It has shown that altering crosslink density of biopolymers will regulate the morphology of Mesenchymal Stem Cells （MSCs） and the subsequent MSCs differentia- tion. These observations have been found in a wide range...It has shown that altering crosslink density of biopolymers will regulate the morphology of Mesenchymal Stem Cells （MSCs） and the subsequent MSCs differentia- tion. These observations have been found in a wide range of biopolymers. However, a recent work published in Nature Materials has revealed that MSCs morphology and differen- tiation was unaffected by crosslink density of polydimethyl- siloxane （PDMS）, which remains elusive. To understand such unusual behaviour, we use nanoindentation tests and modelling to characterize viscoelastic properties and sur- face adhesion of PDMS with different base：crosslink ratio varied from 50：1 （50D） to 10：1 （10D）. It has shown that lower crosslink density leads to lower elastic moduli. De- spite lower nanoindentation elastic moduli, PDMS with lowest crosslink density has higher local surface adhesion which would affect cell-biomaterials interactions. This work suggests that surface adhesion is likely another important physical cue to regulate cell-biomaterials interactions.展开更多
The sensitivity of magnetic Barkhausen noise (MBN) profile to changes in the excitation field strength and the number of turns of the detection coil was investigated in inhomogeneous material. Generally, the 0.5 mm ca...The sensitivity of magnetic Barkhausen noise (MBN) profile to changes in the excitation field strength and the number of turns of the detection coil was investigated in inhomogeneous material. Generally, the 0.5 mm case depth EN 36 steel specimen shows a double peak profile indicative of inhomogeneity through the detected depth the magnetized landscape. Various excitation field amplitudes were applied to the specimen and the induced MBN emission was analyzed for each magnetizing current. Excitation field at the lowest level induced an MBN emission of two peaks of equivalent heights. The first peak occurs at lower field than the second peak in the magnetization period. As the excitation field increased, the height of both peaks increased but the second peak increased in a higher rate than that of the first peak. Beyond certain excitation level, both peaks began to saturate and no increase in the MBN intensity was observed with increased excitation field strength. However, peak position and the number of Barkhausen events, indicated linearly as a function of the applied field strength. The experiment also establishes that the number of turns in the detection coil is important parameter which controls the height of the first peak. Low field peak height increases as the number of turn of the detection coil increases. The results indicate that the potential difference applied to the electromagnet and the sensitivity of the detection coil, determine the MBN profile characteristics.展开更多
In this article, the results obtained from a study on multilayer diamond-like carbon and boron nitride (DLC/BN) films are reported. The microstructure, atomic concentration, hardness and friction coefficient of the fi...In this article, the results obtained from a study on multilayer diamond-like carbon and boron nitride (DLC/BN) films are reported. The microstructure, atomic concentration, hardness and friction coefficient of the films were characterized using transmission electron microscopy, auger electron microscopy, nano-indentation measurements and ball-on-disk friction testing. The effects of bilayer thickness and substrate bias on film growth were investigated. All multilayer films showed alternate DLC and BN layers, except the 2- and 4-nm bilayer of multilayer DLC/BN films deposited without substrate bias. Although the layers were very thin, each layer was distinguishable. This was confirmed by the use of TEM imaging and AES measurements. The hardness values of all the multilayer films were lower than those measured for the monolayer DLC and BN films. However, the hardness can be altered with a change in the bilayer thickness. Furthermore, in the case of the films deposited with substrate bias, multilayer DLC/BN films showed an improvement in wear resistance compared to monolayer DLC and BN films. Thus, the deposition of multilayer DLC/BN films can be considered to be beneficial in prolonging the service life of the surface.展开更多
Existing Metal Additive Manufacturing processes are fast approaching a matured stage in which a wide range of possibilities are available for the incorporation of the rapid fabrication technology to current industrial...Existing Metal Additive Manufacturing processes are fast approaching a matured stage in which a wide range of possibilities are available for the incorporation of the rapid fabrication technology to current industrial practices. In terms of design conventions, the limitless geometrical freedom allows complex structures including cellular internal grids and lattices to be formed without additional tooling. Repair parts and leveraging components can also be produced on demand when required especially for military assets where large volume of inventory is constantly maintained to ensure operational readiness. In this exemplary work, a feasibility study on using stainless steel material with integrated cellular design to manufacture a guide bracket found on a military vehicle via Selective Laser Melting process was conducted. The results showed appreciably better mechanical performance in using a stainless steel honeycomb as compared to the aluminum alloy used for the original component together with a faster production route through SLM.展开更多
Residual stress continues to be important issues in shipbuilding. This paper demonstrates how the heat affected zone that results from welding could be identified nondestructively using MBN （magnetic Barkhausen noise...Residual stress continues to be important issues in shipbuilding. This paper demonstrates how the heat affected zone that results from welding could be identified nondestructively using MBN （magnetic Barkhausen noise） technique. A stress concentration region was created by placing a weld bead on a marine steel plate used in ship construction. MBN measurements were made on the back surface of the welded plate along the weld direction and perpendicular to it in a line that crosses the weld bead. The stress distribution as deduced from the MBN measurements was found to be anisotropic in the material of the heat affected zone. The heat induced anisotropy was completely eliminated by shot peening the HAZ material as revealed by MBN intensity. It was concluded that the directional MBN measurements could be used to characterize the induced anisotropy and hence assess the thermal residual stresses distribution near a localized stresses concentration regions imposed by welding.展开更多
A fully flexure micro/nano transmission platform(MNTP)which has five degrees of freedom is designed on the basis of bridge type amplification mechanism.According to the kinematic theory and the elastic beam theory,the...A fully flexure micro/nano transmission platform(MNTP)which has five degrees of freedom is designed on the basis of bridge type amplification mechanism.According to the kinematic theory and the elastic beam theory,the theoretical output displacement equation of the platform is derived,and then piezoelectric actuator(PZT)is calibrated.Meanwhile,a full closed-loop control strategy of the platform is established using the feedforward proportional-integral-derivative(PID)compound control algorithm based on the Preisach model.Moreover,the total transfer function of the micro positioning system is derived,and the calculation method of output signal is acquired.Finally,the theoretical output displacement is verified by finite element analysis(FEA)and positioning experiments.展开更多
Crosslinking treatment of collagen has often been used to improve the biological stability and mechanical properties of 3D porous collagen scaffolds. However, accompanying these improvements, the collagen fibril surfa...Crosslinking treatment of collagen has often been used to improve the biological stability and mechanical properties of 3D porous collagen scaffolds. However, accompanying these improvements, the collagen fibril surface becomes hydrophobic nature resulting in a reduced surface wettability. The wetting of the collagen fibril by culture medium is reduced and it is difficult for the medium to diffuse into the 3D structure of a porous collagen scaffold. This paper reports a ＂perfusion processing＂ strategy using ozone to improve the surface wettability of chemical crosslinked collagen scaffolds. Surface wettability, surface composition and biological stability were analyzed to evaluate the effectiveness of this surface processing strategy. It was observed that ozone perfusion processing improved surface wettability for both exterior and interior surfaces of the porous 3D collagen scaffold. The improvement in wettability is attributed to the incorporation of oxygen-containing functional groups onto the surface of the collagen fibrils, as confirmed by X-ray Photoelectron Spectroscopy （XPS） analysis. This leads to a significant improvement in water taking capability without compromising the bulk biological stability and mechanical properties, and confirms that ozone perfusion processing is an effective tool to modify the wettability both for interior and exterior surfaces throughout the scaffold.展开更多
Layer manufacture technologies are gaining increasing attention in the manufacturing for the production of polymer mould tooling. Layer manufacture techniques can be used in this potential manufacturing area to produc...Layer manufacture technologies are gaining increasing attention in the manufacturing for the production of polymer mould tooling. Layer manufacture techniques can be used in this potential manufacturing area to produce tooling either indirectly or directly, and powder metal based layer manufacture systems are considered as an effective way of producing rapid tooling. Mechanical properties and accuracy are critical for tooling. This paper reports the results of an experimental study examining the potential of layer manufacturing processes to deliver production tooling for polymer manufacture. A comparison between indirectly selective laser sintering and directly selective laser sintering to provide the tooling was reported. Three main areas were addressed during the study： mechanical strength, accuracy, and build rate. Overviews of the results from the studies were presented.展开更多
The micro-turbine is known as a producer of high-grade energy （work） and also low energy （heat）. The following low grade heat energy have been modeled under ISO ambient conditions （international standard organiza...The micro-turbine is known as a producer of high-grade energy （work） and also low energy （heat）. The following low grade heat energy have been modeled under ISO ambient conditions （international standard organization）, i.e. 15 ℃ and 1 bar, to utilize the waste heat energy of a 200 kW micro-turbine combined with a single effect absorption chiller, an organic ranking cycle using R245fa （ORC-R245 fa） as a working fluid, a multi-effect distillation desalination （MED） and a thermal vapor compression MED Desalination unit （TVC-MED）. The thermal comparison was carried out based on an energy and exergy analysis in terms of electric efficiency, exergetic efficiency, carbon footprint, and energy utilization factor （EUF）. The software package IPSEpro has been used to model and simulate the proposed power plants. As a result, utilizing the exhaust waste heat energy in single-effect absorption chillier has contributed to stabilize ambient temperature fluctuation, and gain the best exergetic efficiency of 39%, while the EUF has reached 72% and the carbon footprint was reduced by 75% in MED and TVC-MED Desalination respectively. The results also reveal that TVC-MED is more efficient than traditional MED as its gain output ratio （GOR） is improved by 5.5%. In addition, ORC-245fa generates an additional 20% of the micro-turbine electricity generation.展开更多
The characteristics of an organic Rankin cycle designed to operate with a low temperature geothermal source and constant temperature cooling water supplied from freshwater ponds typical to those found near Waddan City...The characteristics of an organic Rankin cycle designed to operate with a low temperature geothermal source and constant temperature cooling water supplied from freshwater ponds typical to those found near Waddan City in the Al Jufrah region of Libya were examined. Two working fluids were examined and it was concluded that the most suitable for this application was R-245fa. The off design performance of the organic Rankine cycle was examined and it was shown that the cycle is controlled by the performance of the condenser which is cooling water side temperature limited.展开更多
The paper presents an investigation of energy and exergy analysis of an existing ORC （organic rankine cycle） unit powered by hot geothermal water. The validated model of this unit was used to examine 25 refrigerants...The paper presents an investigation of energy and exergy analysis of an existing ORC （organic rankine cycle） unit powered by hot geothermal water. The validated model of this unit was used to examine 25 refrigerants belonging to different chemical compositions. The study revealed that R141b and R123 produced the best net power, energy efficiency, and exergy efficiency, whereas R125 was the lowest. Hydrofluorocarbons （except R143a）, hydrocarbons, and inorganic reflected attractive energy and exergy efficiencies. All investigated mixtures gained low performance compared with other studied candidates. The R245ca was the best among the hydrofluorocarbons studied refrigerants, and R501 was the best among the mixture refrigerants. Furthermore, within the ORC system, the evaporator was found to have the highest exergy destruction and the refrigerant pump was the lowest.展开更多
Bisphenol-A polycarbonate/dioctyl phthalate blend samples crystallized at a hydrostatic pressure were investigated by WAXD,DSC and SEM measurements.Some novel stereo-open spherulitic structures,i.e.,peony-,cabbage-,se...Bisphenol-A polycarbonate/dioctyl phthalate blend samples crystallized at a hydrostatic pressure were investigated by WAXD,DSC and SEM measurements.Some novel stereo-open spherulitic structures,i.e.,peony-,cabbage-,seaweed-,and lotus-like spherulites,were observed which belong to a three-dimensional structure and were only composed of crystalline region.The foleded-chain lamellar crystal was proved to be the sub-structure of these spherulites.This study also suggests a new route to grow such crystals so as to promote the understanding of the formation process and mechanism of polymer spherulites.展开更多
The interaction between the machining process and the machine tool （IMPMT） plays an important role on high precision components manufacturing. However, most researches are focused on the machining process or the mac...The interaction between the machining process and the machine tool （IMPMT） plays an important role on high precision components manufacturing. However, most researches are focused on the machining process or the machine tool separately, and the interaction between them has been always overlooked. In this paper, a novel simplified method is proposed to realize the simulation of IMPMT by combining use the finite element method and state space method. In this method, the transfer function of the machine tool is built as a small state space. The small state space is obtained from the complicated finite element model of the whole machine tool. Furthermore, the control system of the machine tool is integrated with the transfer function of the machine tool to generate the cutting trajectory. Then, the tool tip response under the cutting force is used to predict the machined surface. Finally, a case study is carried out for a fly-cutting machining process, the dynamic response analysis of an ultra-precision fly-cutting machine tool and the machined surface verifies the effectiveness of this method. This research proposes a simplified method to study the IMPMT, the relationships between the machining process and the machine tool are established and the surface generation is obtained.展开更多
Sizereduction systems have been extensively used in industry for many years. Nevertheless, reliable engi neering tools to be used to predict the comminution of particles are scarce. Computational fluid dynamics （CFD...Sizereduction systems have been extensively used in industry for many years. Nevertheless, reliable engi neering tools to be used to predict the comminution of particles are scarce. Computational fluid dynamics （CFD）discrete element model （DEM） numerical simulation may be used to predict such a complex phe nomenon and therefore establish a proper design and optimization model for comminution systems, They may also be used to predict attrition in systems where particle attrition is significant. Therefore, empirical comminution functions （which are applicable for any attrition/comminution process）, such as： strength distribution, selection, equivalence, breakage, and fatigue, have been integrated into the three dimensional CFDDEM simulation tool. The main drawback of such a design tool is the long computational time required owing to the large number of particles and the minute timestep required to maintain a steady solution while simulating the flow of particulate materials with very fine particles. The present study developed several methods to accelerate CFDDEM simulations： reducing the num ber of operations carried out at the singleparticle level, constructing a DEM grid detached from the CFD grid enabling a no binary search, generating a subgrid within the DEM grid to enable a no binary search for fine particles, and increasing the computational timestep and eliminating the finest particles in the simulation while still tracking their contribution to the process. The total speedup of the simulation process without the elimination of the finest particles was a factor of about 17. The elimination of the finest particles gave additional speedup of a factor of at least 18. Therefore, the simulation of a grinding process can run at least 300 times faster than the conventional method in which a standard no binary search is employed and the smallest particles are tracked.展开更多
The purpose of this study is two-fold： firstly, the development of a cheap, easy-to-construct and effective nanoparticle generator for testing nanoparticle sensors; secondly, the use of such a generator to test the e...The purpose of this study is two-fold： firstly, the development of a cheap, easy-to-construct and effective nanoparticle generator for testing nanoparticle sensors; secondly, the use of such a generator to test the effectiveness of a sensor device in trapping aerosolised nanoparticles. In this study, we have constructed an effective aerosol generator platform, based on aerosol-assisted chemical vapour deposition technology. Under well-controlled experimental conditions, this platform is capable of depositing aerosolised sodium chloride particles homogeneously on a substrate very effectively. Deposited aerosol droplets were subsequently dried and shown to form nanosized cubic crystals that are free from impurities. This platform was employed to test the effectiveness of a MEMS comb device in the electrostatic trapping of nanoparticles. Upon applying a DC bias （0.5 V） to the MEMS device, results showed an increase in nanoparticle deposition on the surface of the device, due to electrostatic precipitation. The presence of an electric field was shown to affect crystal formation upon drying of the aerosol droplets on the substrate; this caused a blotchy appearance on the SEM image, which was not observed in the absence of electric field.展开更多
基金funded by EPSRC–Newcastle University Sandpit Workshop Award
文摘It has shown that altering crosslink density of biopolymers will regulate the morphology of Mesenchymal Stem Cells （MSCs） and the subsequent MSCs differentia- tion. These observations have been found in a wide range of biopolymers. However, a recent work published in Nature Materials has revealed that MSCs morphology and differen- tiation was unaffected by crosslink density of polydimethyl- siloxane （PDMS）, which remains elusive. To understand such unusual behaviour, we use nanoindentation tests and modelling to characterize viscoelastic properties and sur- face adhesion of PDMS with different base：crosslink ratio varied from 50：1 （50D） to 10：1 （10D）. It has shown that lower crosslink density leads to lower elastic moduli. De- spite lower nanoindentation elastic moduli, PDMS with lowest crosslink density has higher local surface adhesion which would affect cell-biomaterials interactions. This work suggests that surface adhesion is likely another important physical cue to regulate cell-biomaterials interactions.
文摘The sensitivity of magnetic Barkhausen noise (MBN) profile to changes in the excitation field strength and the number of turns of the detection coil was investigated in inhomogeneous material. Generally, the 0.5 mm case depth EN 36 steel specimen shows a double peak profile indicative of inhomogeneity through the detected depth the magnetized landscape. Various excitation field amplitudes were applied to the specimen and the induced MBN emission was analyzed for each magnetizing current. Excitation field at the lowest level induced an MBN emission of two peaks of equivalent heights. The first peak occurs at lower field than the second peak in the magnetization period. As the excitation field increased, the height of both peaks increased but the second peak increased in a higher rate than that of the first peak. Beyond certain excitation level, both peaks began to saturate and no increase in the MBN intensity was observed with increased excitation field strength. However, peak position and the number of Barkhausen events, indicated linearly as a function of the applied field strength. The experiment also establishes that the number of turns in the detection coil is important parameter which controls the height of the first peak. Low field peak height increases as the number of turn of the detection coil increases. The results indicate that the potential difference applied to the electromagnet and the sensitivity of the detection coil, determine the MBN profile characteristics.
文摘In this article, the results obtained from a study on multilayer diamond-like carbon and boron nitride (DLC/BN) films are reported. The microstructure, atomic concentration, hardness and friction coefficient of the films were characterized using transmission electron microscopy, auger electron microscopy, nano-indentation measurements and ball-on-disk friction testing. The effects of bilayer thickness and substrate bias on film growth were investigated. All multilayer films showed alternate DLC and BN layers, except the 2- and 4-nm bilayer of multilayer DLC/BN films deposited without substrate bias. Although the layers were very thin, each layer was distinguishable. This was confirmed by the use of TEM imaging and AES measurements. The hardness values of all the multilayer films were lower than those measured for the monolayer DLC and BN films. However, the hardness can be altered with a change in the bilayer thickness. Furthermore, in the case of the films deposited with substrate bias, multilayer DLC/BN films showed an improvement in wear resistance compared to monolayer DLC and BN films. Thus, the deposition of multilayer DLC/BN films can be considered to be beneficial in prolonging the service life of the surface.
文摘Existing Metal Additive Manufacturing processes are fast approaching a matured stage in which a wide range of possibilities are available for the incorporation of the rapid fabrication technology to current industrial practices. In terms of design conventions, the limitless geometrical freedom allows complex structures including cellular internal grids and lattices to be formed without additional tooling. Repair parts and leveraging components can also be produced on demand when required especially for military assets where large volume of inventory is constantly maintained to ensure operational readiness. In this exemplary work, a feasibility study on using stainless steel material with integrated cellular design to manufacture a guide bracket found on a military vehicle via Selective Laser Melting process was conducted. The results showed appreciably better mechanical performance in using a stainless steel honeycomb as compared to the aluminum alloy used for the original component together with a faster production route through SLM.
文摘Residual stress continues to be important issues in shipbuilding. This paper demonstrates how the heat affected zone that results from welding could be identified nondestructively using MBN （magnetic Barkhausen noise） technique. A stress concentration region was created by placing a weld bead on a marine steel plate used in ship construction. MBN measurements were made on the back surface of the welded plate along the weld direction and perpendicular to it in a line that crosses the weld bead. The stress distribution as deduced from the MBN measurements was found to be anisotropic in the material of the heat affected zone. The heat induced anisotropy was completely eliminated by shot peening the HAZ material as revealed by MBN intensity. It was concluded that the directional MBN measurements could be used to characterize the induced anisotropy and hence assess the thermal residual stresses distribution near a localized stresses concentration regions imposed by welding.
基金Supported by the State Key Laboratory of Mechanical Transmission Independent Research Fund(SKLMT-ZZKT-2012 MS 05)
文摘A fully flexure micro/nano transmission platform(MNTP)which has five degrees of freedom is designed on the basis of bridge type amplification mechanism.According to the kinematic theory and the elastic beam theory,the theoretical output displacement equation of the platform is derived,and then piezoelectric actuator(PZT)is calibrated.Meanwhile,a full closed-loop control strategy of the platform is established using the feedforward proportional-integral-derivative(PID)compound control algorithm based on the Preisach model.Moreover,the total transfer function of the micro positioning system is derived,and the calculation method of output signal is acquired.Finally,the theoretical output displacement is verified by finite element analysis(FEA)and positioning experiments.
文摘Crosslinking treatment of collagen has often been used to improve the biological stability and mechanical properties of 3D porous collagen scaffolds. However, accompanying these improvements, the collagen fibril surface becomes hydrophobic nature resulting in a reduced surface wettability. The wetting of the collagen fibril by culture medium is reduced and it is difficult for the medium to diffuse into the 3D structure of a porous collagen scaffold. This paper reports a ＂perfusion processing＂ strategy using ozone to improve the surface wettability of chemical crosslinked collagen scaffolds. Surface wettability, surface composition and biological stability were analyzed to evaluate the effectiveness of this surface processing strategy. It was observed that ozone perfusion processing improved surface wettability for both exterior and interior surfaces of the porous 3D collagen scaffold. The improvement in wettability is attributed to the incorporation of oxygen-containing functional groups onto the surface of the collagen fibrils, as confirmed by X-ray Photoelectron Spectroscopy （XPS） analysis. This leads to a significant improvement in water taking capability without compromising the bulk biological stability and mechanical properties, and confirms that ozone perfusion processing is an effective tool to modify the wettability both for interior and exterior surfaces throughout the scaffold.
文摘Layer manufacture technologies are gaining increasing attention in the manufacturing for the production of polymer mould tooling. Layer manufacture techniques can be used in this potential manufacturing area to produce tooling either indirectly or directly, and powder metal based layer manufacture systems are considered as an effective way of producing rapid tooling. Mechanical properties and accuracy are critical for tooling. This paper reports the results of an experimental study examining the potential of layer manufacturing processes to deliver production tooling for polymer manufacture. A comparison between indirectly selective laser sintering and directly selective laser sintering to provide the tooling was reported. Three main areas were addressed during the study： mechanical strength, accuracy, and build rate. Overviews of the results from the studies were presented.
文摘The micro-turbine is known as a producer of high-grade energy （work） and also low energy （heat）. The following low grade heat energy have been modeled under ISO ambient conditions （international standard organization）, i.e. 15 ℃ and 1 bar, to utilize the waste heat energy of a 200 kW micro-turbine combined with a single effect absorption chiller, an organic ranking cycle using R245fa （ORC-R245 fa） as a working fluid, a multi-effect distillation desalination （MED） and a thermal vapor compression MED Desalination unit （TVC-MED）. The thermal comparison was carried out based on an energy and exergy analysis in terms of electric efficiency, exergetic efficiency, carbon footprint, and energy utilization factor （EUF）. The software package IPSEpro has been used to model and simulate the proposed power plants. As a result, utilizing the exhaust waste heat energy in single-effect absorption chillier has contributed to stabilize ambient temperature fluctuation, and gain the best exergetic efficiency of 39%, while the EUF has reached 72% and the carbon footprint was reduced by 75% in MED and TVC-MED Desalination respectively. The results also reveal that TVC-MED is more efficient than traditional MED as its gain output ratio （GOR） is improved by 5.5%. In addition, ORC-245fa generates an additional 20% of the micro-turbine electricity generation.
文摘The characteristics of an organic Rankin cycle designed to operate with a low temperature geothermal source and constant temperature cooling water supplied from freshwater ponds typical to those found near Waddan City in the Al Jufrah region of Libya were examined. Two working fluids were examined and it was concluded that the most suitable for this application was R-245fa. The off design performance of the organic Rankine cycle was examined and it was shown that the cycle is controlled by the performance of the condenser which is cooling water side temperature limited.
文摘The paper presents an investigation of energy and exergy analysis of an existing ORC （organic rankine cycle） unit powered by hot geothermal water. The validated model of this unit was used to examine 25 refrigerants belonging to different chemical compositions. The study revealed that R141b and R123 produced the best net power, energy efficiency, and exergy efficiency, whereas R125 was the lowest. Hydrofluorocarbons （except R143a）, hydrocarbons, and inorganic reflected attractive energy and exergy efficiencies. All investigated mixtures gained low performance compared with other studied candidates. The R245ca was the best among the hydrofluorocarbons studied refrigerants, and R501 was the best among the mixture refrigerants. Furthermore, within the ORC system, the evaporator was found to have the highest exergy destruction and the refrigerant pump was the lowest.
文摘Bisphenol-A polycarbonate/dioctyl phthalate blend samples crystallized at a hydrostatic pressure were investigated by WAXD,DSC and SEM measurements.Some novel stereo-open spherulitic structures,i.e.,peony-,cabbage-,seaweed-,and lotus-like spherulites,were observed which belong to a three-dimensional structure and were only composed of crystalline region.The foleded-chain lamellar crystal was proved to be the sub-structure of these spherulites.This study also suggests a new route to grow such crystals so as to promote the understanding of the formation process and mechanism of polymer spherulites.
基金Supported by National Natural Science Foundation of China(Grant No.51505107)Natural Scientific Research Innovation Foundation in Harbin Institute of Technology of China(Grant No.HIT.NSRIF.2017029)
文摘The interaction between the machining process and the machine tool （IMPMT） plays an important role on high precision components manufacturing. However, most researches are focused on the machining process or the machine tool separately, and the interaction between them has been always overlooked. In this paper, a novel simplified method is proposed to realize the simulation of IMPMT by combining use the finite element method and state space method. In this method, the transfer function of the machine tool is built as a small state space. The small state space is obtained from the complicated finite element model of the whole machine tool. Furthermore, the control system of the machine tool is integrated with the transfer function of the machine tool to generate the cutting trajectory. Then, the tool tip response under the cutting force is used to predict the machined surface. Finally, a case study is carried out for a fly-cutting machining process, the dynamic response analysis of an ultra-precision fly-cutting machine tool and the machined surface verifies the effectiveness of this method. This research proposes a simplified method to study the IMPMT, the relationships between the machining process and the machine tool are established and the surface generation is obtained.
文摘Sizereduction systems have been extensively used in industry for many years. Nevertheless, reliable engi neering tools to be used to predict the comminution of particles are scarce. Computational fluid dynamics （CFD）discrete element model （DEM） numerical simulation may be used to predict such a complex phe nomenon and therefore establish a proper design and optimization model for comminution systems, They may also be used to predict attrition in systems where particle attrition is significant. Therefore, empirical comminution functions （which are applicable for any attrition/comminution process）, such as： strength distribution, selection, equivalence, breakage, and fatigue, have been integrated into the three dimensional CFDDEM simulation tool. The main drawback of such a design tool is the long computational time required owing to the large number of particles and the minute timestep required to maintain a steady solution while simulating the flow of particulate materials with very fine particles. The present study developed several methods to accelerate CFDDEM simulations： reducing the num ber of operations carried out at the singleparticle level, constructing a DEM grid detached from the CFD grid enabling a no binary search, generating a subgrid within the DEM grid to enable a no binary search for fine particles, and increasing the computational timestep and eliminating the finest particles in the simulation while still tracking their contribution to the process. The total speedup of the simulation process without the elimination of the finest particles was a factor of about 17. The elimination of the finest particles gave additional speedup of a factor of at least 18. Therefore, the simulation of a grinding process can run at least 300 times faster than the conventional method in which a standard no binary search is employed and the smallest particles are tracked.
文摘The purpose of this study is two-fold： firstly, the development of a cheap, easy-to-construct and effective nanoparticle generator for testing nanoparticle sensors; secondly, the use of such a generator to test the effectiveness of a sensor device in trapping aerosolised nanoparticles. In this study, we have constructed an effective aerosol generator platform, based on aerosol-assisted chemical vapour deposition technology. Under well-controlled experimental conditions, this platform is capable of depositing aerosolised sodium chloride particles homogeneously on a substrate very effectively. Deposited aerosol droplets were subsequently dried and shown to form nanosized cubic crystals that are free from impurities. This platform was employed to test the effectiveness of a MEMS comb device in the electrostatic trapping of nanoparticles. Upon applying a DC bias （0.5 V） to the MEMS device, results showed an increase in nanoparticle deposition on the surface of the device, due to electrostatic precipitation. The presence of an electric field was shown to affect crystal formation upon drying of the aerosol droplets on the substrate; this caused a blotchy appearance on the SEM image, which was not observed in the absence of electric field.
