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Mid-Temperature Synthesis of CeO_2-TiO_2 Complex Compound and Its XRD Structure Study 被引量:1
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作者 陈林深 吕光烈 胡秀荣 《Journal of Rare Earths》 SCIE EI CAS CSCD 2003年第2期108-111,共4页
The CeTi 2O 6, which is formed above 1300 ℃ by ceramic method, was obtained at 700 ℃ using sol gel synthesis method. XRD analysis shows that there is 8% deficient of Ce in the structure. The chemical formula is C... The CeTi 2O 6, which is formed above 1300 ℃ by ceramic method, was obtained at 700 ℃ using sol gel synthesis method. XRD analysis shows that there is 8% deficient of Ce in the structure. The chemical formula is Ce 0.92 Ti 2O 5.84 , which has a monoclinic structure with space group of C 2/ m . Its cell parameters are a =0.9811(8) nm, b =0.3726(3) nm, c =0.6831(6) nm, and β =118.84°. After being treated at 1300 ℃ for 3 h, the system keeps stable but the deficient disappears, while the chemical formula change to the normal CeTi 2O 6, and the cell parameters are a =0.9813(3) nm, b =0.3752(4) nm, c =0.6883(5) nm, β =119.05°. The key to synthesis the precursors of CeTi 2O 6 is that Ti 4+ and Ce 3+ ions must reach the atomistic distributing state and prevent the oxidation of Ce 3+ during sol gel process. 展开更多
关键词 Semiconductor materials sol gel process CeO 2 TiO 2 complex compound XRD Rietveld analysis rare earths
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Intergranular Tunnelling and Field-Induced Percolation Fluctuation of Granular Composites (La1-zAgzMnO3)/(MnO2/Mn2O3)
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作者 张宁 包建春 +2 位作者 李刚 耿滔 陈继康 《Chinese Physics Letters》 SCIE CAS CSCD 2005年第11期2940-2943,共4页
We investigate the giant magnetoresistance of composites (La1-xAgzMnO3)1-υ(MnO2/Mn2O3)υ. The magnetoresistive property of the composites shows the characteristics of intergranular tunnelling. A conductivity leap... We investigate the giant magnetoresistance of composites (La1-xAgzMnO3)1-υ(MnO2/Mn2O3)υ. The magnetoresistive property of the composites shows the characteristics of intergranular tunnelling. A conductivity leap has been observed around y = 0.7. The composite (La0.926Ag0.074MnO3)0.698(MnO2/Mn2O3)0.302 has been found to show the greatest magnetoresistance in the samples. Its room-temperature MR ratio reaches 24% under a field of 1.8T. These phenomena suggest a percolation transformation and a kind of field-induced fluctuation in percolation in the samples investigated. 展开更多
关键词 GIANT NEGATIVE MAGNETORESISTANCE ELECTRICAL-TRANSPORT FILMS MANGANITE RESISTIVITY BEHAVIOR SYSTEM
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