The error caused by irreversible demagnetization damages the accurate velocity tracking of an in-wheel motor in a mobile robot.A current feedforward vector control system based on ESO is proposed to compensate it for ...The error caused by irreversible demagnetization damages the accurate velocity tracking of an in-wheel motor in a mobile robot.A current feedforward vector control system based on ESO is proposed to compensate it for the demagnetization motor.A demagnetization mathematical model is established to describe a permanent magnet synchronous motor,which took the change of permanent magnet flux linkage parameters as a factor to count the demagnetization error in velocity tracking.The uncertain disturbance estimation model of the control system is built based on ESO,which eliminates the system error by the feedforward current compensation.It is compared with the vector control method in terms of control accuracy.The simulation results show that the current feedforward vector control method based on ESO reduces the velocity tracking error greatly in conditions of motor demagnetization less than 30%.It is effective to improve the operation accuracy of the mobile robot.展开更多
Bearing ring is the crucial component of bearing. With regard to such problems as material waste, low efficiency and high energy consumption in current process of producing large bearing ring, a new process named &quo...Bearing ring is the crucial component of bearing. With regard to such problems as material waste, low efficiency and high energy consumption in current process of producing large bearing ring, a new process named "casting-rolling compound forming technology" is researched by taking the typical 42CrMo slew bearing as object. Through theoretical analysis, the design criteria of the main casting-rolling forming parameters are put forward at first. Then the constitutive relationship model of as-cast 42CrMo steel and its mathematical model of dynamic recrystallization are obtained according to the results of the hot compression experiment. By a coupled thermal-mechanical finite element model for radial-axial rolling of bearing ring, the fraction of dynamic recrystallization is calculated and recrystallized grains size are predicated. Meanwhile, the effects of the initial rolling temperature and feed rate of idle roll on material microstructure evolution are analyzed. Finally, the industrial rolling experiment is designed and performed, based on the simulation results. In addition, mechanical and metallographic tests are conducted on rolled bearing ring to get the mechanical parameters and metallographic structure. The experimental data and results show that the mechanical properties of bearing ring produced by casting-rolling compound forming technology are up to industrial standard, and a qualified bearing ring can be successfully formed by employing this new technology. Through the study, a process of forming large bearing ring directly by using casting ring blank is obtained, which could provide an effective theoretical guidance for manufacturing large ring parts. It also has an edge in saving material, lowering energy and improving efficiency.展开更多
The effect of solution and aging treatments on microstructure and mechanical properties of warm-rolled 7075 alloy was investigated via optical microscope,electron backscattered diffraction,transmission electron micros...The effect of solution and aging treatments on microstructure and mechanical properties of warm-rolled 7075 alloy was investigated via optical microscope,electron backscattered diffraction,transmission electron microscopy and tensile tests.The 7075 alloy was subjected to solution treatments at 450℃for 1 h(ST1),490℃ for 1 h(ST2)and 1.5 h(ST3).Three aging routes were carried out on samples from ST2:one-step(A1),two-step(A2),and three-step aging(A3).The experimental results show mainly recrystallized equiaxed grains in ST1 and ST3 state but a combination of elongated and equiaxed grains in ST2 condition.Three aged alloys have similar microstructures of sample ST2 while the recrystallization frequency gets decreased after aging.The least recrystallization fraction occurs in A2 state.Three aged 7075 alloys all possess enhanced strength and plasticity.Precipitates characterization reveals the maximum strength is achieved in A2 sample as the matrix precipitates are composed mainly of smallηand manyη′phases.Aging route A2 appears preferable to other two aging conditions for attaining a pretty excellent combination of strength and plasticity.展开更多
Under the background of a transformation of the global energy structure,coal gasification technology has a wide application prospect,but its by-product,the coal gasification residue(CGR),is still not being efficiently...Under the background of a transformation of the global energy structure,coal gasification technology has a wide application prospect,but its by-product,the coal gasification residue(CGR),is still not being efficiently utilized for recycling.The CGR contains abundant carbon components,which could be applied to the microwave absorption field as the carbon matrix.In this study,Fe/CGR composites are fabricated via a two-step method,including the impregnation of Fe^(3+)and the reduction process.The influence of the different loading capacities of the Fe component on the morphology and electromagnetic properties is studied.Moreover,the loading content of Fe and the surface morphology of the Fe/CGR can be reasonably controlled by adjusting the concentration of the ferric nitrate solution.Meanwhile,Fe particles are evenly inserted on the CGR framework,which expands the Fe/CGR interfaces to enhance interfacial polarization,thus further improving the microwave-absorbing(MA)properties of composites.Particularly,as the Fe^(3+)concentration is 1.0 mol/L,the Fe/CGR composite exhibits outstanding performance.The reflection loss reaches-39.3 dB at 2.5 mm,and the absorption bandwidth covers 4.1 GHz at 1.5 mm.In this study,facile processability,resource recycling,appropriately matched impedance,and excellent MA performance are achieved.Finally,the Fe/CGR composites not only enhance the recycling of the CGR but also pioneer a new path for the synthesis of excellent absorbents.展开更多
In this paper,the main researches are focused on the horizontal nonlinear vibration characteristics of roll systems for rolling mill,mainly including the study of forced vibration and free vibration of the roller.Firs...In this paper,the main researches are focused on the horizontal nonlinear vibration characteristics of roll systems for rolling mill,mainly including the study of forced vibration and free vibration of the roller.Firstly,the nonlinear damping parameters and nonlinear stiffness parameters within interface of the rolling mill are both considered,and a fractional-order differential term is also introduced to model the horizontal nonlinear vibration.Secondly,the averaging method is introduced to solve the forced vibration system of the mill roll system,and the amplitude-frequency characteristic curves of the system are obtained for different orders,external excitation amplitudes,stiffness and fractional order coefficients.Thirdly,the amplitude-frequency and phasefrequency characteristics of the free vibration of the mill roll system are investigated at different fractional orders.Then,the accuracy of the averaging method for solving the dynamic characteristics of the system is verified by numerical analysis,and the effect of the fractional differential term coefficients and order on the dynamic characteristics of the roll system are investigated.Finally,the time-frequency characteristics and phase-frequency characteristics of free vibration systems at different fractional orders are studied.The validity of the theoretical study is also verified through experiments.展开更多
The continuously collected cores from the Permo-Carboniferous coal-bearing strata of the eastern Ordos Basin are essential for studying the hydrocarbon potential in this region.This study adopted sedimentological and ...The continuously collected cores from the Permo-Carboniferous coal-bearing strata of the eastern Ordos Basin are essential for studying the hydrocarbon potential in this region.This study adopted sedimentological and geochemical methods to analyze the sedimentary environment,material composition,and geochemical characteristics of the coal-bearing strata.The differences in depositional and paleoclimatic conditions were compared;and the factors influencing the organic matter content of fine-grained sediments were explored.The depositional environment of the Benxi and Jinci formations was lagoon to tidal flat with weakly reduced waters with low salinity and dry-hot paleoclimatic conditions;while that of the Taiyuan Formation was a carbonate platform and shallow water delta front,where the water was highly reductive.The xerothermic climate alternated with the warm and humid climate.The period of maximum transgression in the Permo-Carboniferous has the highest water salinity.The Shanxi Formation was deposited in a shallow water delta front with a brackish and fresh water environment and alternative weak reductiveness.And the paleoclimate condition is dry-hot.The TOC content in fine-grained samples was averaging 1.52%.The main controlling mechanism of organic matter in this area was the input conditions according to the analysis on input and preservation of organic matter.展开更多
Parameter calculation and result storage, as two necessary steps in phase-field simulation play an important role in ensuring the accuracy of simulation results. A strategy of parameter calculation and result storage ...Parameter calculation and result storage, as two necessary steps in phase-field simulation play an important role in ensuring the accuracy of simulation results. A strategy of parameter calculation and result storage is presented for phase-field simulation in α-Mg dendrite growth of Mg-5-wt% Zn alloy under isothermal solidification. Based on the phase diagram and empirical formulas, key parameters of the phase-field model, such as equilibrium partition coefficient k, liquidus slope m, solutal diffusion coefficient in liquid Dl, and solutal diffusion coefficient in solid Ds, can be obtained.Both structured grid method and structured point method can be used to store simulation results, but using the latter method will reduce about 60% storage space and 37.5% storage time compared with the former. Finally, convergent simulation results of α-Mg dendrite growth are obtained and they are in good agreement with the experimental results about optical micrograph, which verify the accuracy of parameters and stability of storage method.展开更多
The evolution of microstructure during hot deformation is key to achieving good mechanical properties in aluminum alloys.We have developed a cellular automaton(CA) based model to simulate the microstructural evolution...The evolution of microstructure during hot deformation is key to achieving good mechanical properties in aluminum alloys.We have developed a cellular automaton(CA) based model to simulate the microstructural evolution in 7075 aluminum alloy during hot deformation.Isothermal compression tests were conducted to obtain material parameters for 7075 aluminum alloy,leading to the establishment of models for dislocation density,nucleation of recrystallized grains,and grain growth.Integrating these aspects with grain topological deformation,our CA model effectively predicts flow stress,dynamic recrystallization(DRX) volume fraction,and average grain size under diverse deformation conditions.A systematic comparison was made between electron back scattered diffraction(EBSD) maps and CA model simulated under different deformation temperatures(573 to 723 K),strain rates(0.001 to 1 s^(-1)),and strain amounts(30% to 70%).These analyses indicate that large strain,high temperature,and low strain rate facilitate dynamic recrystallization and grain refinement.The results from the CA model show good accuracy and predictive capability,with experimental error within 10%.展开更多
Fe/N-based biomass porous carbon composite(Fe/N-p Carbon) was prepared by a facile high-temperature carbonization method from biomass,and the effect of Fe/N-p Carbon on the thermal decomposition of energetic molecular...Fe/N-based biomass porous carbon composite(Fe/N-p Carbon) was prepared by a facile high-temperature carbonization method from biomass,and the effect of Fe/N-p Carbon on the thermal decomposition of energetic molecular perovskite-based material DAP-4 was studied.Biomass porous carbonaceous materials was considered as the micro/nano support layers for in situ deposition of Fe/N precursors.Fe/Np Carbon was prepared simply by the high-temperature carbonization method.It was found that it showed the inherent catalysis properties for thermal decomposition of DAP-4.The heat release of DAP-4/Fe/N-p Carbon by DSC curves tested had increased slightly,compared from DAP-4/Fe/N-p Carbon-0.The decomposition temperature peak of DAP-4 at the presence of Fe/N-p Carbon had reduced by 79°C from384.4°C(pure DAP-4) to 305.4°C(DAP-4/Fe/N-p Carbon-3).The apparent activation energy of DAP-4thermal decomposition also had decreased by 29.1 J/mol.The possible catalytic decomposition mechanism of DAP-4 with Fe/N-p Carbon was proposed.展开更多
In the fiber winding process,strong disturbance,uncertainty,strong coupling,and fiber friction complicate the winding constant tension control.In order to effectively reduce the influence of these problems on the tens...In the fiber winding process,strong disturbance,uncertainty,strong coupling,and fiber friction complicate the winding constant tension control.In order to effectively reduce the influence of these problems on the tension output,this paper proposed a tension fluctuation rejection strategy based on feedforward compensation.In addition to the bias harmonic curve of the unknown state,the tension fluctuation also contains the influence of bounded noise.A tension fluctuation observer(TFO)is designed to cancel the uncertain periodic signal,in which the frequency generator is used to estimate the critical parameter information.Then,the fluctuation signal is reconstructed by a third-order auxiliary filter.The estimated signal feedforward compensates for the actual tension fluctuation.Furthermore,a time-varying parameters fractional-order PID controller(TPFOPID)is realized to attenuate the bounded noise in the fluctuation.Finally,TPFOPID is enhanced by TFO and applied to control a tension control system considering multi-source disturbances.The stability of the method is analyzed by using the Lyapunov theorem.Finally,numerical simulations verify that the proposed scheme improves the tracking ability and robustness of the system in response to tension fluctuations.展开更多
The large-scale multi-objective optimization algorithm(LSMOA),based on the grouping of decision variables,is an advanced method for handling high-dimensional decision variables.However,in practical problems,the intera...The large-scale multi-objective optimization algorithm(LSMOA),based on the grouping of decision variables,is an advanced method for handling high-dimensional decision variables.However,in practical problems,the interaction among decision variables is intricate,leading to large group sizes and suboptimal optimization effects;hence a large-scale multi-objective optimization algorithm based on weighted overlapping grouping of decision variables(MOEAWOD)is proposed in this paper.Initially,the decision variables are perturbed and categorized into convergence and diversity variables;subsequently,the convergence variables are subdivided into groups based on the interactions among different decision variables.If the size of a group surpasses the set threshold,that group undergoes a process of weighting and overlapping grouping.Specifically,the interaction strength is evaluated based on the interaction frequency and number of objectives among various decision variables.The decision variable with the highest interaction in the group is identified and disregarded,and the remaining variables are then reclassified into subgroups.Finally,the decision variable with the strongest interaction is added to each subgroup.MOEAWOD minimizes the interactivity between different groups and maximizes the interactivity of decision variables within groups,which contributed to the optimized direction of convergence and diversity exploration with different groups.MOEAWOD was subjected to testing on 18 benchmark large-scale optimization problems,and the experimental results demonstrate the effectiveness of our methods.Compared with the other algorithms,our method is still at an advantage.展开更多
Foot and root rot caused by Phytophthora parasitica is a substantial threat to citrus cultivation,affecting both yield and quality.Thus,rapid and accurate detection of P.parasitica plays an important role in disease m...Foot and root rot caused by Phytophthora parasitica is a substantial threat to citrus cultivation,affecting both yield and quality.Thus,rapid and accurate detection of P.parasitica plays an important role in disease management.The aim of this study was to develop a simple diagnostic method to detect P.parasitica infection by combining recombinase polymerase amplification and lateral flow strips(LF-RPA).To establish the LF-RPA assay of P.parasitica,the primers and probe designed based on the Ypt1 gene were tested for specificity to P.parasitica,which showed no cross-reactivity with DNAs of other related oomycete species.The LF-RPA assay detected the amount of genomic DNA of P.parasitica which was as low as 1 pg.To make the LF-RPA assay useful in low-resource settings,four simplified DNA extraction methods were compared,after which the LF-RPA assay was applied,with no specialized equipment,to analyze a diverse range of citrus tissues by using a simplified PEG-NaOH method for DNA extraction.This method was successful in detecting P.parasitica in infected plant samples within 30 min.Combining the LF-RPA assay and a simplified DNA extraction method could be a potential detection test for P.parasitica,especially in areas with limited resources.展开更多
The existing researches of hot ring rolling process are mainly based on forged billet. Compared with the existing process, the new ring casting-rolling compound forming process has significant advantages in saving mat...The existing researches of hot ring rolling process are mainly based on forged billet. Compared with the existing process, the new ring casting-rolling compound forming process has significant advantages in saving materials and energy, reducing emission and reducing the production cost. The microstructure evolution of the casting materials during hot deformation is the basis of the research of the new process. However, the researches on the casting materials are rare. The metadynamic recrystallization of the as-cast 42CrMo steel after normalizing and tempering during the hot compression is investigated. The tests are performed on the Gleeble-1500 thermal-mechanical simulator. The influence rule of the deformation parameters on the metadynamic recrystallization is obtained by analyzing the experimental data. The kinetic model of the metadynamic recrystallization is deduced. The analysis results show that the metadynamic recrystallization fraction increases with the increase of the deformation temperature and the strain rate. The metallographic experiments are used to investigate the influence rule of the deformation parameters on the grain size of the metadynamic recrystallization. The experimental results show that the grain of the metadynamic recrystallization could be refined with the increase of the strain rate and the decrease of the deformation temperature during hot compression. The occurrence of the metadynamic recrystallization during the hot deformation is more difficult in as-cast 42CrMo steel than in forged 42CrMo steel. The research can provide the foundation for the further research of the hot deformation behaviors of the as-cast structure and theoretical support for the new ring casting-rolling compound process.展开更多
A novel photocatalyst,bismuth oxychloride(BiOCl) micro-nano particles with a fine ferrite plate structure,was prepared by a low-cost,simple hydrolytic method.The as-prepared BiOCl was characterized by scanning electro...A novel photocatalyst,bismuth oxychloride(BiOCl) micro-nano particles with a fine ferrite plate structure,was prepared by a low-cost,simple hydrolytic method.The as-prepared BiOCl was characterized by scanning electron microscopy(SEM),thermogravimetric analysis-differential thermal analysis(TGA-DTA),X-ray diffraction(XRD),and UV-vis diffuse reflectance spectra(DRS).The effects of preparation conditions such as sodium dodecyl benzene sulfonate(SDBS) dispersant,HCl concentration,and heat treatment temperature on BiOCl performances were investigated.Moreover,its photocatalytic activity was evaluated on the degradation of methylene orange(MO) and was compared with that of TiO 2(P25).The experimental results confirmed that BiOCl micro-nano particles prepared with SDBS,the HCl concentration of 1.5 mol/L,and the heat treatment temperature of 80°C exhibited the best performance for the photodegradation of MO solution,and they showed good stability and better photocatalytic activity than P25 photocatalyst.展开更多
To understand the solidification behavior of austenitic stainless steel in pulsed magnetic field, the solidification process is investigated by means of the self-made high voltage pulse power source and the solidifica...To understand the solidification behavior of austenitic stainless steel in pulsed magnetic field, the solidification process is investigated by means of the self-made high voltage pulse power source and the solidification tester. The results show that the solidification structure of austenitic stainless steel can be remarkably refined in pulsed magnetic field, yet the grains become coarse again when the magnetic intensity is exceedingly large, indicating that an optimal intensity range existed for structure refinement. The solidification temperature can be enhanced with an increase in the magnetic intensity. The solidification time is shortened obviously, but the shortening degree is reduced with the increase of the magnetic intensity.展开更多
Hot deformation behaviors of TC11 alloy with β-annealed lamellar structure and forged equiaxed structure were investigated in the β field in the temperature range of 1 090-1 030 ℃ and strain rate of 0.001-0.1 s-1 b...Hot deformation behaviors of TC11 alloy with β-annealed lamellar structure and forged equiaxed structure were investigated in the β field in the temperature range of 1 090-1 030 ℃ and strain rate of 0.001-0.1 s-1 by means of isothermal compression tests.Hot deformation characteristics and microstructure evolutions of the two starting structures were analyzed.And hot processing power dissipation efficiency maps were established.EBSD technique was used for testing grain boundary characteristic of deformation structures.The results indicate that hot deformation mechanism of TC11 alloy in β field is dynamic recovery accompanied by geometric dynamic recrystallization at large strains,or discontinuous dynamic recrystallization based on the starting structure states and deformation parameters.Accordingly,there are two different grain refining patterns.One is characteristic of new fine grains in the interior of elongated prior β grains that have serrated grain boundaries; and the other is that of new fine grains along elongated prior β grain boundaries.展开更多
Two coordination polymers, namely {[Ni(cpna)(H2biim)(H2O)]·H2O}n(1) and {[Mn(cpna)(H2biim)]·H2O}n(2)(H2cpna = 5-(2'-carboxylphenyl) nicotic acid, H2biim = 2,2'-biimidazole),have been hydrothermally s...Two coordination polymers, namely {[Ni(cpna)(H2biim)(H2O)]·H2O}n(1) and {[Mn(cpna)(H2biim)]·H2O}n(2)(H2cpna = 5-(2'-carboxylphenyl) nicotic acid, H2biim = 2,2'-biimidazole),have been hydrothermally synthesized and characterized by elemental analysis, IR, TG, magnetic properties, and single-crystal X-ray diffraction. Compound 1 exhibits a one- dimensional(1D) step-like chain structure, which further builds a three-dimensional(3D) supramolecular architecture via O–H···O and N–H···O hydrogen-bonding and π-π stacking interactions. Compound 2 possesses a one-dimensional(1D) double chain structure, which is further assembled into a 3D supramolecular framework by N–H···O hydrogen bonding and π-π stacking interactions. Magnetic susceptibility measurement indicates that compound 1 shows a weak antiferromagnetic coupling between the nearest Ni(II) centers, with g = 2.11 and J = –1.87 cm–1.展开更多
Static load tests are an important means of supervising and detecting a crane's lift capacity. Due to space restrictions, however, there are difficulties and potential danger when testing large bridge cranes. To s...Static load tests are an important means of supervising and detecting a crane's lift capacity. Due to space restrictions, however, there are difficulties and potential danger when testing large bridge cranes. To solve the loading problems of large-tonnage cranes during testing, an equivalency test is proposed based on the similarity theory and BP neural networks. The maximum stress and displacement of a large bridge crane is tested in small loads, combined with the training neural network of a similar structure crane through stress and displacement data which is collected by a physics simulation progressively loaded to a static load test load within the material scope of work. The maximum stress and displacement of a crane under a static load test load can be predicted through the relationship of stress, displacement, and load. By measuring the stress and displacement of small tonnage weights, the stress and displacement of large loads can be predicted, such as the maximum load capacity, which is 1.25 times the rated capacity. Experimental study shows that the load reduction test method can reflect the lift capacity of large bridge cranes. The load shedding predictive analysis for Sanxia 1200 t bridge crane test data indicates that when the load is 1.25 times the rated lifting capacity, the predicted displacement and actual displacement error is zero. The method solves the problem that lifting capacities are difficult to obtain and testing accidents are easily possible when 1.25 times related weight loads are tested for large tonnage cranes.展开更多
In spline rolling process,the contact area between roller and workpiece plays an important role in calculating rolling-force and rolling-moment.For the purpose of studying the contact area, contact state between rolle...In spline rolling process,the contact area between roller and workpiece plays an important role in calculating rolling-force and rolling-moment.For the purpose of studying the contact area, contact state between roller and workpiece in process of spline cold rolling based upon cross rolling is analyzed.According to the suitable hypothesis,the mathematic model of roller-tooth-curve in optional position of rolling process is established.Combing the theory of conjugate curves with the theory of envelope curve,the corresponding mathematic model of workpiece-tooth-curve is established.By utilizing establishing mathematic models,the algorithm of entire contact area in rolling process is created.On the basis of the algorithm,calcuiation-prograrn is compiled under MATLAB program language environment.The calcuiation-program actualizes quantitative analysis and quantitative calculation of contact areas.Utilizing the calculation-program,the influence of parameters on contact area is analyzed,and the tendency is consistent with the manufacturing experience.In consideration of rolling-force optimization,the primary process parameters may be selected according to results of calculation.The result of the present study may provide basis for research on rolling-force and rolling-moment.展开更多
Research on compact manufacturing technology for shape and performance controllability of metallic components can realize the simplification and high-reliability of manufacturing process on the premise of satisfying t...Research on compact manufacturing technology for shape and performance controllability of metallic components can realize the simplification and high-reliability of manufacturing process on the premise of satisfying the requirement of macro/micro-structure. It is not only the key paths in improving performance, saving material and energy, and green manufacturing of components used in major equipments, but also the challenging subjects in frontiers of advanced plastic forming. To provide a novel horizon for the manufacturing in the critical components is significant. Focused on the high-performance large-scale components such as bearing rings, flanges, railway wheels, thick-walled pipes, etc, the conventional processes and their developing situations are summarized. The existing problems including multi-pass heating, wasting material and energy, high cost and high-emission are discussed, and the present study unable to meet the manufacturing in high-quality components is also pointed out. Thus, the new techniques related to casting-rolling compound precise forming of rings, compact manufacturing for duplex-metal composite rings, compact manufacturing for railway wheels, and casting-extruding continuous forming of thick-walled pipes are introduced in detail, respectively. The corresponding research contents, such as casting ring blank, hot ring rolling, near solid-state pressure forming, hot extruding, are elaborated. Some findings in through-thickness microstructure evolution and mechanical properties are also presented. The components produced by the new techniques are mainly characterized by fine and homogeneous grains. Moreover, the possible directions for further development of those techniques are suggested. Finally, the key scientific problems are first proposed. All of these results and conclusions have reference value and guiding significance for the integrated control of shape and performance in advanced compact manufacturing.展开更多
基金Sponsored by the National Natural Science Foundation of China(Grant No.51975396)the Natural Science Foundation of Shanxi Province(Grant No.202103021224264).
文摘The error caused by irreversible demagnetization damages the accurate velocity tracking of an in-wheel motor in a mobile robot.A current feedforward vector control system based on ESO is proposed to compensate it for the demagnetization motor.A demagnetization mathematical model is established to describe a permanent magnet synchronous motor,which took the change of permanent magnet flux linkage parameters as a factor to count the demagnetization error in velocity tracking.The uncertain disturbance estimation model of the control system is built based on ESO,which eliminates the system error by the feedforward current compensation.It is compared with the vector control method in terms of control accuracy.The simulation results show that the current feedforward vector control method based on ESO reduces the velocity tracking error greatly in conditions of motor demagnetization less than 30%.It is effective to improve the operation accuracy of the mobile robot.
基金supported by Key Program of National Natural Science Foundation of China(Grant No.51135007)National Natural Science Foundation of China(Grant No.51075290)
文摘Bearing ring is the crucial component of bearing. With regard to such problems as material waste, low efficiency and high energy consumption in current process of producing large bearing ring, a new process named "casting-rolling compound forming technology" is researched by taking the typical 42CrMo slew bearing as object. Through theoretical analysis, the design criteria of the main casting-rolling forming parameters are put forward at first. Then the constitutive relationship model of as-cast 42CrMo steel and its mathematical model of dynamic recrystallization are obtained according to the results of the hot compression experiment. By a coupled thermal-mechanical finite element model for radial-axial rolling of bearing ring, the fraction of dynamic recrystallization is calculated and recrystallized grains size are predicated. Meanwhile, the effects of the initial rolling temperature and feed rate of idle roll on material microstructure evolution are analyzed. Finally, the industrial rolling experiment is designed and performed, based on the simulation results. In addition, mechanical and metallographic tests are conducted on rolled bearing ring to get the mechanical parameters and metallographic structure. The experimental data and results show that the mechanical properties of bearing ring produced by casting-rolling compound forming technology are up to industrial standard, and a qualified bearing ring can be successfully formed by employing this new technology. Through the study, a process of forming large bearing ring directly by using casting ring blank is obtained, which could provide an effective theoretical guidance for manufacturing large ring parts. It also has an edge in saving material, lowering energy and improving efficiency.
基金Funded by the Key Research and Development Program of Shanxi Province (No.201903D121040)。
文摘The effect of solution and aging treatments on microstructure and mechanical properties of warm-rolled 7075 alloy was investigated via optical microscope,electron backscattered diffraction,transmission electron microscopy and tensile tests.The 7075 alloy was subjected to solution treatments at 450℃for 1 h(ST1),490℃ for 1 h(ST2)and 1.5 h(ST3).Three aging routes were carried out on samples from ST2:one-step(A1),two-step(A2),and three-step aging(A3).The experimental results show mainly recrystallized equiaxed grains in ST1 and ST3 state but a combination of elongated and equiaxed grains in ST2 condition.Three aged alloys have similar microstructures of sample ST2 while the recrystallization frequency gets decreased after aging.The least recrystallization fraction occurs in A2 state.Three aged 7075 alloys all possess enhanced strength and plasticity.Precipitates characterization reveals the maximum strength is achieved in A2 sample as the matrix precipitates are composed mainly of smallηand manyη′phases.Aging route A2 appears preferable to other two aging conditions for attaining a pretty excellent combination of strength and plasticity.
基金supported by the National Nature Science Foundation of China(No.51802212)the National College Students’Innovation and Entrepreneurship Training Program(No.2021465)+2 种基金the Natural Science Foundation of Shanxi Province,China(No.201801D221119)the Open Foundation of China-Belarus Belt and Road Joint Laboratory on Electromagnetic Environment Effect(Nos.ZBKF2022030802 and ZBKF2022030702)the Graduate Education Innovation Programs of Taiyuan University of Science and Technology(No.XCX212003)。
文摘Under the background of a transformation of the global energy structure,coal gasification technology has a wide application prospect,but its by-product,the coal gasification residue(CGR),is still not being efficiently utilized for recycling.The CGR contains abundant carbon components,which could be applied to the microwave absorption field as the carbon matrix.In this study,Fe/CGR composites are fabricated via a two-step method,including the impregnation of Fe^(3+)and the reduction process.The influence of the different loading capacities of the Fe component on the morphology and electromagnetic properties is studied.Moreover,the loading content of Fe and the surface morphology of the Fe/CGR can be reasonably controlled by adjusting the concentration of the ferric nitrate solution.Meanwhile,Fe particles are evenly inserted on the CGR framework,which expands the Fe/CGR interfaces to enhance interfacial polarization,thus further improving the microwave-absorbing(MA)properties of composites.Particularly,as the Fe^(3+)concentration is 1.0 mol/L,the Fe/CGR composite exhibits outstanding performance.The reflection loss reaches-39.3 dB at 2.5 mm,and the absorption bandwidth covers 4.1 GHz at 1.5 mm.In this study,facile processability,resource recycling,appropriately matched impedance,and excellent MA performance are achieved.Finally,the Fe/CGR composites not only enhance the recycling of the CGR but also pioneer a new path for the synthesis of excellent absorbents.
基金supported by the National Key Research and Development Program of China (No.2018YFA0707300)the National Natural Science Foundation of China (Nos.51905372, 51804215)+1 种基金the State Key Laboratory of Metal Extrusion and Forging Equipment Technology Open-end FundsChengdu Technological University Laboratory Open Fund.
文摘In this paper,the main researches are focused on the horizontal nonlinear vibration characteristics of roll systems for rolling mill,mainly including the study of forced vibration and free vibration of the roller.Firstly,the nonlinear damping parameters and nonlinear stiffness parameters within interface of the rolling mill are both considered,and a fractional-order differential term is also introduced to model the horizontal nonlinear vibration.Secondly,the averaging method is introduced to solve the forced vibration system of the mill roll system,and the amplitude-frequency characteristic curves of the system are obtained for different orders,external excitation amplitudes,stiffness and fractional order coefficients.Thirdly,the amplitude-frequency and phasefrequency characteristics of the free vibration of the mill roll system are investigated at different fractional orders.Then,the accuracy of the averaging method for solving the dynamic characteristics of the system is verified by numerical analysis,and the effect of the fractional differential term coefficients and order on the dynamic characteristics of the roll system are investigated.Finally,the time-frequency characteristics and phase-frequency characteristics of free vibration systems at different fractional orders are studied.The validity of the theoretical study is also verified through experiments.
基金founded by the National Natural Science Foundation of China(Grant No.41772130)the Postgraduate Research&Practice Innovation Program of Jiangsu Province(Grant No.KYCX22_2602)+1 种基金the Graduate Innovation Program of China University of Mining and Technology(Grant No.2022WLKXJ035)the Fundamental Research Program of Shanxi Province(Grant No.202103021223283)。
文摘The continuously collected cores from the Permo-Carboniferous coal-bearing strata of the eastern Ordos Basin are essential for studying the hydrocarbon potential in this region.This study adopted sedimentological and geochemical methods to analyze the sedimentary environment,material composition,and geochemical characteristics of the coal-bearing strata.The differences in depositional and paleoclimatic conditions were compared;and the factors influencing the organic matter content of fine-grained sediments were explored.The depositional environment of the Benxi and Jinci formations was lagoon to tidal flat with weakly reduced waters with low salinity and dry-hot paleoclimatic conditions;while that of the Taiyuan Formation was a carbonate platform and shallow water delta front,where the water was highly reductive.The xerothermic climate alternated with the warm and humid climate.The period of maximum transgression in the Permo-Carboniferous has the highest water salinity.The Shanxi Formation was deposited in a shallow water delta front with a brackish and fresh water environment and alternative weak reductiveness.And the paleoclimate condition is dry-hot.The TOC content in fine-grained samples was averaging 1.52%.The main controlling mechanism of organic matter in this area was the input conditions according to the analysis on input and preservation of organic matter.
基金Project supported by the National Natural Science Foundation of China (Grant Nos. 52074246, 52275390, 52205429, and 52201146)the National Defense Basic Scientific Research Program of China (Grant Nos. JCKY2020408B002 and WDZC2022-12)+1 种基金the Science and Technology Major Project of Shanxi Province, China (Grant Nos. 20191102008 and 20191102007)the Guiding Local Science and Technology Development Projects by the Central Government, China (Grant Nos. YDZJSX2022A025 and YDZJSX2021A027)。
文摘Parameter calculation and result storage, as two necessary steps in phase-field simulation play an important role in ensuring the accuracy of simulation results. A strategy of parameter calculation and result storage is presented for phase-field simulation in α-Mg dendrite growth of Mg-5-wt% Zn alloy under isothermal solidification. Based on the phase diagram and empirical formulas, key parameters of the phase-field model, such as equilibrium partition coefficient k, liquidus slope m, solutal diffusion coefficient in liquid Dl, and solutal diffusion coefficient in solid Ds, can be obtained.Both structured grid method and structured point method can be used to store simulation results, but using the latter method will reduce about 60% storage space and 37.5% storage time compared with the former. Finally, convergent simulation results of α-Mg dendrite growth are obtained and they are in good agreement with the experimental results about optical micrograph, which verify the accuracy of parameters and stability of storage method.
基金Funded by the Central Government Guides Local Funds for Science and Technology Development(No.YDZJSX20231A045)the Fundamental Research Program of Shanxi Province(Nos.202103021223288 and 202103021224282)。
文摘The evolution of microstructure during hot deformation is key to achieving good mechanical properties in aluminum alloys.We have developed a cellular automaton(CA) based model to simulate the microstructural evolution in 7075 aluminum alloy during hot deformation.Isothermal compression tests were conducted to obtain material parameters for 7075 aluminum alloy,leading to the establishment of models for dislocation density,nucleation of recrystallized grains,and grain growth.Integrating these aspects with grain topological deformation,our CA model effectively predicts flow stress,dynamic recrystallization(DRX) volume fraction,and average grain size under diverse deformation conditions.A systematic comparison was made between electron back scattered diffraction(EBSD) maps and CA model simulated under different deformation temperatures(573 to 723 K),strain rates(0.001 to 1 s^(-1)),and strain amounts(30% to 70%).These analyses indicate that large strain,high temperature,and low strain rate facilitate dynamic recrystallization and grain refinement.The results from the CA model show good accuracy and predictive capability,with experimental error within 10%.
基金National Natural Science Foundation of China(Grant No.21975227)the Found of National defence Science and Technology Key Laboratory (Grant No.6142602210306)。
文摘Fe/N-based biomass porous carbon composite(Fe/N-p Carbon) was prepared by a facile high-temperature carbonization method from biomass,and the effect of Fe/N-p Carbon on the thermal decomposition of energetic molecular perovskite-based material DAP-4 was studied.Biomass porous carbonaceous materials was considered as the micro/nano support layers for in situ deposition of Fe/N precursors.Fe/Np Carbon was prepared simply by the high-temperature carbonization method.It was found that it showed the inherent catalysis properties for thermal decomposition of DAP-4.The heat release of DAP-4/Fe/N-p Carbon by DSC curves tested had increased slightly,compared from DAP-4/Fe/N-p Carbon-0.The decomposition temperature peak of DAP-4 at the presence of Fe/N-p Carbon had reduced by 79°C from384.4°C(pure DAP-4) to 305.4°C(DAP-4/Fe/N-p Carbon-3).The apparent activation energy of DAP-4thermal decomposition also had decreased by 29.1 J/mol.The possible catalytic decomposition mechanism of DAP-4 with Fe/N-p Carbon was proposed.
基金funded by the National Natural Science Foundation of China(Grant Number 52075361)Shanxi Province Science and Technology Major Project(Grant Number 20201102003)+3 种基金Lvliang Science and Technology Guidance Special Key R&D Project(Grant Number 2022XDHZ08)National Natural Science Foundation of China(Grant Number 51905367)Shanxi Natural Science Foundation General Project(Grant Numbers 202103021224271,202203021211201)Shanxi Province Key Research and Development Plan(Grant Number 202102020101013).
文摘In the fiber winding process,strong disturbance,uncertainty,strong coupling,and fiber friction complicate the winding constant tension control.In order to effectively reduce the influence of these problems on the tension output,this paper proposed a tension fluctuation rejection strategy based on feedforward compensation.In addition to the bias harmonic curve of the unknown state,the tension fluctuation also contains the influence of bounded noise.A tension fluctuation observer(TFO)is designed to cancel the uncertain periodic signal,in which the frequency generator is used to estimate the critical parameter information.Then,the fluctuation signal is reconstructed by a third-order auxiliary filter.The estimated signal feedforward compensates for the actual tension fluctuation.Furthermore,a time-varying parameters fractional-order PID controller(TPFOPID)is realized to attenuate the bounded noise in the fluctuation.Finally,TPFOPID is enhanced by TFO and applied to control a tension control system considering multi-source disturbances.The stability of the method is analyzed by using the Lyapunov theorem.Finally,numerical simulations verify that the proposed scheme improves the tracking ability and robustness of the system in response to tension fluctuations.
基金supported in part by the Central Government Guides Local Science and TechnologyDevelopment Funds(Grant No.YDZJSX2021A038)in part by theNational Natural Science Foundation of China under(Grant No.61806138)in part by the China University Industry-University-Research Collaborative Innovation Fund(Future Network Innovation Research and Application Project)(Grant 2021FNA04014).
文摘The large-scale multi-objective optimization algorithm(LSMOA),based on the grouping of decision variables,is an advanced method for handling high-dimensional decision variables.However,in practical problems,the interaction among decision variables is intricate,leading to large group sizes and suboptimal optimization effects;hence a large-scale multi-objective optimization algorithm based on weighted overlapping grouping of decision variables(MOEAWOD)is proposed in this paper.Initially,the decision variables are perturbed and categorized into convergence and diversity variables;subsequently,the convergence variables are subdivided into groups based on the interactions among different decision variables.If the size of a group surpasses the set threshold,that group undergoes a process of weighting and overlapping grouping.Specifically,the interaction strength is evaluated based on the interaction frequency and number of objectives among various decision variables.The decision variable with the highest interaction in the group is identified and disregarded,and the remaining variables are then reclassified into subgroups.Finally,the decision variable with the strongest interaction is added to each subgroup.MOEAWOD minimizes the interactivity between different groups and maximizes the interactivity of decision variables within groups,which contributed to the optimized direction of convergence and diversity exploration with different groups.MOEAWOD was subjected to testing on 18 benchmark large-scale optimization problems,and the experimental results demonstrate the effectiveness of our methods.Compared with the other algorithms,our method is still at an advantage.
基金This work was funded by grants from the Fundamental Research Funds for the Central Universities,China(KYT202001 and JCQY201901)the Special Fund for Agro-scientific Research in the Public Interest,China(201503112).
文摘Foot and root rot caused by Phytophthora parasitica is a substantial threat to citrus cultivation,affecting both yield and quality.Thus,rapid and accurate detection of P.parasitica plays an important role in disease management.The aim of this study was to develop a simple diagnostic method to detect P.parasitica infection by combining recombinase polymerase amplification and lateral flow strips(LF-RPA).To establish the LF-RPA assay of P.parasitica,the primers and probe designed based on the Ypt1 gene were tested for specificity to P.parasitica,which showed no cross-reactivity with DNAs of other related oomycete species.The LF-RPA assay detected the amount of genomic DNA of P.parasitica which was as low as 1 pg.To make the LF-RPA assay useful in low-resource settings,four simplified DNA extraction methods were compared,after which the LF-RPA assay was applied,with no specialized equipment,to analyze a diverse range of citrus tissues by using a simplified PEG-NaOH method for DNA extraction.This method was successful in detecting P.parasitica in infected plant samples within 30 min.Combining the LF-RPA assay and a simplified DNA extraction method could be a potential detection test for P.parasitica,especially in areas with limited resources.
基金supported by Key Program of National Natural Science Foundation of China (Grant No. 51135007)National Natural Science Foundation of China (Grant No. 51075290)+1 种基金Shanxi Provincial Science and Technology Planning Project of China (Grant No. 20100321083)Shanxi Provincial Foundation for Returnees of China (Grant No.2011011025-1)
文摘The existing researches of hot ring rolling process are mainly based on forged billet. Compared with the existing process, the new ring casting-rolling compound forming process has significant advantages in saving materials and energy, reducing emission and reducing the production cost. The microstructure evolution of the casting materials during hot deformation is the basis of the research of the new process. However, the researches on the casting materials are rare. The metadynamic recrystallization of the as-cast 42CrMo steel after normalizing and tempering during the hot compression is investigated. The tests are performed on the Gleeble-1500 thermal-mechanical simulator. The influence rule of the deformation parameters on the metadynamic recrystallization is obtained by analyzing the experimental data. The kinetic model of the metadynamic recrystallization is deduced. The analysis results show that the metadynamic recrystallization fraction increases with the increase of the deformation temperature and the strain rate. The metallographic experiments are used to investigate the influence rule of the deformation parameters on the grain size of the metadynamic recrystallization. The experimental results show that the grain of the metadynamic recrystallization could be refined with the increase of the strain rate and the decrease of the deformation temperature during hot compression. The occurrence of the metadynamic recrystallization during the hot deformation is more difficult in as-cast 42CrMo steel than in forged 42CrMo steel. The research can provide the foundation for the further research of the hot deformation behaviors of the as-cast structure and theoretical support for the new ring casting-rolling compound process.
基金supported by the National Natural Science Foundation of China (No.20876104 and No.21176168)the Science and Technology Foundation of Shanxi Province,China (No.20090311082)
文摘A novel photocatalyst,bismuth oxychloride(BiOCl) micro-nano particles with a fine ferrite plate structure,was prepared by a low-cost,simple hydrolytic method.The as-prepared BiOCl was characterized by scanning electron microscopy(SEM),thermogravimetric analysis-differential thermal analysis(TGA-DTA),X-ray diffraction(XRD),and UV-vis diffuse reflectance spectra(DRS).The effects of preparation conditions such as sodium dodecyl benzene sulfonate(SDBS) dispersant,HCl concentration,and heat treatment temperature on BiOCl performances were investigated.Moreover,its photocatalytic activity was evaluated on the degradation of methylene orange(MO) and was compared with that of TiO 2(P25).The experimental results confirmed that BiOCl micro-nano particles prepared with SDBS,the HCl concentration of 1.5 mol/L,and the heat treatment temperature of 80°C exhibited the best performance for the photodegradation of MO solution,and they showed good stability and better photocatalytic activity than P25 photocatalyst.
基金Item Sponsored by National Natural Science Foundation of China (50274050) and Shanghai Baoshan Iron and Steel Group
文摘To understand the solidification behavior of austenitic stainless steel in pulsed magnetic field, the solidification process is investigated by means of the self-made high voltage pulse power source and the solidification tester. The results show that the solidification structure of austenitic stainless steel can be remarkably refined in pulsed magnetic field, yet the grains become coarse again when the magnetic intensity is exceedingly large, indicating that an optimal intensity range existed for structure refinement. The solidification temperature can be enhanced with an increase in the magnetic intensity. The solidification time is shortened obviously, but the shortening degree is reduced with the increase of the magnetic intensity.
文摘Hot deformation behaviors of TC11 alloy with β-annealed lamellar structure and forged equiaxed structure were investigated in the β field in the temperature range of 1 090-1 030 ℃ and strain rate of 0.001-0.1 s-1 by means of isothermal compression tests.Hot deformation characteristics and microstructure evolutions of the two starting structures were analyzed.And hot processing power dissipation efficiency maps were established.EBSD technique was used for testing grain boundary characteristic of deformation structures.The results indicate that hot deformation mechanism of TC11 alloy in β field is dynamic recovery accompanied by geometric dynamic recrystallization at large strains,or discontinuous dynamic recrystallization based on the starting structure states and deformation parameters.Accordingly,there are two different grain refining patterns.One is characteristic of new fine grains in the interior of elongated prior β grains that have serrated grain boundaries; and the other is that of new fine grains along elongated prior β grain boundaries.
基金Funded by the National Natural Science Foundation of Shanxi Province(No.2013011011-6)the Subject Team of Taiyuan University of Science and Technology
文摘Two coordination polymers, namely {[Ni(cpna)(H2biim)(H2O)]·H2O}n(1) and {[Mn(cpna)(H2biim)]·H2O}n(2)(H2cpna = 5-(2'-carboxylphenyl) nicotic acid, H2biim = 2,2'-biimidazole),have been hydrothermally synthesized and characterized by elemental analysis, IR, TG, magnetic properties, and single-crystal X-ray diffraction. Compound 1 exhibits a one- dimensional(1D) step-like chain structure, which further builds a three-dimensional(3D) supramolecular architecture via O–H···O and N–H···O hydrogen-bonding and π-π stacking interactions. Compound 2 possesses a one-dimensional(1D) double chain structure, which is further assembled into a 3D supramolecular framework by N–H···O hydrogen bonding and π-π stacking interactions. Magnetic susceptibility measurement indicates that compound 1 shows a weak antiferromagnetic coupling between the nearest Ni(II) centers, with g = 2.11 and J = –1.87 cm–1.
基金Supported by National "Twelfth Five-Year" Plan for Science&Technology Support of China(Grant No.2011BAK06B05)National High-tech Research and Development Program of China(863 Program,Grant No.2013AA040203)Shanxi Scholarship Council of China(Grant No.2015-088)
文摘Static load tests are an important means of supervising and detecting a crane's lift capacity. Due to space restrictions, however, there are difficulties and potential danger when testing large bridge cranes. To solve the loading problems of large-tonnage cranes during testing, an equivalency test is proposed based on the similarity theory and BP neural networks. The maximum stress and displacement of a large bridge crane is tested in small loads, combined with the training neural network of a similar structure crane through stress and displacement data which is collected by a physics simulation progressively loaded to a static load test load within the material scope of work. The maximum stress and displacement of a crane under a static load test load can be predicted through the relationship of stress, displacement, and load. By measuring the stress and displacement of small tonnage weights, the stress and displacement of large loads can be predicted, such as the maximum load capacity, which is 1.25 times the rated capacity. Experimental study shows that the load reduction test method can reflect the lift capacity of large bridge cranes. The load shedding predictive analysis for Sanxia 1200 t bridge crane test data indicates that when the load is 1.25 times the rated lifting capacity, the predicted displacement and actual displacement error is zero. The method solves the problem that lifting capacities are difficult to obtain and testing accidents are easily possible when 1.25 times related weight loads are tested for large tonnage cranes.
基金supported by National Natural Science Foundation of China (No.50675145)Shanxi Province Key Project of Science and Technology of China (No.2006031147)+1 种基金Shanxi Province Innovation Project for Graduate Students of China (No.20061027)the Shanxi Province Key Project for Studied-abroad Returnee of China.
文摘In spline rolling process,the contact area between roller and workpiece plays an important role in calculating rolling-force and rolling-moment.For the purpose of studying the contact area, contact state between roller and workpiece in process of spline cold rolling based upon cross rolling is analyzed.According to the suitable hypothesis,the mathematic model of roller-tooth-curve in optional position of rolling process is established.Combing the theory of conjugate curves with the theory of envelope curve,the corresponding mathematic model of workpiece-tooth-curve is established.By utilizing establishing mathematic models,the algorithm of entire contact area in rolling process is created.On the basis of the algorithm,calcuiation-prograrn is compiled under MATLAB program language environment.The calcuiation-program actualizes quantitative analysis and quantitative calculation of contact areas.Utilizing the calculation-program,the influence of parameters on contact area is analyzed,and the tendency is consistent with the manufacturing experience.In consideration of rolling-force optimization,the primary process parameters may be selected according to results of calculation.The result of the present study may provide basis for research on rolling-force and rolling-moment.
基金Supported by National Natural Science Foundation of China(Grant Nos.51675361,51575371)Key Program of National Natural Science Foundation of China(Grant No.51135007)Key Research Project of Shanxi Province(Grant No.03012015004)
文摘Research on compact manufacturing technology for shape and performance controllability of metallic components can realize the simplification and high-reliability of manufacturing process on the premise of satisfying the requirement of macro/micro-structure. It is not only the key paths in improving performance, saving material and energy, and green manufacturing of components used in major equipments, but also the challenging subjects in frontiers of advanced plastic forming. To provide a novel horizon for the manufacturing in the critical components is significant. Focused on the high-performance large-scale components such as bearing rings, flanges, railway wheels, thick-walled pipes, etc, the conventional processes and their developing situations are summarized. The existing problems including multi-pass heating, wasting material and energy, high cost and high-emission are discussed, and the present study unable to meet the manufacturing in high-quality components is also pointed out. Thus, the new techniques related to casting-rolling compound precise forming of rings, compact manufacturing for duplex-metal composite rings, compact manufacturing for railway wheels, and casting-extruding continuous forming of thick-walled pipes are introduced in detail, respectively. The corresponding research contents, such as casting ring blank, hot ring rolling, near solid-state pressure forming, hot extruding, are elaborated. Some findings in through-thickness microstructure evolution and mechanical properties are also presented. The components produced by the new techniques are mainly characterized by fine and homogeneous grains. Moreover, the possible directions for further development of those techniques are suggested. Finally, the key scientific problems are first proposed. All of these results and conclusions have reference value and guiding significance for the integrated control of shape and performance in advanced compact manufacturing.
