[Objectives]This study was conducted to clarify the differences and abundance or deficiency of various elements in tobacco leaves from different positions of CB-1 in Zhangping City,so as to guide the production of pre...[Objectives]This study was conducted to clarify the differences and abundance or deficiency of various elements in tobacco leaves from different positions of CB-1 in Zhangping City,so as to guide the production of precision fertilization.[Methods]The element contents of CB-1 were determined by an X-ray fluorescence spectrometer.[Results]In terms of the contents of carbon,the upper leaves(45.73%)were significantly higher than the cutters(41.53%),and the lower leaves(43.15%)had no significant differences from both of them.For the content of oxygen element,there was no significant difference between the cutters(44.77%)and the lower leaves(43.40%),both of which were significantly higher than the upper leaves(40.75%).The contents of nitrogen,phosphorus,sulfur,boron and nickel all increased with the increase of the position,and they were significantly higher in the upper leaves than in the cutters and lower leaves.The contents of potassium,calcium,magnesium,chlorine and silicon all decreased with the increase of the position,and the lower leaves were significantly higher than the cutters and upper leaves.The contents of aluminum,titanium and chromium increased significantly with the increase of the position.The contents of strontium,zirconium and arsenic decreased significantly with the increase of the position.The element contents of tobacco leaves had significant or extremely significant differences between different parts of CB-1 in Zhangping City mostly.The contents of nitrogen,potassium,calcium,sulfur,chlorine,molybdenum and nickel in tobacco leaves were appropriate,and the contents of manganese and iron were too high,while the contents of phosphorus and copper were slightly low.The contents of magnesium,silicon,boron and sodium were too low.[Conclusions]This study can guide targeted fertilization and regulation of element contents in the tobacco leaves from different parts in production,and is of great significance to improving the production,quality and industrial availability of CB-1.展开更多
A molecularly imprinted polymer （MIP）, prepared around a cotinine template, has been synthesized. The feasibility of using the polymer for solid-phase extraction （SPE） of cotinine from biological samples has been ...A molecularly imprinted polymer （MIP）, prepared around a cotinine template, has been synthesized. The feasibility of using the polymer for solid-phase extraction （SPE） of cotinine from biological samples has been investigated. The results show that cotinine can be quantitatively retained and eluted from the polymer. Experiments with human urine samples indicate that clean target analyte is obtained for HPLC with UV detection using the protocol.展开更多
Macroporous polystyrene microsphere/graphene oxide（PS/GO） composite monolith was first prepared using Pickering emulsion droplets as the soft template. The Pickering emulsion was stabilized by PS/GO composite partic...Macroporous polystyrene microsphere/graphene oxide（PS/GO） composite monolith was first prepared using Pickering emulsion droplets as the soft template. The Pickering emulsion was stabilized by PS/GO composite particles in-situ formed in an acidic water phase. With the evaporation of water and the oil phase（octane）, the Pickering emulsion droplets agglomerated and combined with each other, forming a three-dimensional macroporous PS/GO composite matrix with excellent mechanical strength. The size of the macrospores ranged from 4 mm to 20 mm. The macroporous PS/GO composite monolith exhibited high adsorption capacity for tetracycline（TC） in an aqueous solution at p H 4–6. The maximum adsorption capacity reached 197.9 mg g 1at p H 6. The adsorption behaviour of TC fitted well with the Langmuir model and pseudo-second-order kinetic model. This work offers a simple and efficient approach to fabricate macroporous GO-based monolith with high strength and adsorption ability for organic pollutants.展开更多
基金Supported by Science and Technology Project of China Tobacco Hebei Industrial Co.Ltd.(2021130000300029).
文摘[Objectives]This study was conducted to clarify the differences and abundance or deficiency of various elements in tobacco leaves from different positions of CB-1 in Zhangping City,so as to guide the production of precision fertilization.[Methods]The element contents of CB-1 were determined by an X-ray fluorescence spectrometer.[Results]In terms of the contents of carbon,the upper leaves(45.73%)were significantly higher than the cutters(41.53%),and the lower leaves(43.15%)had no significant differences from both of them.For the content of oxygen element,there was no significant difference between the cutters(44.77%)and the lower leaves(43.40%),both of which were significantly higher than the upper leaves(40.75%).The contents of nitrogen,phosphorus,sulfur,boron and nickel all increased with the increase of the position,and they were significantly higher in the upper leaves than in the cutters and lower leaves.The contents of potassium,calcium,magnesium,chlorine and silicon all decreased with the increase of the position,and the lower leaves were significantly higher than the cutters and upper leaves.The contents of aluminum,titanium and chromium increased significantly with the increase of the position.The contents of strontium,zirconium and arsenic decreased significantly with the increase of the position.The element contents of tobacco leaves had significant or extremely significant differences between different parts of CB-1 in Zhangping City mostly.The contents of nitrogen,potassium,calcium,sulfur,chlorine,molybdenum and nickel in tobacco leaves were appropriate,and the contents of manganese and iron were too high,while the contents of phosphorus and copper were slightly low.The contents of magnesium,silicon,boron and sodium were too low.[Conclusions]This study can guide targeted fertilization and regulation of element contents in the tobacco leaves from different parts in production,and is of great significance to improving the production,quality and industrial availability of CB-1.
基金supported by the National Natural Science Foundation of China(No.20405013)the Scientific Foundation of State Tobacco Monopoly Administration of China(No.110200201017).
文摘A molecularly imprinted polymer （MIP）, prepared around a cotinine template, has been synthesized. The feasibility of using the polymer for solid-phase extraction （SPE） of cotinine from biological samples has been investigated. The results show that cotinine can be quantitatively retained and eluted from the polymer. Experiments with human urine samples indicate that clean target analyte is obtained for HPLC with UV detection using the protocol.
基金supported by the National Natural Science Foundation of China (Nos. 51073146, 51103143, 51173175, 51473152, and 51573174)the Fundamental Research Funds for the Central Universities (Nos. WK2060200012 and WK3450000001)the Foundation of Anhui Key Laboratory of Tobacco Chemistry (China Tobacco Anhui Industrial Co., Ltd.) (No. 2014126)
文摘Macroporous polystyrene microsphere/graphene oxide（PS/GO） composite monolith was first prepared using Pickering emulsion droplets as the soft template. The Pickering emulsion was stabilized by PS/GO composite particles in-situ formed in an acidic water phase. With the evaporation of water and the oil phase（octane）, the Pickering emulsion droplets agglomerated and combined with each other, forming a three-dimensional macroporous PS/GO composite matrix with excellent mechanical strength. The size of the macrospores ranged from 4 mm to 20 mm. The macroporous PS/GO composite monolith exhibited high adsorption capacity for tetracycline（TC） in an aqueous solution at p H 4–6. The maximum adsorption capacity reached 197.9 mg g 1at p H 6. The adsorption behaviour of TC fitted well with the Langmuir model and pseudo-second-order kinetic model. This work offers a simple and efficient approach to fabricate macroporous GO-based monolith with high strength and adsorption ability for organic pollutants.
