationships between the curve form and the slip surface location based on different physical indicators such as displacement rate,relative displacement,and acceleration.The results show that the displacement rate curves of an r-type slope exhibit a clustering feature in the sliding interval,and by solving for the depth of discrete points within the step phase,it is possible to determine the location of the slip surface.On the other hand,D-type slopes have inflection points in the relative displacement curve located at the slip surface.The acceleration curves of B-type slopes exhibit clustering characteristics during the sliding interval,while the scattered acceleration data demonstrate wandering characteristics.Consequently,the slip surface location can be revealed by solving the depth corresponding to the maximum acceleration with cubic spline interpolation.The approach proposed in this paper was applied to the monitoring data of a landslide in Yunnan Province,China.The results indicate that our approach can accurately identify the slip surface location and enable computability of its position,thereby enhancing applicability and reliability of the deep-hole displacement monitoring data. 展开更多
关键词 Inclinometric curve Slip-surface position Displacement rate Relative displacement Acceleration
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A comparative study of data-driven battery capacity estimation based on partial charging curves
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作者 Chuanping Lin Jun Xu +5 位作者 Delong Jiang Jiayang Hou Ying Liang Xianggong Zhang Enhu Li Xuesong Mei 《Journal of Energy Chemistry》 SCIE EI CAS CSCD 2024年第1期409-420,I0010,共13页
With its generality and practicality, the combination of partial charging curves and machine learning(ML) for battery capacity estimation has attracted widespread attention. However, a clear classification,fair compar... With its generality and practicality, the combination of partial charging curves and machine learning(ML) for battery capacity estimation has attracted widespread attention. However, a clear classification,fair comparison, and performance rationalization of these methods are lacking, due to the scattered existing studies. To address these issues, we develop 20 capacity estimation methods from three perspectives:charging sequence construction, input forms, and ML models. 22,582 charging curves are generated from 44 cells with different battery chemistry and operating conditions to validate the performance. Through comprehensive and unbiased comparison, the long short-term memory(LSTM) based neural network exhibits the best accuracy and robustness. Across all 6503 tested samples, the mean absolute percentage error(MAPE) for capacity estimation using LSTM is 0.61%, with a maximum error of only 3.94%. Even with the addition of 3 m V voltage noise or the extension of sampling intervals to 60 s, the average MAPE remains below 2%. Furthermore, the charging sequences are provided with physical explanations related to battery degradation to enhance confidence in their application. Recommendations for using other competitive methods are also presented. This work provides valuable insights and guidance for estimating battery capacity based on partial charging curves. 展开更多
关键词 Lithium-ion battery Partial charging curves Capacity estimation DATA-DRIVEN Sampling frequency
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Effective dynamics for a spin-1/2 particle constrained to a curved layer with inhomogeneous thickness
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作者 梁国华 尹佩林 《Chinese Physics B》 SCIE EI CAS CSCD 2024年第2期78-83,共6页
We derive an effective Hamiltonian for a spin-1/2 particle confined within a curved thin layer with non-uniform thickness using the confining potential approach.Our analysis reveals the presence of a pseudo-magnetic f... We derive an effective Hamiltonian for a spin-1/2 particle confined within a curved thin layer with non-uniform thickness using the confining potential approach.Our analysis reveals the presence of a pseudo-magnetic field and effective spin–orbit interaction(SOI)arising from the curvature,as well as an effective scalar potential resulting from variations in thickness.Importantly,we demonstrate that the physical effect of additional SOI from thickness fluctuations vanishes in low-dimensional systems,thus guaranteeing the robustness of spin interference measurements to thickness imperfection.Furthermore,we establish the applicability of the effective Hamiltonian in both symmetric and asymmetric confinement scenarios,which is crucial for its utilization in one-side etching systems. 展开更多
关键词 curved surface inhomogeneous thickness spin-1/2 particle effective Hamiltonian
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Analytical Determination of Size and Location of Roadside Horizontal Sightline Offsets for Compound Curves
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作者 Timur Mauga 《Journal of Transportation Technologies》 2024年第1期119-135,共17页
AASHTO’s guideline for geometric design of highways and similar guidelines require that roadside areas on the inside of horizontal curves be cleared of high objects to provide stopping sight distance. The guidelines ... AASHTO’s guideline for geometric design of highways and similar guidelines require that roadside areas on the inside of horizontal curves be cleared of high objects to provide stopping sight distance. The guidelines have analytical models for determining the extent of clearance, known as the horizontal sightline offset or clearance offset, for simple curves. Researchers in the past have developed analytical models for clearance offsets for spiraled and reverse curves. Very few researchers developed analytical models for available sight distances for compound curves. Still missing are models for horizontal sightline offsets and locations of the offsets for compound curves. The objective of this paper is to present development of analytical models and charts for determining horizontal sightline offsets and their locations for compound curves. The paper considers curves whose component arcs are individually shorter than stopping sight distance. The resulting models and the charts have been verified with accurate values determined using graphical methods. The models and the charts will find application in geometric design of highway compound curves. 展开更多
关键词 Sight Distance Roadside Clearance Offsets Compound curves
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Parameter calibration of the tensile-shear interactive damage constitutive model for sandstone failure
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作者 Yun Shu Zheming Zhu +4 位作者 Meng Wang Weiting Gao Fei Wang Duanying Wan Yuntao Wang 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2024年第4期1153-1174,共22页
The tensile-shear interactive damage(TSID)model is a novel and powerful constitutive model for rock-like materials.This study proposes a methodology to calibrate the TSID model parameters to simulate sandstone.The bas... The tensile-shear interactive damage(TSID)model is a novel and powerful constitutive model for rock-like materials.This study proposes a methodology to calibrate the TSID model parameters to simulate sandstone.The basic parameters of sandstone are determined through a series of static and dynamic tests,including uniaxial compression,Brazilian disc,triaxial compression under varying confining pressures,hydrostatic compression,and dynamic compression and tensile tests with a split Hopkinson pressure bar.Based on the sandstone test results from this study and previous research,a step-by-step procedure for parameter calibration is outlined,which accounts for the categories of the strength surface,equation of state(EOS),strain rate effect,and damage.The calibrated parameters are verified through numerical tests that correspond to the experimental loading conditions.Consistency between numerical results and experimental data indicates the precision and reliability of the calibrated parameters.The methodology presented in this study is scientifically sound,straightforward,and essential for improving the TSID model.Furthermore,it has the potential to contribute to other rock constitutive models,particularly new user-defined models. 展开更多
关键词 Damage constitutive model Parameter calibration Rock modeling SANDSTONE Dynamic impact load Tensile-shear interactive damage(TSID)model
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Nonlinear dynamics of a circular curved cantilevered pipe conveying pulsating fluid based on the geometrically exact model
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作者 Runqing CAO Zilong GUO +2 位作者 Wei CHEN Huliang DAI Lin WANG 《Applied Mathematics and Mechanics(English Edition)》 SCIE EI CSCD 2024年第2期261-276,共16页
Due to the novel applications of flexible pipes conveying fluid in the field of soft robotics and biomedicine,the investigations on the mechanical responses of the pipes have attracted considerable attention.The fluid... Due to the novel applications of flexible pipes conveying fluid in the field of soft robotics and biomedicine,the investigations on the mechanical responses of the pipes have attracted considerable attention.The fluid-structure interaction(FSI)between the pipe with a curved shape and the time-varying internal fluid flow brings a great challenge to the revelation of the dynamical behaviors of flexible pipes,especially when the pipe is highly flexible and usually undergoes large deformations.In this work,the geometrically exact model(GEM)for a curved cantilevered pipe conveying pulsating fluid is developed based on the extended Hamilton's principle.The stability of the curved pipe with three different subtended angles is examined with the consideration of steady fluid flow.Specific attention is concentrated on the large-deformation resonance of circular pipes conveying pulsating fluid,which is often encountered in practical engineering.By constructing bifurcation diagrams,oscillating shapes,phase portraits,time traces,and Poincarémaps,the dynamic responses of the curved pipe under various system parameters are revealed.The mean flow velocity of the pulsating fluid is chosen to be either subcritical or supercritical.The numerical results show that the curved pipe conveying pulsating fluid can exhibit rich dynamical behaviors,including periodic and quasi-periodic motions.It is also found that the preferred instability type of a cantilevered curved pipe conveying steady fluid is mainly in the flutter of the second mode.For a moderate value of the mass ratio,however,a third-mode flutter may occur,which is quite different from that of a straight pipe system. 展开更多
关键词 curved pipe conveying fluid pulsating fluid geometrically exact model(GEM) nonlinear dynamics parametric vibration FLUTTER
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On the calibration of a shear stress criterion for rock joints to represent the full stress-strain profile
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作者 Akram Deiminiat Jonathan D.Aubertin Yannic Ethier 《Journal of Rock Mechanics and Geotechnical Engineering》 SCIE CSCD 2024年第2期379-392,共14页
Conventional numerical solutions developed to describe the geomechanical behavior of rock interfaces subjected to differential load emphasize peak and residual shear strengths.The detailed analysis of preand post-peak... Conventional numerical solutions developed to describe the geomechanical behavior of rock interfaces subjected to differential load emphasize peak and residual shear strengths.The detailed analysis of preand post-peak shear stress-displacement behavior is central to various time-dependent and dynamic rock mechanic problems such as rockbursts and structural instabilities in highly stressed conditions.The complete stress-displacement surface(CSDS)model was developed to describe analytically the pre-and post-peak behavior of rock interfaces under differential loads.Original formulations of the CSDS model required extensive curve-fitting iterations which limited its practical applicability and transparent integration into engineering tools.The present work proposes modifications to the CSDS model aimed at developing a comprehensive and modern calibration protocol to describe the complete shear stressdisplacement behavior of rock interfaces under differential loads.The proposed update to the CSDS model incorporates the concept of mobilized shear strength to enhance the post-peak formulations.Barton’s concepts of joint roughness coefficient(JRC)and joint compressive strength(JCS)are incorporated to facilitate empirical estimations for peak shear stress and normal closure relations.Triaxial/uniaxial compression test and direct shear test results are used to validate the updated model and exemplify the proposed calibration method.The results illustrate that the revised model successfully predicts the post-peak and complete axial stressestrain and shear stressedisplacement curves for rock joints. 展开更多
关键词 Full shear profile Post-peak shear behavior Rock joint Joint roughness coefficient(JRC) Axial stress-strain curve
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Resilient performance of self-centering hybrid rocking walls with curved interface under pseudo-static loading
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作者 Su Xing Yan Shi +1 位作者 Sun Xianglei Wang Tao 《Earthquake Engineering and Engineering Vibration》 SCIE EI CSCD 2024年第1期65-85,共21页
Frame and rocking wall(FRW)structures have excellent resilient performance during earthquakes.However,the concrete at interfacial corners of rocking walls(RWs)is easily crushed due to local extreme compression during ... Frame and rocking wall(FRW)structures have excellent resilient performance during earthquakes.However,the concrete at interfacial corners of rocking walls(RWs)is easily crushed due to local extreme compression during the rocking process.An innovative RW with a curved interface is proposed to prevent interfacial corners from producing local damage,enhancing its earthquake resilient performance(ERP).The precast wall panel with a curved interface is assembled into an integral self-centering hybrid rocking wall(SCRW)by two post-tensioned unbonded prestressed tendons.Moreover,two ordinary energy dissipation steel rebars and two shear reinforcements are arranged to increase the energy dissipation capacity and lateral resistance.Two SCRW specimens and one monolithic reinforced concrete(RC)shear wall(SW)were tested under pseudo-static loading to compare the ERPs of the proposed SCRW and the SW,focusing on studying the effect of the curved interface on the SCRW.The key resilient performance of rocking effects,failure modes,and hysteretic properties of the SCRW were explored.The results show that nonlinear deformations of the SCRW are concentrated along the interface between the SCRW and the foundation,avoiding damage within the SCRW.The restoring force provided by the prestressed tendons can effectively realize self-centering capacity with small residual deformation,and the resilient performance of the SCRW is better than that of monolithic SW.In addition,the curved interface of the SCRW makes the rocking center change and move inward,partially relieving the stress concentration and crush of concrete.The rocking range of the rocking center is about 41.4%of the width of the SCRW. 展开更多
关键词 self-centering hybrid rocking wall(SCRW) monolithic shear wall(SW) earthquake resilient performance(ERP) curved interface rocking center
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Dynamic and electrical responses of a curved sandwich beam with glass reinforced laminate layers and a pliable core in the presence of a piezoelectric layer under low-velocity impact
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作者 N.SHAHVEISI S.FELI 《Applied Mathematics and Mechanics(English Edition)》 SCIE EI CSCD 2024年第1期155-178,共24页
The dynamic responses and generated voltage in a curved sandwich beam with glass reinforced laminate(GRL)layers and a pliable core in the presence of a piezoelectric layer under low-velocity impact(LVI)are investigate... The dynamic responses and generated voltage in a curved sandwich beam with glass reinforced laminate(GRL)layers and a pliable core in the presence of a piezoelectric layer under low-velocity impact(LVI)are investigated.The current study aims to carry out a dynamic analysis on the sandwich beam when the impactor hits the top face sheet with an initial velocity.For the layer analysis,the high-order shear deformation theory(HSDT)and Frostig's second model for the displacement fields of the core layer are used.The classical non-adhesive elastic contact theory and Hunter's principle are used to calculate the dynamic responses in terms of time.In order to validate the analytical method,the outcomes of the current investigation are compared with those gained by the experimental tests carried out by other researchers for a rectangular composite plate subject to the LVI.Finite element(FE)simulations are conducted by means of the ABAQUS software.The effects of the parameters such as foam modulus,layer material,fiber angle,impactor mass,and its velocity on the generated voltage are reviewed. 展开更多
关键词 analytical model piezoelectric layer curved sandwich beam glass reinforced laminate(GRL) pliable core low-velocity impact(LVI) classical non-adhesive elastic contact theory
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A Review of the Key Points in the Design of Small-Radius Curved Ramp Bridges
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作者 Yuxiao Zhang 《Journal of World Architecture》 2024年第1期97-102,共6页
This article explores the fundamentals of small-radius curved ramp bridges.It covers the selection of box girder spans,support methods,and forms,along with design optimization techniques for this type of bridge struct... This article explores the fundamentals of small-radius curved ramp bridges.It covers the selection of box girder spans,support methods,and forms,along with design optimization techniques for this type of bridge structure.The purpose of this paper is to provide robust support for enhancing the design quality of these bridges and ensuring their efficacy in real-world applications. 展开更多
关键词 Bridge design Small-radius curve ramp Box girder span Support method Support form
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Abductive statistical methods improve the results of calibration curve bioassays:An example of determining zinc bioavailability in broiler chickens
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作者 Gene M.Pesti Lynne Billard +3 位作者 Shu-Biao Wu Robert A.Swick Thi Thanh Hoai Nguyen Natalie Morgan 《Animal Nutrition》 SCIE CSCD 2022年第3期294-304,共11页
In this paper,we discuss the theory behind calibration curve experiments and their application to a zinc(Zn)bioavailability study with broiler chickens.Seven replicates of 16 male commercial broiler chicks were fed st... In this paper,we discuss the theory behind calibration curve experiments and their application to a zinc(Zn)bioavailability study with broiler chickens.Seven replicates of 16 male commercial broiler chicks were fed starter diets for 14 days.Six diets had different levels of a potential Zn source and one was a positive control with standard industry levels of Zn for comparison.Four commonly used methods of calculating bioavailability means and confidence intervals(CI)from a calibration curve(standard curve)experiment to estimate the bioavailability of a new zinc source in broiler chickens were compared.The methods compared were the following:1)the Counter-Intuitive Method uses a multiple-range test to compare unknown test and standard samples;2)the Intuitive Method uses standard linear regression and inverts the equation to predict Zn bioavailability for each replicate of test samples;3)the Abductive Method uses Graybill's Equation,based on theory and observation,to estimate CI's;and 4)the Sophistic Method uses reverse regression,and calculates Zn bioavailability values directly from the equation.The Counter-Intuitive Method only gives information about which standards the test samples are,or are not,significantly different from respectively(average available Zn not predicted).The Intuitive Method ignores error about the standard curve and theoretically cannot estimate the CI directly(X±SEM=107.5±15.8 mg Zn/kg).The Sophistic Method underestimates and overestimates the test sample mean values above and below the mean of the standards,respectively(X=96.6 mg Zn/kg).The Abductive Method has an advantage over the other methods:The mean prediction estimation is consistent with theory(107.5±6.1 mg Zn/kg;X±SEM).When test or“unknown”samples are near the mean of the standard samples,the CI is smaller than when near the extremes of the calibration curve.When calibration curve error is small(R^(2)>approximately 0.95),there is little advantage to using the Abductive Method,but when calibration curve error is larger,as in many bioassays with growing animals,the Abductive Method improves the accuracy of the CI calculations.The Abductive Method was used to demonstrate the influence of the number of replicate samples on experimental power and cost. 展开更多
关键词 calibration curve Standard curve Confidence interval BIOAVAILABILITY
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Calibration Curve Establishment and Fractionation Temperature Selection of Polyethylene for Preparative Temperature Rising Elution Fractionation 被引量:1
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作者 Yan-hu Xue Shu-qin Bo 姬相玲 《Chinese Journal of Polymer Science》 SCIE CAS CSCD 2015年第7期1000-1008,共9页
A series of copolymers of ethylene with 1-hexene synthesized using a metallocene catalyst are selected and mixed. The blend is fractionated via preparative temperature rising elution fractionation(P-TREF). All fractio... A series of copolymers of ethylene with 1-hexene synthesized using a metallocene catalyst are selected and mixed. The blend is fractionated via preparative temperature rising elution fractionation(P-TREF). All fractions are characterized via high-temperature gel permeation chromatography(GPC), 13 C nuclear magnetic resonance spectroscopy(13C-NMR), and differential scanning calorimetry(DSC). The changes in the DSC melting peak temperatures of the fractions from P-TREF as a function of elution temperature are almost linear, thereby providing a reference through which the elution temperature of TREF experiments could be selected. Moreover, the standard calibration curve(ethylene/1-hexene) of P-TREF is established, which relates to the degree of short-chain branching of the fractions. The standard calibration curve of P-TREF is beneficial to study on the complicated branching structure of polyethylene. A convenient method for selecting the fractionation temperature for TREF experiments is elaborated. The polyethylene sample is fractionated via successive self-nucleation and annealing(SSA) thermal fractionation. A multiple-melting endotherm is obtained through the final DSC heating scan for the sample after SSA thermal fractionation. A series of fractionation temperatures are then selected through the relationship between the DSC melting peak temperature and TREF elution temperature. 展开更多
关键词 升温淋洗分级 温度选择 校准曲线 聚乙烯 制备型 洗脱 差示扫描量热 凝胶渗透色谱法
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保守开髓洞型及One Curve根管预备对下颌第一磨牙近中根管危险区的影响
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作者 史富茹 陈浩 +2 位作者 李霞 高瑞芳 李然 《口腔疾病防治》 2023年第7期480-487,共8页
目的研究使用One Curve预备系统时,保守开髓洞型对下颌第一磨牙近中根管危险区的侧穿风险的影响,为临床选择更优的髓腔入路提供依据。方法选择符合纳入标准的20颗因严重牙周病拔除冠根完整、近中根具有近颊根管与近舌根管2个独立根管,... 目的研究使用One Curve预备系统时,保守开髓洞型对下颌第一磨牙近中根管危险区的侧穿风险的影响,为临床选择更优的髓腔入路提供依据。方法选择符合纳入标准的20颗因严重牙周病拔除冠根完整、近中根具有近颊根管与近舌根管2个独立根管,弯曲度为0°~20°的下颌第一磨牙,根据髓腔通路设计随机分为2组:传统开髓洞型组与保守开髓洞型组。传统开髓洞型髓室顶完全去除,保守开髓洞型尽可能多地保留髓室顶及颈周牙本质,使用One Curve单支锉行根管预备。对预备前后的离体牙进行锥形束CT扫描,定位近中根根分叉下方0~7.0 mm位置,以1 mm为间隔确定测量截面。测量各截面中根管近远中侧最小根管壁厚度。结果①20颗下颌第一磨牙近中根预备前CT测量结果示:危险区位于根分叉下0~4 mm,近颊根管近中侧平均厚度为1.18 mm,远中侧为1.08 mm。近舌根管近中侧平均厚度为1.28 mm,远中侧为1.07 mm。②传统开髓洞型组与保守开髓洞型组的下颌第一磨牙的近中根管的危险区的根管壁厚度减少量比较无显著差异(t=1.319,P=0.19)。③传统开髓洞型的近颊根管根尖偏移更偏向近中,保守开髓洞型更趋向于远中侧。而两组在近舌根管的偏移趋势均偏向远中。结论使用One Curve预备系统时,临床上使用基于微创理念的保守开髓洞型不会增加下颌第一磨牙近中根管危险区的穿通风险。 展开更多
关键词 微创根管治疗 下颌第一磨牙 危险区 One curve 牙本质 锥形束CT 根管预备 根尖偏移
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Excitation curve calibration for the SSRF booster magnets and applications in the commissioning 被引量:1
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作者 HOU Jie SUN Xiaoying +3 位作者 CHEN Guangling ZHOU Xuemei LI Haohu LIU Guimin 《Nuclear Science and Techniques》 SCIE CAS CSCD 2008年第4期204-208,共5页
The Shanghai Synchrotron Radiation Facility (SSRF) is a low emittance third-generation synchrotron radiation light source under commissioning. The excitation curve calibration for the booster magnets is important to p... The Shanghai Synchrotron Radiation Facility (SSRF) is a low emittance third-generation synchrotron radiation light source under commissioning. The excitation curve calibration for the booster magnets is important to provide the magnet current configurations as reference. Calibration studies give the polynomial coefficients of each type of magnets and provide the magnet current configurations under different beam energies as beam is ramped at speed of 2 Hz. The applications of calibration in booster commissioning which show the accuracy of the magnetic excitation curve calibration are also discussed. 展开更多
关键词 加速器 核技术 磁铁 检测标准
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Calibration of the Infiltration Rate Curve from the LN Trend Line at Eight Sites of Interest, Based on Infiltration Tests Carried out
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作者 Victor Rogelio Tirado Picado 《Open Journal of Applied Sciences》 CAS 2022年第7期1098-1115,共18页
The purpose of this research is to demonstrate that a calibration curve can be obtained that can be used for any infiltration test, with the double ring method, as well as an equation that helps speed up data processi... The purpose of this research is to demonstrate that a calibration curve can be obtained that can be used for any infiltration test, with the double ring method, as well as an equation that helps speed up data processing. The experimentation was carried out in eight points in Nicaragua, of which five were distributed in Managua and three in Rivas-Nandaime. These results can be used for purposes of other studies of interest. As a result, a calibration curve is obtained, and an expression equal to  is deduced, which will be the equation to determine the average infiltration of a field test occupying the double ring, for a total of 7 hours. And it is from the result that the texture of the soil can be determined by means of the indicator table. The basic methodology allowed analyzing the data since they are obtained, processed and analyzed, resulting in the calibration curve for infiltration tests. Finally, an equation was determined from the averages of the processed data, resulting in a correlation of 0.9976, above 0.5, which means it is very high and reliable. 展开更多
关键词 Double Ring INFILTRATION calibration Logarithmic curve Data Adjustment
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Design and development of the deep-rock in-situ condition-preserved coring calibration platform 被引量:1
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作者 Yihang Li Heping Xie +8 位作者 Ru Zhang Zetian Zhang Zhilong Zhang Heng Gao Wei Huang Jixun Zhang Jiming Gao Xin Ma Ruibing Xu 《International Journal of Mining Science and Technology》 SCIE EI CAS CSCD 2023年第11期1377-1395,共19页
To systematically validate and calibrate the theory and technology of the deep in-situ conditionpreserved coring, the in-situ conditions at different depths should be simulated, and the full-size coring tests should b... To systematically validate and calibrate the theory and technology of the deep in-situ conditionpreserved coring, the in-situ conditions at different depths should be simulated, and the full-size coring tests should be carried out in this simulated environment. Therefore, a deep-rock in-situ conditionpreserved coring calibration platform was designed and developed. The self-tightening sealing structure and the quick-disassembly structure were designed on the basis of an innovative segmented nonuniformdiameter structure, which was a breakthrough from the traditional high-pressure vessel frame and was verified by finite element simulation and actual testing under extreme working conditions, respectively.To simulate the actual deep in-situ environment with a temperature of 150℃ and pressure of 140 MPa for a large Φ450 mm×H1400 mm core, temperature and pressure control systems were designed by coupling, and a pre-embedded high-pressure-resistant temperature sensor was designed. Finally, highprecision assembly automation, complex movement coordination of the coring device with the platform,and rotary dynamic sealing were achieved by utilizing the combination of adaptive cabin body servo control and an adaptive mechanical structure in a limited space, laying a solid foundation for the calibration of in-situ condition-preserved coring. 展开更多
关键词 In-situ condition-preserved coring calibration Deep Earth science Coring simulation Rotary dynamic seal
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